Database of Zeolite Structures
 
Framework Type RTE
29Si CP MAS NMR spectrum of as-made pure silica RUB-3


Note: Toggle plots by clicking on the legend

Peak
Q-type
Chemical Shift
Relative
Peak Width
Peak Shape
Label
(ppm)
Peak Area
(ppm)
(x)L (1-x)G
A
Q4(0Al)
-115.82
1.000
0.60
0.744
B
Q4(0Al)
-113.14
1.000
0.56
0.744
C
Q4(0Al)
-112.57
1.000
0.56
0.744


References
Spectrum

  Authors: Marler, B., Grünewald-Lüke, A. and Gies, H.
  Title: Decasils, a new order-disorder family of microporous silicas
  Reference: Zeolites, 15, 388-399 (1995)
  Figure: Figure 7  

Crystal Structure

  Authors: Marler, B., Grünewald-Lüke, A. and Gies, H.
  Title: Structure refinement of the as-synthesized and the calcined form of zeolite RUB-3 (RTE)
  Reference: Microporous Mesoporous Mat., 26, 49-59 (1998)

Digitization and Modeling of Spectrum

  To reference this collection of solid-state NMR spectra, we suggest:
  Authors: Brouwer, D.H., Brouwer, C.C., Mesa, S., Semelhago, C.A., Steckley, E.E., Sun, M.P.Y., Mikolajewski, J.G., and Baerlocher, Ch.
  Title: Solid-state 29Si NMR spectra of pure silica zeolites for the International Zeolite Association Database of Zeolite Structures
  Reference: Microporous Mesoporous Mat., 297, 110000 (2020)
Spectrum information

  Obs. freq. 59.6 MHz (Field = 7 Tesla)
  Pulse sequence cross polarization
  Spectrum Digitized and processed by Brouwer Lab, Redeemer University
  Data processing Spectrum digitized with WebPlotDigitizer and deconvoluted with Mathematica notebook
 

Chemical Formula

  |(ABH)2 | [Si24O48]-RTE
ABH = C7H13N = exo-2-aminobicyclo[2.2.1.]heptane
= bicyclo[2.2.1]heptan-2-amine
SMILES: C1CC2CC1CC2N
Images:  stick or 

Downloads

  Download digitized spectrum in JCAMP-DX format
(This file includes also the data listed on this page)
  Download all lines from the above plot in .csv format
(This file contains only the plotted data)

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