Database of Zeolite Structures
 
Framework Type SOD
31P MAS NMR spectrum of calcined AlPO-SOD


Note: Toggle plots by clicking on the legend

Peak
T site
Q-type
Chemical Shift
Relative
Peak Width
Peak Shape
Assigment
(topological)
(ppm)
Peak Area
(ppm)
(x)L (1-x)G
P1
T1
Q4(4Al)
-28.88
1.000
2.41
0.453


References
Spectrum

  Authors: Roux, M., Marichal, C., Paillaud, J.L., Fernandez, C., Baerlocher, C., Chezeau, J.M.
  Title: Structural investigation by multinuclear solid state NMR and X-ray diffraction of as-synthesized, dehydrated, and calcined AlPO4-SOD
  Reference: J. Phys. Chem. B, 105, 9083-9092 (2001)
  Figure: Figure 15a  

Peak Assignment

  Authors: Roux, M., Marichal, C., Paillaud, J.L., Fernandez, C., Baerlocher, C., Chezeau, J.M.
  Title: Structural investigation by multinuclear solid state NMR and X-ray diffraction of as-synthesized, dehydrated, and calcined AlPO4-SOD
  Reference: J. Phys. Chem. B, 105, 9083-9092 (2001)
  Method: single peak
  Figure: Figure 15a, Table 8  

Crystal Structure

  Authors: Roux, M., Marichal, C., Paillaud, J.L., Fernandez, C., Baerlocher, C., Chezeau, J.M.
  Title: Structural investigation by multinuclear solid state NMR and X-ray diffraction of as-synthesized, dehydrated, and calcined AlPO4-SOD
  Reference: J. Phys. Chem. B, 105, 9083-9092 (2001)

Digitization and Modeling of Spectrum

  To reference this collection of solid-state NMR spectra, we suggest:
  Authors: Brouwer, D.H. and White, A.L.
  Title: A comprehensive collection of solid-state 31P NMR spectra of aluminophosphate zeolites.
  Reference: Microporous Mesoporous Mat., 337, 111934 (2022)
Spectrum information

  Obs. freq. 161.9 MHz (Field = 9.4 Tesla)
  Pulse sequence single pulse
  MAS frequency 3.5-8 kHz
  Spectrum Digitized and processed by Brouwer Lab, Redeemer University
  Data processing Spectrum digitized with WebPlotDigitizer and deconvoluted with Mathematica notebook
 
  CommentThe additional peaks are spinning sidebands.

Chemical Formula

  [Al - P - O]-SOD

Downloads

  Download digitized spectrum in JCAMP-DX format
(This file includes also the data listed on this page)
  Download all lines from the above plot in .csv format
(This file contains only the plotted data)

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