##TITLE= "29Si MAS NMR spectrum of dehydrated JBW" ##JCAMP-DX= 5.01 ##DATA TYPE= NMR SPECTRUM ##DATA CLASS= XYDATA ##ORIGIN= "Asselman et al., Chem. Mater. , (2022), Figure 3 center left" ##OWNER= "processed by H. Koller, University of Münster" ##LONG DATE= 17.08.2022 10:00 ##SOURCE REFERENCE= JBW-29Si-Asselman-2022-JBW_dehydrated ##DATA PROCESSING= "Spectrum digitized with WebPlotDigitizer and deconvoluted with dmfit: D. Massiot et al., Magn. Reson. Chem., 40, 70-76 (2002)" $$Sample information ##NAMES= JBW ##NAMES= "dehydrated JBW" ##NAMES= "dehydrated JBW" ##SAMPLE DESCRIPTION= "dehydrated JBW" ##TEMPERATURE= N.A. " $$Bibliographic information" ##$AUTHORS= "Asselman, K.; Radhakrishnan, S.; Pellens, N.; Chandran, C.V.; Houlleberghs, M.; Xu, Y.; Martens, J.A.; Sree, S.P.; Kirschhock, C.E.A.; Breynaert, E." ##$TITLE= "HSIL-Based Synthesis of Ultracrystalline K,Na-JBW, a Zeolite Exhibiting Exceptional Framework Ordering and Flexibility" ##$JOURNAL= Chem. Mater. ##$VOLUME= ##$PAGES= in press ##$YEAR= 2022 ##$DOI= 10.1021/acs.chemmater.2c01059 ##$FIGURE= Fig. 3 center left $$Peak information (Positions in ppm, Relative peak areas, Peak widths in ppm, Lorentzian/Gaussian shape parameter) ##$NUM PEAKS= 3 ##$PEAK TSITES= 0 0 0 ##$PEAK LABELS= A B C ##$Q TYPE= Q4(4Al) Q4(4Al) Q4(4Al) ##$PEAK POSITIONS= -83.47 -85.19 -87.18 ##$PEAK AREAS= 0.3139 0.3208 0.3654 ##$PEAK WIDTHS= 1.25 1.47 1.52 ##$PEAK SHAPES= 0 0.25 0.27 ##$PEAK_CQ= ##$PEAK_etaQ= ##$NUMBERING REF= #BEZUG! ##$ASSIGN REF= #BEZUG! ##$ASSIGN METHOD= $$Spectrum acquisition information ##.OBSERVE NUCLEUS= 29Si ##.OBSERVE FREQUENCY= 59.62 ##.PULSE SEQUENCE= single pulse ##.MAS FREQUENCY= 10 $$Spectrum data information ##XUNITS= ppm ##YUNITS= arbitrary units ##FIRSTX= -79.10 ##LASTX= -92.85 ##XFACTOR= 1 ##YFACTOR= 1 ##NPOINTS= 276 ##FIRSTY= 0.0271 $$Spectrum data ##XYDATA= (X++(Y..Y)) -79.1000 0.0272 -79.1500 0.0230 -79.2000 0.0196 -79.2500 0.0176 -79.3000 0.0041 -79.3500 0.0026 -79.4000 0.0017 -79.4500 0.0027 -79.5000 0.0030 -79.5500 0.0034 -79.6000 0.0148 -79.6500 0.0173 -79.7000 0.0190 -79.7500 0.0194 -79.8000 0.0189 -79.8500 0.0179 -79.9000 0.0121 -79.9500 0.0031 -80.0000 -0.0009 -80.0500 -0.0080 -80.1000 -0.0138 -80.1500 -0.0175 -80.2000 -0.0193 -80.2500 -0.0194 -80.3000 -0.0158 -80.3500 -0.0104 -80.4000 -0.0043 -80.4500 0.0013 -80.5000 0.0018 -80.5500 0.0160 -80.6000 0.0188 -80.6500 0.0200 -80.7000 0.0200 -80.7500 0.0195 -80.8000 0.0189 -80.8500 0.0172 -80.9000 0.0155 -80.9500 0.0111 -81.0000 0.0065 -81.0500 0.0041 -81.1000 0.0078 -81.1500 0.0121 -81.2000 0.0157 -81.2500 0.0167 -81.3000 0.0185 -81.3500 0.0189 -81.4000 0.0193 -81.4500 0.0188 -81.5000 0.0179 -81.5500 0.0165 -81.6000 0.0124 -81.6500 0.0052 -81.7000 0.0033 -81.7500 0.0021 -81.8000 0.0023 -81.8500 0.0032 -81.9000 0.0038 -81.9500 0.0175 -82.0000 0.0185 -82.0500 0.0245 -82.1000 0.0388 -82.1500 0.0550 -82.2000 0.0692 -82.2500 0.0826 -82.3000 0.1008 -82.3500 0.1181 -82.4000 0.1334 -82.4500 0.1583 -82.5000 0.1876 -82.5500 0.2201 -82.6000 0.2598 -82.6500 0.3013 -82.7000 0.3452 -82.7500 0.4011 -82.8000 0.4513 -82.8500 0.4955 -82.9000 0.5401 -82.9500 0.5848 -83.0000 0.6342 -83.0500 0.6856 -83.1000 0.7495 -83.1500 0.7998 -83.2000 0.8470 -83.2500 0.8943 -83.3000 0.9279 -83.3500 0.9650 -83.4000 0.9830 -83.4500 0.9931 -83.5000 1.0001 -83.5500 0.9936 -83.6000 0.9797 -83.6500 0.9568 -83.7000 0.9306 -83.7500 0.9017 -83.8000 0.8707 -83.8500 0.8380 -83.9000 0.8044 -83.9500 0.7702 -84.0000 0.7361 -84.0500 0.7026 -84.1000 0.6703 -84.1500 0.6397 -84.2000 0.6113 -84.2500 0.5858 -84.3000 0.5637 -84.3500 0.5515 -84.4000 0.5482 -84.4500 0.5478 -84.5000 0.5519 -84.5500 0.5586 -84.6000 0.5711 -84.6500 0.5865 -84.7000 0.6216 -84.7500 0.6433 -84.8000 0.6724 -84.8500 0.6956 -84.9000 0.7161 -84.9500 0.7366 -85.0000 0.7536 -85.0500 0.7665 -85.1000 0.7776 -85.1500 0.7837 -85.2000 0.7873 -85.2500 0.7859 -85.3000 0.7819 -85.3500 0.7738 -85.4000 0.7566 -85.4500 0.7386 -85.5000 0.7231 -85.5500 0.7042 -85.6000 0.6813 -85.6500 0.6551 -85.7000 0.6273 -85.7500 0.6062 -85.8000 0.5827 -85.8500 0.5634 -85.9000 0.5409 -85.9500 0.5251 -86.0000 0.5120 -86.0500 0.5018 -86.1000 0.4936 -86.1500 0.4899 -86.2000 0.4878 -86.2500 0.4869 -86.3000 0.4868 -86.3500 0.4923 -86.4000 0.5014 -86.4500 0.5163 -86.5000 0.5330 -86.5500 0.5517 -86.6000 0.5722 -86.6500 0.5940 -86.7000 0.6354 -86.7500 0.6750 -86.8000 0.7069 -86.8500 0.7365 -86.9000 0.7605 -86.9500 0.7754 -87.0000 0.7895 -87.0500 0.7993 -87.1000 0.8069 -87.1500 0.8112 -87.2000 0.8098 -87.2500 0.8035 -87.3000 0.7968 -87.3500 0.7844 -87.4000 0.7671 -87.4500 0.7416 -87.5000 0.7027 -87.5500 0.6705 -87.6000 0.6388 -87.6500 0.6117 -87.7000 0.5747 -87.7500 0.5425 -87.8000 0.5024 -87.8500 0.4686 -87.9000 0.4441 -87.9500 0.4232 -88.0000 0.3978 -88.0500 0.3676 -88.1000 0.3274 -88.1500 0.2977 -88.2000 0.2791 -88.2500 0.2489 -88.3000 0.2278 -88.3500 0.2037 -88.4000 0.1873 -88.4500 0.1641 -88.5000 0.1466 -88.5500 0.1275 -88.6000 0.1117 -88.6500 0.1003 -88.7000 0.0891 -88.7500 0.0823 -88.8000 0.0753 -88.8500 0.0688 -88.9000 0.0620 -88.9500 0.0563 -89.0000 0.0507 -89.0500 0.0446 -89.1000 0.0398 -89.1500 0.0348 -89.2000 0.0311 -89.2500 0.0290 -89.3000 0.0268 -89.3500 0.0256 -89.4000 0.0237 -89.4500 0.0214 -89.5000 0.0187 -89.5500 0.0169 -89.6000 0.0156 -89.6500 0.0142 -89.7000 0.0133 -89.7500 0.0133 -89.8000 0.0133 -89.8500 0.0133 -89.9000 0.0139 -89.9500 0.0170 -90.0000 0.0226 -90.0500 0.0311 -90.1000 0.0394 -90.1500 0.0473 -90.2000 0.0550 -90.2500 0.0606 -90.3000 0.0624 -90.3500 0.0621 -90.4000 0.0582 -90.4500 0.0525 -90.5000 0.0455 -90.5500 0.0389 -90.6000 0.0328 -90.6500 0.0275 -90.7000 0.0236 -90.7500 0.0223 -90.8000 0.0217 -90.8500 0.0223 -90.9000 0.0231 -90.9500 0.0231 -91.0000 0.0223 -91.0500 0.0206 -91.1000 0.0175 -91.1500 0.0158 -91.2000 0.0124 -91.2500 0.0128 -91.3000 0.0128 -91.3500 0.0128 -91.4000 0.0128 -91.4500 0.0127 -91.5000 0.0148 -91.5500 0.0165 -91.6000 0.0199 -91.6500 0.0220 -91.7000 0.0229 -91.7500 0.0199 -91.8000 0.0163 -91.8500 0.0143 -91.9000 0.0057 -91.9500 -0.0016 -92.0000 -0.0029 -92.0500 -0.0043 -92.1000 -0.0031 -92.1500 -0.0014 -92.2000 0.0151 -92.2500 0.0210 -92.3000 0.0322 -92.3500 0.0415 -92.4000 0.0488 -92.4500 0.0531 -92.5000 0.0520 -92.5500 0.0470 -92.6000 0.0385 -92.6500 0.0283 -92.7000 0.0188 -92.7500 0.0013 -92.8000 -0.0075 -92.8500 -0.0122 ##END=