29Si MAS NMR spectrum of low Si/Al mordenite ##freq 1 ##ppm Spectrum Model A B C ----- -85.1 0.0337713 0.421006 3.44463e-034 1.55482e-010 0.421006 -85.2 0.248779 0.427238 6.33704e-034 2.03692e-010 0.427238 -85.3 0.444788 0.433609 1.16314e-033 2.6649e-010 0.433609 -85.4 0.667795 0.440123 2.13002e-033 3.48178e-010 0.440123 -85.5 0.944803 0.446782 3.89167e-033 4.54293e-010 0.446782 -85.6 1.18381 0.453592 7.09402e-033 5.91947e-010 0.453592 -85.7 1.27682 0.460558 1.29018e-032 7.70271e-010 0.460558 -85.8 1.11783 0.467684 2.34107e-032 1.00096e-009 0.467684 -85.9 0.773836 0.474974 4.23819e-032 1.29899e-009 0.474974 -86 0.412844 0.482435 7.65507e-032 1.68347e-009 0.482435 -86.1 0.126852 0.49007 1.3795e-031 2.17882e-009 0.49007 -86.2 0.0518606 0.497887 2.48026e-031 2.8161e-009 0.497887 -86.3 0.112869 0.50589 4.44914e-031 3.63488e-009 0.50589 -86.4 0.127876 0.514085 7.96266e-031 4.68538e-009 0.514085 -86.5 0.117885 0.522479 1.42182e-030 6.03132e-009 0.522479 -86.6 0.110893 0.531077 2.53298e-030 7.75343e-009 0.531077 -86.7 0.105901 0.539887 4.50218e-030 9.9538e-009 0.539887 -86.8 0.0919092 0.548915 7.98395e-030 1.27614e-008 0.548915 -86.9 0.122917 0.558169 1.41259e-029 1.63388e-008 0.558169 -87 0.173925 0.567655 2.49354e-029 2.08908e-008 0.567655 -87.1 0.166934 0.577383 4.39159e-029 2.66749e-008 0.577383 -87.2 0.0719419 0.587359 7.71665e-029 3.40145e-008 0.587359 -87.3 -0.16705 0.597593 1.35282e-028 4.33152e-008 0.597593 -87.4 -0.450042 0.608093 2.36621e-028 5.50844e-008 0.608093 -87.5 -0.610034 0.618868 4.12925e-028 6.9957e-008 0.618868 -87.6 -0.554026 0.629928 7.18938e-028 8.87252e-008 0.629928 -87.7 -0.263018 0.641283 1.24886e-027 1.12377e-007 0.641283 -87.8 0.0989904 0.652943 2.16442e-027 1.42141e-007 0.652943 -87.9 0.426998 0.66492 3.74259e-027 1.79545e-007 0.66492 -88 0.736006 0.677224 6.45662e-027 2.26487e-007 0.677224 -88.1 0.990015 0.689867 1.11133e-026 2.85316e-007 0.689867 -88.2 1.16202 0.702863 1.90845e-026 3.58941e-007 0.702862 -88.3 1.28703 0.716223 3.26982e-026 4.50954e-007 0.716223 -88.4 1.33904 0.729962 5.58947e-026 5.6579e-007 0.729961 -88.5 1.21005 0.744093 9.53278e-026 7.08911e-007 0.744092 -88.6 0.926055 0.758632 1.62208e-025 8.87037e-007 0.758631 -88.7 0.663063 0.773594 2.75377e-025 1.10842e-006 0.773593 -88.8 0.499072 0.788996 4.6643e-025 1.38319e-006 0.788995 -88.9 0.429079 0.804855 7.88223e-025 1.72374e-006 0.804853 -89 0.459088 0.821189 1.32897e-024 2.14524e-006 0.821186 -89.1 0.505096 0.838016 2.23554e-024 2.6662e-006 0.838013 -89.2 0.507104 0.855358 3.75193e-024 3.3092e-006 0.855354 -89.3 0.503112 0.873234 6.28246e-024 4.10173e-006 0.87323 -89.4 0.50512 0.891668 1.04956e-023 5.07719e-006 0.891662 -89.5 0.512128 0.910682 1.7494e-023 6.27617e-006 0.910675 -89.6 0.540136 0.930301 2.9092e-023 7.7478e-006 0.930293 -89.7 0.533145 0.950552 4.82682e-023 9.5516e-006 0.950543 -89.8 0.485153 0.971463 7.9901e-023 1.17594e-005 0.971451 -89.9 0.377161 0.993062 1.31961e-022 1.44581e-005 0.993047 -90 0.140169 1.01538 2.17442e-022 1.77521e-005 1.01536 -90.1 -0.166823 1.03845 3.57474e-022 2.17671e-005 1.03843 -90.2 -0.430815 1.06232 5.86338e-022 2.66541e-005 1.06229 -90.3 -0.564806 1.087 9.59523e-022 3.25944e-005 1.08697 -90.4 -0.590799 1.11256 1.56663e-021 3.98047e-005 1.11252 -90.5 -0.592791 1.13903 2.55199e-021 4.85444e-005 1.13898 -90.6 -0.605783 1.16645 4.14759e-021 5.91231e-005 1.1664 -90.7 -0.588774 1.19489 6.72536e-021 7.19099e-005 1.19482 -90.8 -0.476766 1.22439 1.08802e-020 8.73442e-005 1.2243 -90.9 -0.266758 1.25501 1.75616e-020 0.000105948 1.2549 -91 0.10525 1.28681 2.8281e-020 0.000128341 1.28668 -91.1 0.644258 1.31987 4.54388e-020 0.000155256 1.31972 -91.2 1.34727 1.35426 7.28388e-020 0.000187564 1.35408 -91.3 2.06227 1.39007 1.16494e-019 0.000226288 1.38984 -91.4 2.61528 1.42737 1.85885e-019 0.000272638 1.4271 -91.5 2.99829 1.46628 2.9593e-019 0.000328039 1.46595 -91.6 3.2143 1.50688 4.70044e-019 0.000394165 1.50649 -91.7 3.36431 1.54931 7.44887e-019 0.000472981 1.54884 -91.8 3.52032 1.59369 1.17773e-018 0.000566791 1.59312 -91.9 3.65632 1.64015 1.85782e-018 0.00067829 1.63947 -92 3.59233 1.68885 2.92392e-018 0.000810628 1.68804 -92.1 3.23434 1.73995 4.59124e-018 0.000967479 1.73899 -92.2 2.77035 1.79364 7.1928e-018 0.00115312 1.79249 -92.3 2.42336 1.85012 1.12427e-017 0.00137253 1.84874 -92.4 2.20336 1.90959 1.75325e-017 0.00163148 1.90796 -92.5 2.09237 1.9723 2.72785e-017 0.00193666 1.97036 -92.6 2.06338 2.0385 4.2345e-017 0.00229583 2.03621 -92.7 1.97639 2.10848 6.55822e-017 0.00271794 2.10576 -92.8 1.7274 2.18253 1.01338e-016 0.00321332 2.17931 -92.9 1.4434 2.26098 1.5623e-016 0.00379386 2.25718 -93 1.26241 2.34418 2.40302e-016 0.00447323 2.33971 -93.1 1.26842 2.43253 3.68769e-016 0.00526714 2.42726 -93.2 1.53543 2.52642 5.64617e-016 0.00619358 2.52023 -93.3 1.97044 2.6263 8.62496e-016 0.00727315 2.61903 -93.4 2.48744 2.73265 1.31451e-015 0.00852936 2.72412 -93.5 2.95445 2.84596 1.99882e-015 0.00998905 2.83597 -93.6 3.27746 2.96676 3.0324e-015 0.0116827 2.95508 -93.7 3.54847 3.09563 4.58989e-015 0.0136452 3.08199 -93.8 3.84648 3.23317 6.93141e-015 0.0159157 3.21725 -93.9 4.14549 3.38 1.04434e-014 0.0185391 3.36146 -94 4.36249 3.53678 1.56989e-014 0.0215656 3.51522 -94.1 4.4265 3.70421 2.3545e-014 0.0250525 3.67916 -94.2 4.41551 3.88301 3.52315e-014 0.0290637 3.85394 -94.3 4.40952 4.07391 5.25976e-014 0.0336718 4.04024 -94.4 4.40453 4.27769 7.83438e-014 0.0389578 4.23873 -94.5 4.38753 4.49513 1.16425e-013 0.0450128 4.45012 -94.6 4.44354 4.72706 1.7262e-013 0.0519387 4.67512 -94.7 4.67055 4.97427 2.55352e-013 0.0598494 4.91442 -94.8 5.02356 5.23762 3.76869e-013 0.0688718 5.16875 -94.9 5.46457 5.51793 5.54939e-013 0.0791474 5.43878 -95 5.93958 5.81604 8.15272e-013 0.0908334 5.72521 -95.1 6.33458 6.13279 1.19499e-012 0.104104 6.02868 -95.2 6.69159 6.46898 1.74754e-012 0.119152 6.34983 -95.3 7.0136 6.82542 2.54974e-012 0.136192 6.68923 -95.4 7.22561 7.20287 3.71164e-012 0.155459 7.04741 -95.5 7.40562 7.60207 5.39063e-012 0.177211 7.42485 -95.6 7.56162 8.02368 7.81118e-012 0.201734 7.82194 -95.7 7.72163 8.46833 1.12927e-011 0.229341 8.23898 -95.8 7.96564 8.93654 1.62885e-011 0.260374 8.67617 -95.9 8.34365 9.42877 2.34405e-011 0.295208 9.13356 -96 8.89866 9.94533 3.36555e-011 0.334249 9.61108 -96.1 9.64666 10.4864 4.82114e-011 0.377943 10.1085 -96.2 10.4527 11.052 6.89042e-011 0.426773 10.6253 -96.3 11.1107 11.642 9.82529e-011 0.48126 11.1607 -96.4 11.6697 12.2559 1.39781e-010 0.541971 11.7139 -96.5 12.3387 12.893 1.98406e-010 0.609518 12.2835 -96.6 13.1997 13.5524 2.80972e-010 0.684557 12.8678 -96.7 14.2057 14.2326 3.96986e-010 0.767797 13.4648 -96.8 15.1797 14.9317 5.59617e-010 0.859997 14.0717 -96.9 15.9887 15.6476 7.87063e-010 0.961968 14.6857 -97 16.7627 16.3775 1.10441e-009 1.07458 15.3029 -97.1 17.5877 17.1178 1.54617e-009 1.19875 15.9191 -97.2 18.4358 17.8648 2.15966e-009 1.33546 16.5293 -97.3 19.2408 18.6138 3.00965e-009 1.48576 17.128 -97.4 19.9468 19.3598 4.18457e-009 1.65075 17.7091 -97.5 20.5098 20.0973 5.80482e-009 1.83157 18.2657 -97.6 20.9948 20.8202 8.03396e-009 2.02947 18.7907 -97.7 21.4978 21.5224 1.10936e-008 2.24571 19.2767 -97.8 21.9448 22.1977 1.52835e-008 2.48163 19.716 -97.9 22.2928 22.8401 2.10074e-008 2.73864 20.1014 -98 22.5468 23.4441 2.88089e-008 3.01819 20.4259 -98.1 22.8368 24.0052 3.9417e-008 3.32178 20.6834 -98.2 23.2698 24.5197 5.38076e-008 3.65098 20.8687 -98.3 23.8698 24.9855 7.32837e-008 4.00738 20.9781 -98.4 24.5889 25.4018 9.95805e-008 4.39264 21.0092 -98.5 25.2939 25.7697 1.35003e-007 4.80844 20.9613 -98.6 25.8109 26.092 1.82607e-007 5.25649 20.8355 -98.7 26.0449 26.373 2.4643e-007 5.73854 20.6345 -98.8 26.1009 26.6186 3.31798e-007 6.25633 20.3622 -98.9 26.1249 26.8359 4.45714e-007 6.81164 20.0242 -99 26.2519 27.033 5.97369e-007 7.40623 19.6267 -99.1 26.5839 27.2187 7.98788e-007 8.04185 19.1768 -99.2 27.0409 27.4021 1.06567e-006 8.72024 18.6819 -99.3 27.4219 27.5926 1.41847e-006 9.44309 18.1495 -99.4 27.6509 27.7992 1.88373e-006 10.2121 17.5871 -99.5 27.8799 28.0305 2.49586e-006 11.0287 17.0018 -99.6 28.1879 28.2947 3.29933e-006 11.8947 16.4001 -99.7 28.656 28.5994 4.35145e-006 12.8112 15.7881 -99.8 29.355 28.9512 5.72593e-006 13.7798 15.1713 -99.9 30.29 29.3561 7.51729e-006 14.8017 14.5545 -100 31.337 29.8195 9.84644e-006 15.8778 13.9417 -100.1 32.231 30.3458 1.28677e-005 17.0092 13.3367 -100.2 32.846 30.9388 1.67774e-005 18.1966 12.7422 -100.3 33.209 31.6015 2.18249e-005 19.4406 12.1609 -100.4 33.426 32.3363 2.83259e-005 20.7416 11.5947 -100.5 33.567 33.1451 3.6679e-005 22.0999 11.0451 -100.6 33.756 34.0289 4.73865e-005 23.5153 10.5136 -100.7 34.116 34.9885 6.10795e-005 24.9875 10.0009 -100.8 34.679 36.0239 7.85488e-005 26.5161 9.50768 -100.9 35.5951 37.1348 0.000100783 28.1003 9.03443 -101 36.8941 38.3204 0.000129014 29.7389 8.58134 -101.1 38.3271 39.5792 0.000164774 31.4306 8.14846 -101.2 39.6481 40.9095 0.000209965 33.1736 7.73569 -101.3 40.7751 42.3092 0.000266935 34.9661 7.34282 -101.4 41.8281 43.7755 0.000338586 36.8056 6.96951 -101.5 42.9491 45.3055 0.000428485 38.6897 6.61537 -101.6 44.2731 46.8957 0.000541009 40.6153 6.2799 -101.7 46.0741 48.5425 0.000681518 42.5792 5.96257 -101.8 48.3171 50.2414 0.000856551 44.5778 5.66279 -101.9 50.4691 51.9882 0.00107407 46.6072 5.37991 -102 52.4531 53.7779 0.00134374 48.6633 5.11328 -102.1 54.5582 55.6053 0.00167726 50.7414 4.86221 -102.2 56.7732 57.465 0.00208876 52.8369 4.62601 -102.3 58.9702 59.3513 0.00259526 54.9447 4.40397 -102.4 61.1322 61.2581 0.00321718 57.0595 4.19539 -102.5 63.1112 63.1792 0.003979 59.1756 3.99955 -102.6 64.9532 65.1081 0.00490993 61.2874 3.81577 -102.7 67.0002 67.0383 0.00604477 63.3889 3.64335 -102.8 69.2372 68.9631 0.00742485 65.474 3.48163 -102.9 71.3592 70.8754 0.00909911 67.5364 3.32996 -103 73.3032 72.7685 0.0111253 69.5697 3.18771 -103.1 75.3402 74.6353 0.0135716 71.5675 3.05427 -103.2 77.3902 76.4688 0.0165178 73.5232 2.92907 -103.3 79.3483 78.2621 0.0200574 75.4305 2.81155 -103.4 81.1593 80.0083 0.0242998 77.2828 2.70118 -103.5 82.4923 81.7006 0.029372 79.0738 2.59747 -103.6 83.6553 83.3324 0.0354215 80.797 2.49995 -103.7 84.8763 84.8971 0.042619 82.4463 2.40817 -103.8 86.1453 86.3887 0.0511615 84.0158 2.32172 -103.9 87.5573 87.8011 0.0612754 85.4996 2.24021 -104 88.9793 89.1286 0.0732205 86.8921 2.16329 -104.1 90.3003 90.3661 0.0872936 88.1881 2.09062 -104.2 91.5443 91.5084 0.103833 89.3827 2.02188 -104.3 92.7703 92.5512 0.123223 90.4712 1.95679 -104.4 93.8223 93.4903 0.145898 91.4493 1.89509 -104.5 94.5953 94.3221 0.172351 92.3132 1.83652 -104.6 95.0524 95.0435 0.203132 93.0595 1.78087 -104.7 95.2174 95.652 0.238862 93.6852 1.72792 -104.8 95.3324 96.1456 0.280233 94.1879 1.6775 -104.9 95.4964 96.5228 0.328016 94.5654 1.62942 -105 95.5644 96.7828 0.383065 94.8162 1.58352 -105.1 95.5524 96.9254 0.446329 94.9395 1.53966 -105.2 95.5464 96.9511 0.518847 94.9345 1.4977 -105.3 95.5394 96.8608 0.601766 94.8015 1.45753 -105.4 95.5224 96.6562 0.696336 94.5408 1.41903 -105.5 95.3754 96.3397 0.803921 94.1536 1.3821 -105.6 95.0404 95.9141 0.926 93.6415 1.34664 -105.7 94.6154 95.3831 1.06417 93.0064 1.31257 -105.8 93.9855 94.7509 1.22016 92.2509 1.27981 -105.9 93.0125 94.0222 1.3958 91.3781 1.24829 -106 91.9415 93.2024 1.59307 90.3914 1.21793 -106.1 91.0445 92.2973 1.81404 89.2946 1.18868 -106.2 90.2415 91.3135 2.06094 88.0921 1.16047 -106.3 89.3555 90.2578 2.33606 86.7885 1.13327 -106.4 88.3885 89.1376 2.64185 85.3887 1.107 -106.5 87.2055 87.9606 2.98081 83.8982 1.08164 -106.6 85.7515 86.735 3.35556 82.3223 1.05714 -106.7 84.0015 85.4693 3.76875 80.6671 1.03345 -106.8 82.2395 84.1721 4.22312 78.9385 1.01055 -106.9 80.6355 82.8524 4.72142 77.1426 0.988388 -107 79.0995 81.5192 5.26642 75.2858 0.96694 -107.1 77.6666 80.1816 5.86086 73.3746 0.946175 -107.2 76.3236 78.8488 6.50744 71.4153 0.926062 -107.3 75.3456 77.53 7.20879 69.4146 0.906575 -107.4 74.6866 76.2339 7.96742 67.3788 0.887688 -107.5 74.0926 74.9696 8.7857 65.3145 0.869376 -107.6 73.4616 73.7454 9.66581 63.228 0.851616 -107.7 72.6966 72.5695 10.6097 61.1254 0.834387 -107.8 71.7196 71.4498 11.6191 59.0131 0.817666 -107.9 70.6546 70.3936 12.6953 56.8968 0.801436 -108 69.6636 69.4075 13.8394 54.7824 0.785676 -108.1 68.7606 68.4978 15.0521 52.6754 0.77037 -108.2 67.9316 67.67 16.3334 50.5811 0.755499 -108.3 67.2237 66.9287 17.6832 48.5044 0.741049 -108.4 66.7047 66.278 19.1007 46.4503 0.727002 -108.5 66.3327 65.7209 20.5844 44.4231 0.713345 -108.6 66.0977 65.2597 22.1326 42.427 0.700064 -108.7 65.8937 64.8958 23.7427 40.4659 0.687145 -108.8 65.7387 64.6295 25.4115 38.5434 0.674574 -108.9 65.6877 64.4603 27.1353 36.6627 0.662341 -109 65.6827 64.3866 28.9095 34.8266 0.650433 -109.1 65.6757 64.4059 30.7292 33.0379 0.638839 -109.2 65.6677 64.5147 32.5885 31.2987 0.627547 -109.3 65.7257 64.7087 34.481 29.6111 0.616549 -109.4 65.9437 64.9823 36.3999 27.9766 0.605833 -109.5 66.3708 65.3295 38.3374 26.3967 0.595391 -109.6 66.9268 65.7431 40.2855 24.8724 0.585213 -109.7 67.3218 66.2153 42.2355 23.4045 0.57529 -109.8 67.5208 66.7375 44.1784 21.9935 0.565614 -109.9 67.7188 67.3006 46.1048 20.6396 0.556178 -110 67.9958 67.8947 48.0048 19.343 0.546973 -110.1 68.3048 68.5098 49.8685 18.1033 0.537992 -110.2 68.6108 69.1353 51.6859 16.9203 0.529228 -110.3 68.8588 69.7604 53.4466 15.7931 0.520674 -110.4 69.0848 70.3742 55.1406 14.7212 0.512323 -110.5 69.3378 70.9656 56.7579 13.7035 0.504169 -110.6 69.6668 71.5239 58.2887 12.739 0.496206 -110.7 70.0979 72.0384 59.7236 11.8263 0.488429 -110.8 70.4779 72.4986 61.0535 10.9643 0.480831 -110.9 70.7679 72.8946 62.2699 10.1513 0.473407 -111 71.1049 73.217 63.3649 9.38593 0.466152 -111.1 71.5239 73.457 64.3314 8.66656 0.459061 -111.2 71.8359 73.6065 65.1629 7.99152 0.452129 -111.3 72.0629 73.6582 65.8538 7.35911 0.445351 -111.4 72.4079 73.6058 66.3994 6.7676 0.438723 -111.5 72.6839 73.4436 66.7961 6.21523 0.43224 -111.6 72.7949 73.1673 67.0412 5.70025 0.425899 -111.7 72.7559 72.7734 67.1328 5.22088 0.419695 -111.8 72.4689 72.2595 67.0705 4.77537 0.413625 -111.9 72.0329 71.6242 66.8546 4.36198 0.407684 -112 71.478 70.8674 66.4866 3.97899 0.401869 -112.1 70.843 69.9899 65.969 3.62474 0.396176 -112.2 70.116 68.9936 65.3055 3.29757 0.390603 -112.3 69.233 67.8814 64.5003 2.99587 0.385145 -112.4 68.182 66.657 63.5591 2.71811 0.3798 -112.5 66.917 65.3254 62.488 2.46277 0.374565 -112.6 65.505 63.892 61.2941 2.22841 0.369436 -112.7 64.297 62.3633 59.9852 2.01363 0.364411 -112.8 62.732 60.7463 58.5697 1.81709 0.359487 -112.9 60.631 59.0486 57.0565 1.63752 0.354661 -113 58.798 57.2785 55.4549 1.47371 0.349932 -113.1 57.168 55.4445 53.7747 1.32449 0.345295 -113.2 55.4491 53.5554 52.0259 1.18877 0.34075 -113.3 53.5461 51.6204 50.2185 1.06553 0.336292 -113.4 51.4641 49.6485 48.3629 0.953766 0.331922 -113.5 49.2491 47.6492 46.469 0.852576 0.327635 -113.6 47.0341 45.6314 44.5469 0.761093 0.32343 -113.7 44.7051 43.6042 42.6064 0.678509 0.319305 -113.8 42.0341 41.5763 40.657 0.60407 0.315258 -113.9 39.1991 39.5562 38.7079 0.537072 0.311287 -114 36.4361 37.5519 36.7677 0.47686 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