PST-22 (OH method)
from Verified Synthesis, 4th Edition, 2025, page 348
Diffractometer: XRDynamic500
Wavelength: CuK(alpha 1,2): 1.5406 Å
Data collected by M. Fahda
-----
3.00835563	2694
3.025066899	2489
3.041778168	2412
3.058489437	2377
3.075200706	2302
3.091911975	2255
3.108623244	2218
3.125334513	2207
3.142045782	2051
3.158757051	2020
3.17546832	1926
3.192179589	1894
3.208890858	1870
3.225602127	1834
3.242313396	1745
3.259024665	1703
3.275735934	1682
3.292447203	1733
3.309158472	1613
3.325869741	1597
3.34258101	1622
3.359292279	1546
3.376003548	1604
3.392714817	1470
3.409426085	1459
3.426137354	1465
3.442848623	1436
3.459559892	1453
3.476271161	1408
3.49298243	1415
3.509693699	1458
3.526404968	1354
3.543116237	1357
3.559827506	1328
3.576538775	1372
3.593250044	1305
3.609961313	1324
3.626672582	1254
3.643383851	1232
3.66009512	1285
3.676806389	1220
3.693517658	1311
3.710228927	1236
3.726940196	1291
3.743651465	1304
3.760362734	1294
3.777074003	1250
3.793785272	1188
3.810496541	1218
3.82720781	1216
3.843919079	1212
3.860630348	1170
3.877341617	1200
3.894052886	1171
3.910764155	1164
3.927475424	1162
3.944186693	1190
3.960897962	1154
3.977609231	1173
3.9943205	1166
4.011031769	1123
4.027743038	1130
4.044454307	1160
4.061165576	1104
4.077876845	1137
4.094588114	1156
4.111299383	1142
4.128010652	1159
4.144721921	1101
4.16143319	1137
4.178144459	1121
4.194855728	1058
4.211566996	1047
4.228278265	1139
4.244989534	1107
4.261700803	1106
4.278412072	1074
4.295123341	1044
4.31183461	1098
4.328545879	1009
4.345257148	1110
4.361968417	1058
4.378679686	1047
4.395390955	1065
4.412102224	1071
4.428813493	1068
4.445524762	1069
4.462236031	1058
4.4789473	1020
4.495658569	991
4.512369838	1023
4.529081107	1027
4.545792376	1062
4.562503645	1028
4.579214914	1008
4.595926183	1041
4.612637452	994
4.629348721	987
4.64605999	1055
4.662771259	1039
4.679482528	1026
4.696193797	965
4.712905066	978
4.729616335	1019
4.746327604	1019
4.763038873	1017
4.779750142	1005
4.796461411	919
4.81317268	967
4.829883949	967
4.846595218	1033
4.863306487	956
4.880017756	1019
4.896729025	946
4.913440294	1016
4.930151563	927
4.946862832	929
4.963574101	935
4.98028537	974
4.996996639	904
5.013707907	927
5.030419176	996
5.047130445	918
5.063841714	952
5.080552983	926
5.097264252	976
5.113975521	887
5.13068679	984
5.147398059	947
5.164109328	951
5.180820597	969
5.197531866	979
5.214243135	928
5.230954404	926
5.247665673	896
5.264376942	921
5.281088211	974
5.29779948	944
5.314510749	916
5.331222018	897
5.347933287	924
5.364644556	924
5.381355825	913
5.398067094	982
5.414778363	919
5.431489632	893
5.448200901	904
5.46491217	929
5.481623439	929
5.498334708	909
5.515045977	924
5.531757246	917
5.548468515	927
5.565179784	848
5.581891053	873
5.598602322	799
5.615313591	924
5.63202486	925
5.648736129	929
5.665447398	866
5.682158667	865
5.698869936	822
5.715581205	902
5.732292474	832
5.749003743	883
5.765715012	876
5.782426281	860
5.799137549	885
5.815848818	824
5.832560087	846
5.849271356	819
5.865982625	861
5.882693894	835
5.899405163	882
5.916116432	838
5.932827701	833
5.94953897	851
5.966250239	861
5.982961508	862
5.999672777	853
6.016384046	806
6.033095315	858
6.049806584	840
6.066517853	858
6.083229122	869
6.099940391	840
6.11665166	827
6.133362929	816
6.150074198	799
6.166785467	780
6.183496736	806
6.200208005	849
6.216919274	866
6.233630543	822
6.250341812	829
6.267053081	778
6.28376435	857
6.300475619	863
6.317186888	804
6.333898157	811
6.350609426	836
6.367320695	796
6.384031964	821
6.400743233	809
6.417454502	776
6.434165771	850
6.45087704	758
6.467588309	812
6.484299578	788
6.501010847	792
6.517722116	789
6.534433385	788
6.551144654	792
6.567855923	785
6.584567192	844
6.60127846	833
6.617989729	782
6.634700998	836
6.651412267	766
6.668123536	782
6.684834805	776
6.701546074	761
6.718257343	732
6.734968612	790
6.751679881	795
6.76839115	786
6.785102419	739
6.801813688	740
6.818524957	781
6.835236226	780
6.851947495	760
6.868658764	812
6.885370033	778
6.902081302	767
6.918792571	753
6.93550384	786
6.952215109	769
6.968926378	793
6.985637647	779
7.002348916	774
7.019060185	726
7.035771454	757
7.052482723	708
7.069193992	765
7.085905261	767
7.10261653	767
7.119327799	776
7.136039068	763
7.152750337	747
7.169461606	732
7.186172875	761
7.202884144	761
7.219595413	723
7.236306682	773
7.253017951	734
7.26972922	755
7.286440489	740
7.303151758	739
7.319863027	698
7.336574296	752
7.353285565	746
7.369996834	692
7.386708103	735
7.403419371	805
7.42013064	721
7.436841909	740
7.453553178	708
7.470264447	719
7.486975716	753
7.503686985	726
7.520398254	756
7.537109523	727
7.553820792	712
7.570532061	748
7.58724333	703
7.603954599	721
7.620665868	688
7.637377137	722
7.654088406	732
7.670799675	732
7.687510944	683
7.704222213	722
7.720933482	702
7.737644751	694
7.75435602	677
7.771067289	700
7.787778558	685
7.804489827	700
7.821201096	728
7.837912365	714
7.854623634	718
7.871334903	716
7.888046172	690
7.904757441	737
7.92146871	708
7.938179979	693
7.954891248	695
7.971602517	717
7.988313786	703
8.005025055	696
8.021736324	704
8.038447593	700
8.055158862	635
8.071870131	706
8.0885814	724
8.105292669	718
8.122003938	684
8.138715207	720
8.155426476	643
8.172137745	720
8.188849013	701
8.205560282	663
8.222271551	649
8.23898282	739
8.255694089	709
8.272405358	702
8.289116627	685
8.305827896	701
8.322539165	687
8.339250434	626
8.355961703	657
8.372672972	712
8.389384241	709
8.40609551	664
8.422806779	716
8.439518048	716
8.456229317	661
8.472940586	696
8.489651855	664
8.506363124	681
8.523074393	699
8.539785662	694
8.556496931	726
8.5732082	683
8.589919469	707
8.606630738	716
8.623342007	684
8.640053276	655
8.656764545	652
8.673475814	751
8.690187083	689
8.706898352	671
8.723609621	647
8.74032089	726
8.757032159	761
8.773743428	671
8.790454697	710
8.807165966	669
8.823877235	719
8.840588504	757
8.857299773	680
8.874011042	728
8.890722311	699
8.90743358	727
8.924144849	716
8.940856118	718
8.957567387	722
8.974278656	697
8.990989924	716
9.007701193	796
9.024412462	738
9.041123731	744
9.057835	710
9.074546269	716
9.091257538	710
9.107968807	725
9.124680076	748
9.141391345	692
9.158102614	756
9.174813883	752
9.191525152	736
9.208236421	758
9.22494769	784
9.241658959	815
9.258370228	812
9.275081497	814
9.291792766	869
9.308504035	932
9.325215304	863
9.341926573	866
9.358637842	1023
9.375349111	1005
9.39206038	1016
9.408771649	1086
9.425482918	1093
9.442194187	1244
9.458905456	1242
9.475616725	1353
9.492327994	1445
9.509039263	1438
9.525750532	1584
9.542461801	1814
9.55917307	1783
9.575884339	1947
9.592595608	2040
9.609306877	2202
9.626018146	2538
9.642729415	2625
9.659440684	2860
9.676151953	3042
9.692863222	3524
9.709574491	3839
9.72628576	4310
9.742997029	4800
9.759708298	5173
9.776419566	5999
9.793130835	6828
9.809842104	7638
9.826553373	8537
9.843264642	9218
9.859975911	9576
9.87668718	9634
9.893398449	8671
9.910109718	7120
9.926820987	5409
9.943532256	3771
9.960243525	2781
9.976954794	1966
9.993666063	1638
10.01037733	1388
10.0270886	1216
10.04379987	1084
10.06051114	1069
10.07722241	1006
10.09393368	844
10.11064495	859
10.12735622	817
10.14406748	834
10.16077875	814
10.17749002	743
10.19420129	793
10.21091256	747
10.22762383	714
10.2443351	765
10.26104637	725
10.27775764	727
10.29446891	717
10.31118017	732
10.32789144	694
10.34460271	701
10.36131398	665
10.37802525	702
10.39473652	698
10.41144779	647
10.42815906	647
10.44487033	660
10.4615816	700
10.47829286	723
10.49500413	645
10.5117154	714
10.52842667	686
10.54513794	675
10.56184921	690
10.57856048	723
10.59527175	709
10.61198302	732
10.62869428	731
10.64540555	748
10.66211682	799
10.67882809	788
10.69553936	797
10.71225063	816
10.7289619	812
10.74567317	846
10.76238444	957
10.77909571	934
10.79580697	982
10.81251824	1033
10.82922951	1098
10.84594078	1124
10.86265205	1181
10.87936332	1206
10.89607459	1328
10.91278586	1369
10.92949713	1498
10.9462084	1731
10.96291966	1793
10.97963093	1958
10.9963422	2172
11.01305347	2485
11.02976474	2649
11.04647601	2979
11.06318728	3149
11.07989855	3134
11.09660982	3118
11.11332109	2774
11.13003235	2270
11.14674362	1835
11.16345489	1424
11.18016616	1082
11.19687743	898
11.2135887	885
11.23029997	767
11.24701124	736
11.26372251	721
11.28043378	629
11.29714504	706
11.31385631	593
11.33056758	635
11.34727885	589
11.36399012	598
11.38070139	580
11.39741266	568
11.41412393	569
11.4308352	563
11.44754646	553
11.46425773	564
11.480969	541
11.49768027	565
11.51439154	578
11.53110281	565
11.54781408	555
11.56452535	567
11.58123662	558
11.59794789	527
11.61465915	591
11.63137042	526
11.64808169	543
11.66479296	566
11.68150423	528
11.6982155	508
11.71492677	561
11.73163804	533
11.74834931	537
11.76506058	573
11.78177184	496
11.79848311	541
11.81519438	530
11.83190565	527
11.84861692	514
11.86532819	540
11.88203946	537
11.89875073	524
11.915462	506
11.93217327	548
11.94888453	523
11.9655958	497
11.98230707	519
11.99901834	535
12.01572961	533
12.03244088	491
12.04915215	489
12.06586342	508
12.08257469	508
12.09928596	501
12.11599722	526
12.13270849	507
12.14941976	509
12.16613103	493
12.1828423	507
12.19955357	490
12.21626484	503
12.23297611	503
12.24968738	470
12.26639864	510
12.28310991	514
12.29982118	491
12.31653245	468
12.33324372	452
12.34995499	459
12.36666626	486
12.38337753	487
12.4000888	494
12.41680007	460
12.43351133	468
12.4502226	512
12.46693387	470
12.48364514	496
12.50035641	512
12.51706768	452
12.53377895	482
12.55049022	502
12.56720149	457
12.58391276	475
12.60062402	473
12.61733529	479
12.63404656	516
12.65075783	457
12.6674691	452
12.68418037	471
12.70089164	457
12.71760291	446
12.73431418	427
12.75102545	440
12.76773671	476
12.78444798	477
12.80115925	491
12.81787052	487
12.83458179	478
12.85129306	483
12.86800433	465
12.8847156	474
12.90142687	469
12.91813814	462
12.9348494	466
12.95156067	465
12.96827194	436
12.98498321	462
13.00169448	448
13.01840575	460
13.03511702	468
13.05182829	455
13.06853956	476
13.08525082	460
13.10196209	464
13.11867336	409
13.13538463	465
13.1520959	470
13.16880717	472
13.18551844	470
13.20222971	453
13.21894098	418
13.23565225	515
13.25236351	440
13.26907478	485
13.28578605	449
13.30249732	441
13.31920859	429
13.33591986	433
13.35263113	476
13.3693424	469
13.38605367	469
13.40276494	416
13.4194762	449
13.43618747	458
13.45289874	457
13.46961001	521
13.48632128	421
13.50303255	467
13.51974382	468
13.53645509	456
13.55316636	454
13.56987763	441
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13.60330016	472
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13.6367227	456
13.65343397	466
13.67014524	412
13.68685651	377
13.70356778	472
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13.73699032	474
13.75370158	427
13.77041285	452
13.78712412	448
13.80383539	405
13.82054666	462
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13.8539692	426
13.87068047	457
13.88739174	432
13.904103	432
13.92081427	420
13.93752554	463
13.95423681	459
13.97094808	436
13.98765935	469
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14.15477204	468
14.17148331	520
14.18819458	504
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14.27175092	569
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14.338596	676
14.35530727	722
14.37201854	682
14.38872981	723
14.40544107	755
14.42215234	728
14.43886361	723
14.45557488	636
14.47228615	580
14.48899742	473
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14.53913123	468
14.55584249	460
14.57255376	473
14.58926503	472
14.6059763	460
14.62268757	481
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14.65611011	428
14.67282138	433
14.68953265	509
14.70624392	493
14.72295518	498
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14.75637772	494
14.77308899	498
14.78980026	535
14.80651153	543
14.8232228	515
14.83993407	577
14.85664534	612
14.87335661	622
14.89006787	674
14.90677914	645
14.92349041	759
14.94020168	799
14.95691295	765
14.97362422	869
14.99033549	962
15.00704676	1012
15.02375803	1157
15.0404693	1170
15.05718056	1425
15.07389183	1515
15.0906031	1737
15.10731437	1950
15.12402564	2268
15.14073691	2361
15.15744818	2789
15.17415945	2975
15.19087072	3107
15.20758199	3184
15.22429325	2964
15.24100452	2693
15.25771579	2299
15.27442706	1967
15.29113833	1667
15.3078496	1264
15.32456087	1107
15.34127214	853
15.35798341	774
15.37469467	630
15.39140594	603
15.40811721	585
15.42482848	573
15.44153975	521
15.45825102	511
15.47496229	481
15.49167356	458
15.50838483	474
15.5250961	425
15.54180736	460
15.55851863	455
15.5752299	441
15.59194117	436
15.60865244	427
15.62536371	450
15.64207498	473
15.65878625	449
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15.69220879	441
15.70892005	459
15.72563132	460
15.74234259	437
15.75905386	491
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15.7924764	436
15.80918767	385
15.82589894	511
15.84261021	433
15.85932148	478
15.87603274	495
15.89274401	522
15.90945528	577
15.92616655	575
15.94287782	505
15.95958909	610
15.97630036	628
15.99301163	682
16.0097229	697
16.02643417	780
16.04314543	828
16.0598567	934
16.07656797	993
16.09327924	1072
16.10999051	1148
16.12670178	1260
16.14341305	1387
16.16012432	1335
16.17683559	1252
16.19354685	1107
16.21025812	927
16.22696939	820
16.24368066	737
16.26039193	624
16.2771032	596
16.29381447	573
16.31052574	560
16.32723701	564
16.34394828	590
16.36065954	641
16.37737081	732
16.39408208	754
16.41079335	779
16.42750462	788
16.44421589	877
16.46092716	917
16.47763843	1005
16.4943497	1139
16.51106097	1365
16.52777223	1430
16.5444835	1674
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