PST-22 (F method)
from Verified Synthesis, 4th Edition, 2025, page 345
Diffractometer: XRDynamic500
Wavelength: CuK(alpha 1,2): 1.5406 Å
Data collected by M. Fahda
-----
3.00835563	3285
3.025066899	3235
3.041778168	3117
3.058489437	3203
3.075200706	2994
3.091911975	2937
3.108623244	2820
3.125334513	2714
3.142045782	2739
3.158757051	2627
3.17546832	2568
3.192179589	2532
3.208890858	2392
3.225602127	2414
3.242313396	2346
3.259024665	2284
3.275735934	2211
3.292447203	2278
3.309158472	2159
3.325869741	2109
3.34258101	2098
3.359292279	2023
3.376003548	2077
3.392714817	2049
3.409426086	2055
3.426137354	1948
3.442848623	2001
3.459559892	1882
3.476271161	1885
3.49298243	1855
3.509693699	1909
3.526404968	1808
3.543116237	1908
3.559827506	1891
3.576538775	1831
3.593250044	1807
3.609961313	1837
3.626672582	1826
3.643383851	1834
3.66009512	1721
3.676806389	1759
3.693517658	1739
3.710228927	1709
3.726940196	1720
3.743651465	1702
3.760362734	1581
3.777074003	1725
3.793785272	1732
3.810496541	1683
3.82720781	1726
3.843919079	1659
3.860630348	1687
3.877341617	1700
3.894052886	1671
3.910764155	1624
3.927475424	1684
3.944186693	1631
3.960897962	1590
3.977609231	1557
3.9943205	1592
4.011031769	1607
4.027743038	1596
4.044454307	1623
4.061165576	1626
4.077876845	1547
4.094588114	1582
4.111299383	1583
4.128010652	1561
4.144721921	1625
4.16143319	1540
4.178144459	1563
4.194855728	1637
4.211566997	1592
4.228278265	1562
4.244989534	1442
4.261700803	1545
4.278412072	1511
4.295123341	1540
4.31183461	1496
4.328545879	1624
4.345257148	1596
4.361968417	1519
4.378679686	1470
4.395390955	1476
4.412102224	1478
4.428813493	1498
4.445524762	1475
4.462236031	1449
4.4789473	1523
4.495658569	1489
4.512369838	1459
4.529081107	1512
4.545792376	1457
4.562503645	1481
4.579214914	1466
4.595926183	1496
4.612637452	1491
4.629348721	1438
4.64605999	1443
4.662771259	1457
4.679482528	1362
4.696193797	1428
4.712905066	1449
4.729616335	1416
4.746327604	1447
4.763038873	1465
4.779750142	1403
4.796461411	1432
4.81317268	1506
4.829883949	1435
4.846595218	1384
4.863306487	1413
4.880017756	1399
4.896729025	1385
4.913440294	1418
4.930151563	1342
4.946862832	1316
4.963574101	1359
4.98028537	1335
4.996996639	1384
5.013707908	1391
5.030419177	1328
5.047130445	1295
5.063841714	1354
5.080552983	1338
5.097264252	1400
5.113975521	1373
5.13068679	1363
5.147398059	1319
5.164109328	1322
5.180820597	1310
5.197531866	1308
5.214243135	1320
5.230954404	1262
5.247665673	1275
5.264376942	1319
5.281088211	1310
5.29779948	1257
5.314510749	1277
5.331222018	1294
5.347933287	1357
5.364644556	1290
5.381355825	1258
5.398067094	1331
5.414778363	1304
5.431489632	1263
5.448200901	1263
5.46491217	1334
5.481623439	1257
5.498334708	1289
5.515045977	1346
5.531757246	1308
5.548468515	1233
5.565179784	1312
5.581891053	1254
5.598602322	1286
5.615313591	1262
5.63202486	1276
5.648736129	1285
5.665447398	1238
5.682158667	1242
5.698869936	1239
5.715581205	1231
5.732292474	1282
5.749003743	1250
5.765715012	1262
5.782426281	1256
5.79913755	1224
5.815848819	1259
5.832560088	1222
5.849271356	1213
5.865982625	1221
5.882693894	1240
5.899405163	1266
5.916116432	1202
5.932827701	1218
5.94953897	1184
5.966250239	1233
5.982961508	1256
5.999672777	1182
6.016384046	1238
6.033095315	1193
6.049806584	1215
6.066517853	1233
6.083229122	1215
6.099940391	1215
6.11665166	1237
6.133362929	1148
6.150074198	1164
6.166785467	1223
6.183496736	1174
6.200208005	1168
6.216919274	1192
6.233630543	1149
6.250341812	1139
6.267053081	1185
6.28376435	1216
6.300475619	1151
6.317186888	1179
6.333898157	1171
6.350609426	1111
6.367320695	1167
6.384031964	1178
6.400743233	1118
6.417454502	1185
6.434165771	1087
6.45087704	1156
6.467588309	1174
6.484299578	1092
6.501010847	1154
6.517722116	1144
6.534433385	1125
6.551144654	1152
6.567855923	1127
6.584567192	1154
6.601278461	1157
6.61798973	1154
6.634700999	1164
6.651412268	1112
6.668123536	1152
6.684834805	1167
6.701546074	1179
6.718257343	1110
6.734968612	1171
6.751679881	1088
6.76839115	1060
6.785102419	1132
6.801813688	1103
6.818524957	1163
6.835236226	1066
6.851947495	1118
6.868658764	1116
6.885370033	1088
6.902081302	1070
6.918792571	1110
6.93550384	1117
6.952215109	1097
6.968926378	1097
6.985637647	1069
7.002348916	1121
7.019060185	1113
7.035771454	1015
7.052482723	1016
7.069193992	1094
7.085905261	1039
7.10261653	1035
7.119327799	1098
7.136039068	1040
7.152750337	1033
7.169461606	1016
7.186172875	1046
7.202884144	1010
7.219595413	1013
7.236306682	1056
7.253017951	1039
7.26972922	1073
7.286440489	1021
7.303151758	1017
7.319863027	1007
7.336574296	1055
7.353285565	1086
7.369996834	989
7.386708103	1040
7.403419372	1084
7.420130641	984
7.43684191	1026
7.453553179	1060
7.470264447	1060
7.486975716	1026
7.503686985	994
7.520398254	1032
7.537109523	1007
7.553820792	1049
7.570532061	1035
7.58724333	984
7.603954599	1061
7.620665868	1030
7.637377137	1011
7.654088406	1030
7.670799675	994
7.687510944	977
7.704222213	1020
7.720933482	966
7.737644751	1028
7.75435602	1036
7.771067289	1028
7.787778558	1084
7.804489827	1023
7.821201096	1043
7.837912365	1021
7.854623634	899
7.871334903	969
7.888046172	997
7.904757441	957
7.92146871	1014
7.938179979	983
7.954891248	1009
7.971602517	973
7.988313786	1012
8.005025055	1007
8.021736324	1035
8.038447593	996
8.055158862	1045
8.071870131	993
8.0885814	1026
8.105292669	1053
8.122003938	1013
8.138715207	1002
8.155426476	991
8.172137745	973
8.188849014	988
8.205560283	950
8.222271552	1042
8.238982821	952
8.25569409	1036
8.272405359	1030
8.289116627	969
8.305827896	978
8.322539165	1016
8.339250434	1077
8.355961703	1055
8.372672972	1065
8.389384241	1027
8.40609551	1012
8.422806779	1078
8.439518048	1061
8.456229317	1061
8.472940586	1032
8.489651855	1019
8.506363124	1074
8.523074393	1073
8.539785662	1126
8.556496931	1148
8.5732082	1121
8.589919469	1126
8.606630738	1170
8.623342007	1148
8.640053276	1186
8.656764545	1215
8.673475814	1259
8.690187083	1256
8.706898352	1338
8.723609621	1303
8.74032089	1413
8.757032159	1483
8.773743428	1511
8.790454697	1598
8.807165966	1549
8.823877235	1616
8.840588504	1697
8.857299773	1794
8.874011042	1891
8.890722311	1868
8.90743358	1948
8.924144849	1946
8.940856118	1971
8.957567387	2051
8.974278656	1939
8.990989925	1933
9.007701194	1918
9.024412463	1810
9.041123732	1762
9.057835001	1724
9.07454627	1719
9.091257538	1732
9.107968807	1696
9.124680076	1774
9.141391345	1831
9.158102614	1839
9.174813883	1982
9.191525152	1997
9.208236421	2050
9.22494769	2172
9.241658959	2255
9.258370228	2441
9.275081497	2589
9.291792766	2702
9.308504035	2950
9.325215304	3097
9.341926573	3297
9.358637842	3510
9.375349111	3713
9.39206038	4219
9.408771649	4443
9.425482918	4886
9.442194187	5242
9.458905456	5589
9.475616725	5997
9.492327994	6427
9.509039263	6881
9.525750532	7378
9.542461801	7754
9.55917307	8121
9.575884339	8607
9.592595608	8626
9.609306877	8587
9.626018146	8825
9.642729415	8504
9.659440684	8169
9.676151953	7830
9.692863222	7148
9.709574491	6581
9.72628576	5751
9.742997029	5108
9.759708298	4671
9.776419567	4037
9.793130836	3565
9.809842105	3057
9.826553374	2768
9.843264643	2448
9.859975912	2242
9.876687181	1922
9.89339845	1688
9.910109718	1718
9.926820987	1618
9.943532256	1496
9.960243525	1352
9.976954794	1224
9.993666063	1201
10.01037733	1200
10.0270886	1064
10.04379987	1080
10.06051114	1053
10.07722241	1078
10.09393368	998
10.11064495	1090
10.12735622	982
10.14406748	997
10.16077875	1019
10.17749002	1021
10.19420129	1003
10.21091256	997
10.22762383	988
10.2443351	911
10.26104637	958
10.27775764	945
10.29446891	954
10.31118017	925
10.32789144	921
10.34460271	836
10.36131398	859
10.37802525	948
10.39473652	942
10.41144779	894
10.42815906	927
10.44487033	865
10.4615816	893
10.47829286	912
10.49500413	898
10.5117154	913
10.52842667	908
10.54513794	931
10.56184921	969
10.57856048	945
10.59527175	955
10.61198302	989
10.62869429	997
10.64540555	1008
10.66211682	992
10.67882809	1070
10.69553936	1074
10.71225063	1045
10.7289619	1075
10.74567317	1193
10.76238444	1160
10.77909571	1237
10.79580697	1370
10.81251824	1506
10.82922951	1447
10.84594078	1630
10.86265205	1727
10.87936332	1779
10.89607459	1957
10.91278586	2161
10.92949713	2390
10.9462084	2505
10.96291966	2817
10.97963093	2908
10.9963422	2887
11.01305347	2869
11.02976474	2733
11.04647601	2455
11.06318728	2102
11.07989855	1707
11.09660982	1405
11.11332109	1186
11.13003235	1099
11.14674362	977
11.16345489	910
11.18016616	862
11.19687743	811
11.2135887	815
11.23029997	769
11.24701124	843
11.26372251	784
11.28043378	813
11.29714504	760
11.31385631	772
11.33056758	742
11.34727885	790
11.36399012	810
11.38070139	777
11.39741266	782
11.41412393	769
11.4308352	714
11.44754647	796
11.46425773	716
11.480969	693
11.49768027	692
11.51439154	750
11.53110281	695
11.54781408	687
11.56452535	686
11.58123662	678
11.59794789	679
11.61465915	701
11.63137042	762
11.64808169	715
11.66479296	759
11.68150423	696
11.6982155	683
11.71492677	733
11.73163804	674
11.74834931	724
11.76506058	692
11.78177184	681
11.79848311	699
11.81519438	721
11.83190565	722
11.84861692	693
11.86532819	693
11.88203946	722
11.89875073	727
11.915462	665
11.93217327	704
11.94888453	695
11.9655958	669
11.98230707	643
11.99901834	681
12.01572961	696
12.03244088	649
12.04915215	625
12.06586342	709
12.08257469	624
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12.11599722	663
12.13270849	656
12.14941976	658
12.16613103	663
12.1828423	687
12.19955357	632
12.21626484	645
12.23297611	639
12.24968738	679
12.26639865	630
12.28310991	649
12.29982118	663
12.31653245	661
12.33324372	637
12.34995499	623
12.36666626	616
12.38337753	642
12.4000888	626
12.41680007	689
12.43351133	628
12.4502226	619
12.46693387	623
12.48364514	623
12.50035641	680
12.51706768	657
12.53377895	647
12.55049022	708
12.56720149	630
12.58391276	626
12.60062402	651
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12.65075783	605
12.6674691	585
12.68418037	602
12.70089164	613
12.71760291	628
12.73431418	623
12.75102545	611
12.76773671	626
12.78444798	598
12.80115925	626
12.81787052	572
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12.85129306	627
12.86800433	659
12.8847156	616
12.90142687	620
12.91813814	607
12.9348494	635
12.95156067	621
12.96827194	628
12.98498321	637
13.00169448	621
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13.08525083	578
13.10196209	619
13.11867336	644
13.13538463	589
13.1520959	624
13.16880717	572
13.18551844	598
13.20222971	603
13.21894098	622
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13.33591986	563
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14.20490585	809
14.22161712	766
14.23832838	699
14.25503965	687
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14.30517346	601
14.32188473	573
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14.42215234	545
14.43886361	565
14.45557488	583
14.47228615	599
14.48899742	573
14.50570869	574
14.52241996	617
14.53913123	619
14.5558425	640
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14.65611011	607
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14.75637772	701
14.77308899	759
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14.8232228	846
14.83993407	912
14.85664534	989
14.87335661	988
14.89006787	1175
14.90677914	1259
14.92349041	1360
14.94020168	1409
14.95691295	1528
14.97362422	1705
14.99033549	1948
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15.02375803	2529
15.0404693	2841
15.05718056	3162
15.07389183	3644
15.0906031	3937
15.10731437	4155
15.12402564	4238
15.14073691	4107
15.15744818	3726
15.17415945	3167
15.19087072	2645
15.20758199	2069
15.22429325	1784
15.24100452	1429
15.25771579	1261
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15.29113833	945
15.3078496	913
15.32456087	858
15.34127214	767
15.35798341	754
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15.39140594	639
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15.42482848	639
15.44153975	611
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15.54180737	631
15.55851863	585
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15.72563132	615
15.74234259	694
15.75905386	662
15.77576513	688
15.7924764	747
15.80918767	731
15.82589894	770
15.84261021	803
15.85932148	812
15.87603274	924
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16.02643417	1800
16.04314543	2039
16.0598567	2208
16.07656797	2025
16.09327924	2123
16.10999051	1923
16.12670178	1732
16.14341305	1528
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