ZK-5
from Verified Synthesis, 4th Edition, 2025, page 205
Diffractometer: XRDynamic500
Wavelength: CuK(alpha 1,2): 1.5406 Å
Data collected by M. Fahda
-----
3	2194.85238
3.02	2242.50786
3.04	2180.74074
3.06	2177.4634
3.08	2035.19356
3.1	2108.11496
3.12	1942.0527
3.14	2070.18043
3.16	2081.21303
3.18	1956.59538
3.2	2041.85155
3.22	1961.53369
3.24	1964.70229
3.26	1988.6173
3.28	2007.14944
3.3	1971.48023
3.32	1890.86019
3.34	1998.56018
3.36	2006.6887
3.38	2022.031
3.4	1975.55823
3.42	1894.42076
3.44	1989.98338
3.46	2026.58181
3.48	1939.96598
3.5	1925.40968
3.52	1854.9965
3.54	1873.22569
3.56	1714.21167
3.58	1769.06946
3.6	1768.27024
3.62	1865.02058
3.64	1840.80415
3.66	1890.76258
3.68	1851.64056
3.7	1795.76889
3.72	1764.47119
3.74	1742.5898
3.76	1795.10498
3.78	1789.3764
3.8	1745.97281
3.82	1752.45998
3.84	1636.00649
3.86	1790.13338
3.88	1781.32502
3.9	1714.3386
3.92	1672.75334
3.94	1670.65472
3.96	1631.73618
3.98	1568.91361
4	1568.20626
4.02	1607.49967
4.04	1620.52786
4.06	1661.77508
4.08	1630.52459
4.1	1651.74917
4.12	1486.50297
4.14	1517.80213
4.16	1532.92138
4.18	1625.52097
4.2	1684.32795
4.22	1539.79202
4.24	1528.47074
4.26	1616.87473
4.28	1531.81023
4.3	1506.71152
4.32	1555.74324
4.34	1521.428
4.36	1476.94282
4.38	1596.32061
4.4	1481.15226
4.42	1521.428
4.44	1498.01694
4.46	1457.60376
4.48	1385.57082
4.5	1477.74634
4.52	1384.80077
4.54	1373.78646
4.56	1392.11274
4.58	1452.83906
4.6	1472.81432
4.62	1524.17364
4.64	1386.60861
4.66	1460.08514
4.68	1438.09948
4.7	1387.23589
4.72	1435.32688
4.74	1353.54047
4.76	1440.69709
4.78	1344.42051
4.8	1326.36744
4.82	1371.2682
4.84	1337.4947
4.86	1330.26826
4.88	1300.75815
4.9	1424.77032
4.92	1272.26352
4.94	1414.25495
4.96	1351.9541
4.98	1491.82715
5	1360.79806
5.02	1405.95845
5.04	1383.54954
5.06	1407.14614
5.08	1246.8416
5.1	1307.62121
5.12	1312.51477
5.14	1352.53862
5.16	1251.52419
5.18	1259.77541
5.2	1345.31544
5.22	1296.85192
5.24	1299.67304
5.26	1226.26589
5.28	1288.17222
5.3	1267.29157
5.32	1284.91846
5.34	1337.18632
5.36	1180.45515
5.38	1236.55839
5.4	1265.57476
5.42	1260.73563
5.44	1288.98558
5.46	1211.79667
5.48	1152.34
5.5	1221.29342
5.52	1191.82308
5.54	1259.49072
5.56	1232.79949
5.58	1206.5419
5.6	1332.97512
5.62	1224.6039
5.64	1188.55304
5.66	1160.36702
5.68	1128.38749
5.7	1106.14426
5.72	1185.20307
5.74	1205.82522
5.76	1143.32325
5.78	953.24319
5.8	1091.60466
5.82	1105.89429
5.84	1032.03983
5.86	1114.21838
5.88	1034.88892
5.9	1140.22433
5.92	1086.9997
5.94	1131.72076
5.96	1009.19262
5.98	1080.59605
6	1081.32916
6.02	991.6183
6.04	1062.17255
6.06	1067.22339
6.08	1047.50951
6.1	1045.79006
6.12	1027.90892
6.14	1014.59901
6.16	1096.18896
6.18	1058.91185
6.2	1019.35196
6.22	973.15003
6.24	1016.59944
6.26	965.16509
6.28	957.3624
6.3	1083.32409
6.32	1023.65319
6.34	1072.02555
6.36	924.35703
6.38	999.73174
6.4	998.6049
6.42	1049.54911
6.44	1082.98637
6.46	1074.33914
6.48	991.6183
6.5	1084.88207
6.52	1050.82667
6.54	1045.55388
6.56	1122.18924
6.58	1196.97014
6.6	1268.69929
6.62	1258.53694
6.64	1409.79171
6.66	1550.42042
6.68	1432.69309
6.7	1279.65709
6.72	1124.72698
6.74	1004.70135
6.76	1009.19262
6.78	979.3667
6.8	975.30451
6.82	962.27011
6.84	887.04479
6.86	987.99164
6.88	976.18814
6.9	890.05799
6.92	898.08735
6.94	919.91545
6.96	925.05801
6.98	894.6882
7	911.92523
7.02	929.98316
7.04	921.0204
7.06	932.29917
7.08	925.19261
7.1	901.52425
7.12	859.42216
7.14	846.93923
7.16	845.97985
7.18	831.41562
7.2	860.39151
7.22	918.02469
7.24	856.78441
7.26	816.25583
7.28	821.95638
7.3	876.5771
7.32	839.59423
7.34	916.62913
7.36	786.05231
7.38	934.76723
7.4	807.02377
7.42	834.73251
7.44	842.83172
7.46	914.86331
7.48	877.99048
7.5	976.00964
7.52	811.90099
7.54	885.84392
7.56	837.40576
7.58	751.99653
7.6	790.53912
7.62	855.55923
7.64	814.96458
7.66	808.62982
7.68	860.91823
7.7	866.54019
7.72	814.92995
7.74	841.4037
7.76	900.4804
7.78	757.21537
7.8	813.49386
7.82	759.97754
7.84	780.14632
7.86	761.87403
7.88	768.57334
7.9	788.39383
7.92	793.81856
7.94	775.03506
7.96	757.65371
7.98	757.31119
8	820.80453
8.02	782.47699
8.04	787.806
8.06	769.09393
8.08	834.73251
8.1	758.77559
8.12	824.61525
8.14	788.95317
8.16	805.5654
8.18	740.40847
8.2	798.3406
8.22	788.03742
8.24	789.86685
8.26	804.86192
8.28	792.5798
8.3	809.74945
8.32	747.88382
8.34	718.68499
8.36	840.92959
8.38	781.86812
8.4	734.93763
8.42	721.99091
8.44	783.00664
8.46	659.56114
8.48	772.35593
8.5	723.315
8.52	758.33968
8.54	727.40463
8.56	743.35587
8.58	762.4727
8.6	738.56915
8.62	809.70369
8.64	735.7884
8.66	726.42076
8.68	714.96207
8.7	704.73656
8.72	776.14023
8.74	715.22634
8.76	719.04974
8.78	721.16268
8.8	742.94002
8.82	805.04443
8.84	671.90657
8.86	716.57598
8.88	732.15969
8.9	732.49008
8.92	739.10017
8.94	656.86346
8.96	708.67089
8.98	690.99434
9	674.77973
9.02	694.20822
9.04	764.11523
9.06	699.92421
9.08	665.43087
9.1	727.2425
9.12	695.46613
9.14	707.5511
9.16	823.4414
9.18	789.10763
9.2	747.14217
9.22	771.94508
9.24	831.79166
9.26	842.26017
9.28	863.50816
9.3	857.68894
9.32	953.45846
9.34	992.48812
9.36	1178.76543
9.38	1286.59597
9.4	1559.05781
9.42	2146.51756
9.44	2170.53729
9.46	1661.54029
9.48	1054.20552
9.5	918.37963
9.52	771.70753
9.54	720.98497
9.56	703.24739
9.58	764.36811
9.6	724.27984
9.62	664.82785
9.64	737.26286
9.66	688.31785
9.68	722.97011
9.7	713.57723
9.72	709.99715
9.74	706.06488
9.76	627.70701
9.78	760.83841
9.8	677.78448
9.82	686.8216
9.84	651.74392
9.86	668.89855
9.88	625.93509
9.9	669.79777
9.92	675.82429
9.94	635.9262
9.96	628.84185
9.98	728.88665
10	644.52238
10.02	588.4226
10.04	711.2828
10.06	641.20116
10.08	665.43333
10.1	651.44975
10.12	687.28766
10.14	633.97636
10.16	633.31462
10.18	695.23013
10.2	649.79182
10.22	683.51575
10.24	654.4035
10.26	700.96411
10.28	654.14009
10.3	632.88496
10.32	686.66639
10.34	672.37859
10.36	620.08703
10.38	557.48629
10.4	648.71903
10.42	693.184
10.44	623.4208
10.46	626.75156
10.48	634.49265
10.5	566.49241
10.52	694.20822
10.54	599.65855
10.56	563.93949
10.58	567.14694
10.6	627.74415
10.62	620.36755
10.64	606.90735
10.66	604.39453
10.68	655.02826
10.7	622.0355
10.72	559.03818
10.74	626.85857
10.76	615.49725
10.78	590.76099
10.8	635.35201
10.82	630.17728
10.84	597.44748
10.86	646.91202
10.88	573.21295
10.9	628.94326
10.92	641.05635
10.94	620.08703
10.96	597.53086
10.98	606.19869
11	615.2195
11.02	616.74535
11.04	589.01089
11.06	618.13944
11.08	679.55605
11.1	595.10516
11.12	629.9808
11.14	624.54993
11.16	648.91293
11.18	628.69977
11.2	653.66255
11.22	626.92796
11.24	611.61118
11.26	561.34794
11.28	661.66721
11.3	576.45516
11.32	605.35063
11.34	640.76694
11.36	601.7366
11.38	615.7773
11.4	610.75899
11.42	600.51521
11.44	643.58887
11.46	616.19601
11.48	681.44029
11.5	590.22757
11.52	712.48353
11.54	671.46544
11.56	738.45975
11.58	624.40856
11.6	691.61854
11.62	588.95438
11.64	596.26026
11.66	582.15737
11.68	597.85235
11.7	578.37609
11.72	623.58671
11.74	578.13684
11.76	578.50685
11.78	616.75025
11.8	576.82943
11.82	578.79277
11.84	539.22216
11.86	608.41469
11.88	595.8551
11.9	595.18105
11.92	597.53086
11.94	647.05825
11.96	568.69622
11.98	668.90551
12	588.07786
12.02	511.38576
12.04	510.92391
12.06	609.51564
12.08	538.73451
12.1	576.95991
12.12	611.74921
12.14	585.87065
12.16	579.42387
12.18	619.66673
12.2	627.74415
12.22	599.52312
12.24	512.42798
12.26	520.65617
12.28	537.2911
12.3	594.10575
12.32	536.92667
12.34	522.464
12.36	550.45267
12.38	595.04643
12.4	528.97775
12.42	522.93693
12.44	535.23985
12.46	529.44363
12.48	527.76818
12.5	589.62047
12.52	566.62066
12.54	552.13834
12.56	534.39391
12.58	548.51776
12.6	562.23635
12.62	544.77385
12.64	537.53433
12.66	626.21844
12.68	599.92958
12.7	592.03255
12.72	564.02163
12.74	590.09437
12.76	580.83998
12.78	553.62814
12.8	579.42387
12.82	556.05853
12.84	561.72834
12.86	600.7862
12.88	550.89114
12.9	488.11516
12.92	576.17794
12.94	525.01137
12.96	558.6602
12.98	499.30082
13	531.02984
13.02	528.12631
13.04	493.11671
13.06	619.80677
13.08	519.59888
13.1	476.94465
13.12	536.67178
13.14	583.1393
13.16	533.19045
13.18	563.91668
13.2	507.08415
13.22	621.8749
13.24	557.69547
13.26	594.70279
13.28	591.42912
13.3	683.00715
13.32	775.38544
13.34	797.43505
13.36	872.78912
13.38	895.86036
13.4	783.71396
13.42	666.33745
13.44	603.13471
13.46	563.40727
13.48	535.83634
13.5	591.83073
13.52	535.47388
13.54	513.24155
13.56	568.56785
13.58	542.56331
13.6	485.26749
13.62	564.81037
13.64	538.00468
13.66	525.12985
13.68	545.39109
13.7	534.39391
13.72	570.37037
13.74	525.48563
13.76	508.11621
13.78	538.36934
13.8	527.15233
13.82	545.96584
13.84	513.95446
13.86	557.56921
13.88	503.83085
13.9	551.14013
13.92	508.34613
13.94	500.6568
13.96	551.26471
13.98	492.73345
14	572.31067
14.02	489.03845
14.04	549.45728
14.06	499.75309
14.08	497.82965
14.1	548.46548
14.12	542.59552
14.14	549.01495
14.16	559.92214
14.18	523.32528
14.2	516.107
14.22	505.85039
14.24	504.28805
14.26	532.4683
14.28	519.13035
14.3	511.03929
14.32	530.53498
14.34	543.54356
14.36	519.01335
14.38	485.9777
14.4	546.95513
14.42	578.87502
14.44	523.32528
14.46	485.21031
14.48	545.47254
14.5	499.63994
14.52	540.78687
14.54	470.88445
14.56	535.36092
14.58	617.16904
14.6	509.46361
14.62	542.44103
14.64	608.55209
14.66	574.12178
14.68	539.93197
14.7	523.79813
14.72	630.74539
14.74	558.62068
14.76	538.50945
14.78	681.24534
14.8	688.72398
14.82	701.43956
14.84	741.75192
14.86	833.89951
14.88	992.05223
14.9	1228.2163
14.92	1391.64281
14.94	1623.04096
14.96	1558.79663
14.98	1279.7289
15	1137.3769
15.02	772.46902
15.04	709.51624
15.06	707.12138
15.08	636.78945
15.1	570.37037
15.12	680.32287
15.14	640.98032
15.16	572.56554
15.18	544.77385
15.2	507.8865
15.22	543.75296
15.24	502.22823
15.26	564.04418
15.28	545.59578
15.3	524.03487
15.32	533.66891
15.34	529.5756
15.36	501.56379
15.38	532.10796
15.4	521.67701
15.42	467.06739
15.44	542.38175
15.46	523.79813
15.48	533.67094
15.5	511.11367
15.52	558.70762
15.54	558.99983
15.56	530.78314
15.58	519.99511
15.6	539.58848
15.62	528.36534
15.64	560.68204
15.66	537.03464
15.68	504.82386
15.7	540.20012
15.72	566.74897
15.74	507.31314
15.76	465.91154
15.78	542.01287
15.8	587.54602
15.82	628.45507
15.84	653.43672
15.86	562.74527
15.88	590.42177
15.9	588.07786
15.92	680.47644
15.94	664.83601
15.96	651.36867
15.98	532.22516
16	586.88258
16.02	600.10918
16.04	536.08848
16.06	544.77385
16.08	582.78133
16.1	514.41853
16.12	501.10988
16.14	564.29935
16.16	529.20363
16.18	501.67044
16.2	484.06172
16.22	525.45985
16.24	520.49584
16.26	481.10137
16.28	525.01137
16.3	506.8811
16.32	513.19277
16.34	592.50128
16.36	656.86346
16.38	689.25222
16.4	708.19055
16.42	648.52417
16.44	589.2964
16.46	480.55787
16.48	476.64574
16.5	496.46896
16.52	450.53242
16.54	512.15111
16.56	514.00589
16.58	464.08868
16.6	448.4442
16.62	521.28542
16.64	487.89454
16.66	501.89698
16.68	503.14661
16.7	396.20065
16.72	476.62159
16.74	447.3441
16.76	502.69148
16.78	411.44195
16.8	504.71006
16.82	457.48541
16.84	455.16251
16.86	494.43295
16.88	490.40032
16.9	516.57333
16.92	458.77491
16.94	492.17593
16.96	406.3951
16.98	448.14017
17	459.29366
17.02	508.00133
17.04	446.63596
17.06	476.72923
17.08	419.51231
17.1	441.41087
17.12	463.2244
17.14	392.95283
17.16	414.36871
17.18	455.67717
17.2	446.63596
17.22	468.76501
17.24	485.15763
17.26	435.196
17.28	444.22497
17.3	424.07393
17.32	516.107
17.34	451.65213
17.36	430.07
17.38	411.44195
17.4	469.9322
17.42	494.56378
17.44	451.55011
17.46	446.03076
17.48	410.51548
17.5	504.04378
17.52	427.58658
17.54	431.29221
17.56	473.74656
17.58	443.9242
17.6	500.54366
17.62	497.72432
17.64	463.56524
17.66	551.70036
17.68	592.16622
17.7	545.22622
17.72	552.94714
17.74	602.047
17.76	519.36451
17.78	472.05811
17.8	442.51911
17.82	514.0704
17.84	440.61338
17.86	425.03316
17.88	431.58442
17.9	417.2323
17.92	479.79904
17.94	510.80857
17.96	515.81577
17.98	432.26777
18	459.7503
18.02	419.0385
18.04	392.92181
18.06	432.26777
18.08	478.42698
18.1	433.68403
18.12	464.50829
18.14	532.46626
18.16	423.1288
18.18	444.12467
18.2	485.53889
18.22	499.52685
18.24	443.52096
18.26	446.43404
18.28	509.11852
18.3	443.42057
18.32	539.71069
18.34	502.23717
18.36	528.48493
18.38	521.75621
18.4	498.61986
18.42	548.39361
18.44	544.15801
18.46	480.88382
18.48	546.83128
18.5	406.94664
18.52	495.34649
18.54	463.01485
18.56	426.6488
18.58	409.4963
18.6	451.7542
18.62	452.36758
18.64	479.58267
18.66	418.55595
18.68	491.28652
18.7	410.4711
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