##TITLE=              31P MAS NMR spectrum of as-made IST-1 (with methylamine template)
##JCAMP-DX=           5.01
##DATA TYPE=          NMR SPECTRUM
##DATA CLASS=         XYDATA
##ORIGIN=             Jorda et al. Microporous Mesoporous Mater., 65, 43-57 (2003) Figure 1b
##OWNER=              Digitized and processed by Brouwer Lab, Redeemer University
##LONG DATE=          2020/07/22 09:27:03
##SOURCE REFERENCE=   PON-31P-Jorda-2003-asmade
##DATA PROCESSING=    Spectrum digitized with WebPlotDigitizer and deconvoluted with Mathematica notebook

$$Sample information 
##NAMES=              PON
##NAMES=              IST-1
##SAMPLE DESCRIPTION= IST-1, as-made

$$Bibliographic information 
##$AUTHORS=           Jorda, J.L., McCusker, L.B., Baerlocher, C., Morais, C.M., Rocha, J., Fernandez, C., Borges, C., LourenA~\[Section]o, J.P., Ribeiro, M.F., Gabelica, Z.
##$TITLE=             Structure analysis of the novel microporous aluminophosphate IST-1 using synchrotron powder diffraction data and HETCOR MAS NMR
##$JOURNAL=           Microporous and Mesoporous Materials
##$VOLUME=            65
##$PAGES=             43-57
##$YEAR=              2003
##$DOI=               10.1016/S1387-1811(03)00499-2
##$FIGURE=            Figure 1b

$$Peak information    (Positions in ppm, Relative peak areas, Peak widths in ppm, Lorentzian/Gaussian shape parameter)
##$NUM PEAKS=         3
##$PEAK LABELS=        P3         P2         P1        
##$PEAK TSITES=        T6         T5         T4        
##$PEAK POSITIONS=    -27.8541   -18.2328   -16.4494   
##$PEAK AREAS=         1.         1.         1.        
##$PEAK WIDTHS=        1.46027    1.09122    1.59729   
##$PEAK SHAPES=        0.28669    0.28669    0.28669   
##$NUMBERING REF=     Jorda et al. Microporous Mesoporous Mater., 65, 43-57 (2003)
##$ASSIGN REF=        Jorda et al. Microporous Mesoporous Mater., 65, 43-57 (2003) Figure 3
##$ASSIGN METHOD=     2D correlation NMR
##$COMMENT=           Peak assignments based on a 2D 27Al/31P correlation spectrum

$$Spectrum acquisition information 
##.OBSERVE NUCLEUS=   ^31P
##.OBSERVE FREQUENCY= 161.9
##.PULSE SEQUENCE=    single pulse
##.MAS FREQUENCY=     10000

$$Spectrum data information 
##XUNITS=             PPM
##YUNITS=             ARBITRARY UNITS
##FIRSTX=              0.00000              
##LASTX=              -44.7                 
##XFACTOR=            1
##YFACTOR=            1
##NPOINTS=            448
##FIRSTY=             -0.00005              

$$Spectrum data
##XYDATA=             (X++(Y..Y))
  0.00000            -0.00005              
 -0.1                -0.00005              
 -0.2                -0.00005              
 -0.3                -0.00005              
 -0.4                -0.00005              
 -0.5                -0.00005              
 -0.6                -0.00005              
 -0.7                -0.00005              
 -0.8                -0.00005              
 -0.9                -0.00005              
 -1.                 -0.00005              
 -1.1                -0.00005              
 -1.2                -0.00005              
 -1.3                -0.00005              
 -1.4                -0.00005              
 -1.5                -0.00005              
 -1.6                -0.00005              
 -1.7                -0.00005              
 -1.8                -0.00005              
 -1.9                -0.00005              
 -2.                 -0.00005              
 -2.1                -0.00005              
 -2.2                -0.00005              
 -2.3                -0.00005              
 -2.4                -0.00005              
 -2.5                -0.00005              
 -2.6                -0.00005              
 -2.7                -0.00005              
 -2.8                -0.00005              
 -2.9                -0.00005              
 -3.                 -0.00005              
 -3.1                -0.00005              
 -3.2                -0.00005              
 -3.3                -0.00005              
 -3.4                -0.00005              
 -3.5                -0.00005              
 -3.6                -0.00005              
 -3.7                -0.00005              
 -3.8                -0.00005              
 -3.9                -0.00005              
 -4.                 -0.00005              
 -4.1                -0.00005              
 -4.2                -0.00005              
 -4.3                -0.00005              
 -4.4                -0.00005              
 -4.5                -0.00005              
 -4.6                -0.00005              
 -4.7                -0.00005              
 -4.8                -0.00005              
 -4.9                -0.00005              
 -5.                 -0.00005              
 -5.1                -0.00005              
 -5.2                -0.00005              
 -5.3                -0.00005              
 -5.4                -0.00005              
 -5.5                -0.00005              
 -5.6                -0.00005              
 -5.7                -0.00005              
 -5.8                -0.00005              
 -5.9                -0.00005              
 -6.                 -0.00005              
 -6.1                -0.00005              
 -6.2                -0.00005              
 -6.3                -0.00005              
 -6.4                -0.00005              
 -6.5                -0.00005              
 -6.6                -0.00005              
 -6.7                -0.00005              
 -6.8                -0.00005              
 -6.9                -0.00005              
 -7.                 -0.00005              
 -7.1                -0.00005              
 -7.2                -0.00005              
 -7.3                -0.00005              
 -7.4                -0.00005              
 -7.5                -0.00005              
 -7.6                -0.00005              
 -7.7                -0.00005              
 -7.8                -0.00005              
 -7.9                -0.00005              
 -8.                 -0.00005              
 -8.1                -0.00005              
 -8.2                -0.00005              
 -8.3                -0.00005              
 -8.4                -0.00005              
 -8.5                 0.00001              
 -8.6                 0.00108              
 -8.7                 0.00290              
 -8.8                 0.00424              
 -8.9                 0.00347              
 -9.                  0.00188              
 -9.1                 0.00331              
 -9.2                 0.00621              
 -9.3                 0.00780              
 -9.4                 0.00790              
 -9.5                 0.00788              
 -9.6                 0.00789              
 -9.7                 0.00789              
 -9.8                 0.00789              
 -9.9                 0.00789              
 -10.                 0.00789              
 -10.1                0.00789              
 -10.2                0.00789              
 -10.3                0.00789              
 -10.4                0.00789              
 -10.5                0.00789              
 -10.6                0.00789              
 -10.7                0.00789              
 -10.8                0.00789              
 -10.9                0.00789              
 -11.                 0.00789              
 -11.1                0.00789              
 -11.2                0.00789              
 -11.3                0.00789              
 -11.4                0.00789              
 -11.5                0.00789              
 -11.6                0.00789              
 -11.7                0.00788              
 -11.8                0.00791              
 -11.9                0.00782              
 -12.                 0.00844              
 -12.1                0.00975              
 -12.2                0.01040              
 -12.3                0.01106              
 -12.4                0.01320              
 -12.5                0.01258              
 -12.6                0.01138              
 -12.7                0.01205              
 -12.8                0.01177              
 -12.9                0.01118              
 -13.                 0.01351              
 -13.1                0.01469              
 -13.2                0.01447              
 -13.3                0.01452              
 -13.4                0.01452              
 -13.5                0.01445              
 -13.6                0.01490              
 -13.7                0.01639              
 -13.8                0.01895              
 -13.9                0.02068              
 -14.                 0.02169              
 -14.1                0.02357              
 -14.2                0.02771              
 -14.3                0.03086              
 -14.4                0.03312              
 -14.5                0.03829              
 -14.6                0.04538              
 -14.7                0.05182              
 -14.8                0.06261              
 -14.9                0.07234              
 -15.                 0.08509              
 -15.1                0.10082              
 -15.2                0.11319              
 -15.3                0.14026              
 -15.4                0.17247              
 -15.5                0.20979              
 -15.6                0.25807              
 -15.7                0.29974              
 -15.8                0.33415              
 -15.9                0.39417              
 -16.                 0.43486              
 -16.1                0.47459              
 -16.2                0.51403              
 -16.3                0.53765              
 -16.4                0.55565              
 -16.5                0.55972              
 -16.6                0.55436              
 -16.7                0.52490              
 -16.8                0.48810              
 -16.9                0.45100              
 -17.                 0.41020              
 -17.1                0.38495              
 -17.2                0.36991              
 -17.3                0.37702              
 -17.4                0.39453              
 -17.5                0.42377              
 -17.6                0.47595              
 -17.7                0.53020              
 -17.8                0.59585              
 -17.9                0.67203              
 -18.                 0.72355              
 -18.1                0.76274              
 -18.2                0.79158              
 -18.3                0.78896              
 -18.4                0.76037              
 -18.5                0.70799              
 -18.6                0.63510              
 -18.7                0.51511              
 -18.8                0.38274              
 -18.9                0.27961              
 -19.                 0.19492              
 -19.1                0.12915              
 -19.2                0.08893              
 -19.3                0.07296              
 -19.4                0.05851              
 -19.5                0.04223              
 -19.6                0.03352              
 -19.7                0.02854              
 -19.8                0.02373              
 -19.9                0.02145              
 -20.                 0.02030              
 -20.1                0.01885              
 -20.2                0.01682              
 -20.3                0.01491              
 -20.4                0.01444              
 -20.5                0.01432              
 -20.6                0.01313              
 -20.7                0.01099              
 -20.8                0.00924              
 -20.9                0.00815              
 -21.                 0.00781              
 -21.1                0.00791              
 -21.2                0.00788              
 -21.3                0.00789              
 -21.4                0.00789              
 -21.5                0.00789              
 -21.6                0.00789              
 -21.7                0.00789              
 -21.8                0.00789              
 -21.9                0.00789              
 -22.                 0.00789              
 -22.1                0.00789              
 -22.2                0.00789              
 -22.3                0.00789              
 -22.4                0.00789              
 -22.5                0.00789              
 -22.6                0.00789              
 -22.7                0.00789              
 -22.8                0.00789              
 -22.9                0.00789              
 -23.                 0.00789              
 -23.1                0.00789              
 -23.2                0.00789              
 -23.3                0.00789              
 -23.4                0.00789              
 -23.5                0.00789              
 -23.6                0.00789              
 -23.7                0.00789              
 -23.8                0.00789              
 -23.9                0.00789              
 -24.                 0.00789              
 -24.1                0.00789              
 -24.2                0.00789              
 -24.3                0.00789              
 -24.4                0.00789              
 -24.5                0.00789              
 -24.6                0.00788              
 -24.7                0.00791              
 -24.8                0.00781              
 -24.9                0.00849              
 -25.                 0.00994              
 -25.1                0.01192              
 -25.2                0.01392              
 -25.3                0.01461              
 -25.4                0.01449              
 -25.5                0.01449              
 -25.6                0.01484              
 -25.7                0.01622              
 -25.8                0.01855              
 -25.9                0.02105              
 -26.                 0.02378              
 -26.1                0.02758              
 -26.2                0.03351              
 -26.3                0.04126              
 -26.4                0.05230              
 -26.5                0.06717              
 -26.6                0.08716              
 -26.7                0.10314              
 -26.8                0.12887              
 -26.9                0.16857              
 -27.                 0.22275              
 -27.1                0.27989              
 -27.2                0.34202              
 -27.3                0.39302              
 -27.4                0.43180              
 -27.5                0.47651              
 -27.6                0.52232              
 -27.7                0.56383              
 -27.8                0.58099              
 -27.9                0.58069              
 -28.                 0.56881              
 -28.1                0.53745              
 -28.2                0.48626              
 -28.3                0.43245              
 -28.4                0.38300              
 -28.5                0.33388              
 -28.6                0.27286              
 -28.7                0.21882              
 -28.8                0.17839              
 -28.9                0.15070              
 -29.                 0.12074              
 -29.1                0.08984              
 -29.2                0.07213              
 -29.3                0.05617              
 -29.4                0.04495              
 -29.5                0.03834              
 -29.6                0.03332              
 -29.7                0.02944              
 -29.8                0.02605              
 -29.9                0.02200              
 -30.                 0.01791              
 -30.1                0.01506              
 -30.2                0.01446              
 -30.3                0.01404              
 -30.4                0.01173              
 -30.5                0.00904              
 -30.6                0.00788              
 -30.7                0.00789              
 -30.8                0.00789              
 -30.9                0.00789              
 -31.                 0.00789              
 -31.1                0.00789              
 -31.2                0.00789              
 -31.3                0.00789              
 -31.4                0.00789              
 -31.5                0.00788              
 -31.6                0.00790              
 -31.7                0.00786              
 -31.8                0.00791              
 -31.9                0.00560              
 -32.                 0.00312              
 -32.1                0.00271              
 -32.2                0.00213              
 -32.3                0.00206              
 -32.4                0.00353              
 -32.5                0.00354              
 -32.6                0.00227              
 -32.7                0.00099              
 -32.8                0.00009              
 -32.9               -0.00009              
 -33.                -0.00004              
 -33.1               -0.00006              
 -33.2               -0.00005              
 -33.3               -0.00005              
 -33.4               -0.00005              
 -33.5               -0.00005              
 -33.6               -0.00005              
 -33.7               -0.00005              
 -33.8               -0.00005              
 -33.9               -0.00005              
 -34.                -0.00005              
 -34.1               -0.00005              
 -34.2               -0.00005              
 -34.3               -0.00005              
 -34.4               -0.00005              
 -34.5               -0.00005              
 -34.6               -0.00005              
 -34.7               -0.00005              
 -34.8               -0.00005              
 -34.9               -0.00005              
 -35.                -0.00005              
 -35.1               -0.00005              
 -35.2               -0.00005              
 -35.3               -0.00005              
 -35.4               -0.00005              
 -35.5               -0.00005              
 -35.6               -0.00005              
 -35.7               -0.00005              
 -35.8               -0.00005              
 -35.9               -0.00005              
 -36.                -0.00005              
 -36.1               -0.00005              
 -36.2               -0.00005              
 -36.3               -0.00005              
 -36.4               -0.00005              
 -36.5               -0.00005              
 -36.6               -0.00005              
 -36.7               -0.00005              
 -36.8               -0.00005              
 -36.9               -0.00005              
 -37.                -0.00005              
 -37.1               -0.00005              
 -37.2               -0.00005              
 -37.3               -0.00005              
 -37.4               -0.00005              
 -37.5               -0.00005              
 -37.6               -0.00005              
 -37.7               -0.00005              
 -37.8               -0.00005              
 -37.9               -0.00005              
 -38.                -0.00005              
 -38.1               -0.00005              
 -38.2               -0.00005              
 -38.3               -0.00005              
 -38.4               -0.00005              
 -38.5               -0.00005              
 -38.6               -0.00005              
 -38.7               -0.00005              
 -38.8               -0.00005              
 -38.9               -0.00005              
 -39.                -0.00005              
 -39.1               -0.00005              
 -39.2               -0.00005              
 -39.3               -0.00005              
 -39.4               -0.00005              
 -39.5               -0.00005              
 -39.6               -0.00005              
 -39.7               -0.00005              
 -39.8               -0.00005              
 -39.9               -0.00005              
 -40.                -0.00005              
 -40.1               -0.00005              
 -40.2               -0.00005              
 -40.3               -0.00005              
 -40.4               -0.00005              
 -40.5               -0.00005              
 -40.6               -0.00005              
 -40.7               -0.00005              
 -40.8               -0.00005              
 -40.9               -0.00005              
 -41.                -0.00005              
 -41.1               -0.00005              
 -41.2               -0.00005              
 -41.3               -0.00005              
 -41.4               -0.00005              
 -41.5               -0.00005              
 -41.6               -0.00005              
 -41.7               -0.00005              
 -41.8               -0.00005              
 -41.9               -0.00005              
 -42.                -0.00005              
 -42.1               -0.00005              
 -42.2               -0.00005              
 -42.3               -0.00005              
 -42.4               -0.00005              
 -42.5               -0.00005              
 -42.6               -0.00005              
 -42.7               -0.00005              
 -42.8               -0.00005              
 -42.9               -0.00005              
 -43.                -0.00005              
 -43.1               -0.00005              
 -43.2               -0.00005              
 -43.3               -0.00005              
 -43.4               -0.00005              
 -43.5               -0.00005              
 -43.6               -0.00005              
 -43.7               -0.00005              
 -43.8               -0.00005              
 -43.9               -0.00005              
 -44.                -0.00005              
 -44.1               -0.00005              
 -44.2               -0.00005              
 -44.3               -0.00005              
 -44.4               -0.00005              
 -44.5               -0.00005              
 -44.6               -0.00005              
 -44.7               -0.00005              
##END=
