##TITLE=              29Si MAS NMR spectrum of Offretite
##JCAMP-DX=           5.01
##DATA TYPE=          NMR SPECTRUM
##DATA CLASS=         XYDATA
##ORIGIN=             Fyfe et al. Chem. Lett., 12, 1547-1550 (1983) Figure 1d
##OWNER=              Digitized and processed by Brouwer Lab, Redeemer University College
##LONG DATE=          2019/06/20 16:00:57
##SOURCE REFERENCE=   OFF-29Si-Fyfe-1983
##DATA PROCESSING=    Spectrum digitized with WebPlotDigitizer and deconvoluted with Mathematica notebook

$$Sample information 
##NAMES=              OFF
##NAMES=              Offretite
##SAMPLE DESCRIPTION= Offretite, dealuminated

$$Bibliographic information 
##$AUTHORS=           Fyfe, C.A., Gobbi, G.C., Murphy, W.J., Ozubko, R.S., Slack, D.A.
##$TITLE=             Investigation of the factors affecting the 29Si MAS NMR linewidths of zeolites
##$JOURNAL=           Chemistry Letters
##$VOLUME=            12
##$PAGES=             1547-1550
##$YEAR=              1983
##$DOI=               10.1246/cl.1983.1547
##$FIGURE=            Figure 1d

$$Peak information    (Positions in ppm, Relative peak areas, Peak widths in ppm, Lorentzian/Gaussian shape parameter)
##$NUM PEAKS=         2
##$PEAK TSITES=        T2         T1        
##$PEAK LABELS=        Si2        Si1       
##$PEAK POSITIONS=    -114.986   -109.69    
##$PEAK AREAS=         1.         2.        
##$PEAK WIDTHS=        1.2976     1.0895    
##$PEAK SHAPES=        1          1         
##$NUMBERING REF=     Gard and Tait, Acta Crystallogr., B28, 825-834 (1972)
##$ASSIGN REF=        Fyfe et al. Chem. Lett., 12, 1547-1550 (1983)
##$ASSIGN METHOD=     relative peak intensities

$$Spectrum acquisition information 
##.OBSERVE NUCLEUS=   ^29Si
##.OBSERVE FREQUENCY= 79.5
##.PULSE SEQUENCE=    single pulse
##.MAS FREQUENCY=     

$$Spectrum data information 
##XUNITS=             PPM
##YUNITS=             ARBITRARY UNITS
##FIRSTX=             -89.89                
##LASTX=              -124.81               
##XFACTOR=            1
##YFACTOR=            1
##NPOINTS=            1165
##FIRSTY=             -0.00728              

$$Spectrum data
##XYDATA=             (X++(Y..Y))
 -89.89              -0.00728              
 -89.92              -0.00679              
 -89.95              -0.00910              
 -89.98              -0.00966              
 -90.01              -0.00940              
 -90.04              -0.00939              
 -90.07              -0.00942              
 -90.1               -0.01064              
 -90.13              -0.01052              
 -90.16              -0.01200              
 -90.19              -0.01518              
 -90.22              -0.01504              
 -90.25              -0.01486              
 -90.28              -0.01498              
 -90.31              -0.01494              
 -90.34              -0.01494              
 -90.37              -0.01495              
 -90.4               -0.01494              
 -90.43              -0.01494              
 -90.46              -0.01494              
 -90.49              -0.01494              
 -90.52              -0.01495              
 -90.55              -0.01494              
 -90.58              -0.01496              
 -90.61              -0.01493              
 -90.64              -0.01406              
 -90.67              -0.01075              
 -90.7               -0.00918              
 -90.73              -0.00927              
 -90.76              -0.00683              
 -90.79              -0.00329              
 -90.82              -0.00224              
 -90.85              -0.00266              
 -90.88              -0.00255              
 -90.91              -0.00254              
 -90.94              -0.00269              
 -90.97              -0.00218              
 -91.                -0.00335              
 -91.03              -0.00672              
 -91.06              -0.00694              
 -91.09              -0.00630              
 -91.12              -0.00764              
 -91.15              -0.00962              
 -91.18              -0.00947              
 -91.21              -0.00998              
 -91.24              -0.01298              
 -91.27              -0.01530              
 -91.3               -0.01492              
 -91.33              -0.01497              
 -91.36              -0.01435              
 -91.39              -0.01250              
 -91.42              -0.01041              
 -91.45              -0.00945              
 -91.48              -0.00954              
 -91.51              -0.00873              
 -91.54              -0.00791              
 -91.57              -0.00809              
 -91.6               -0.00810              
 -91.63              -0.00791              
 -91.66              -0.00867              
 -91.69              -0.00955              
 -91.72              -0.00944              
 -91.75              -0.00956              
 -91.78              -0.00862              
 -91.81              -0.00802              
 -91.84              -0.00795              
 -91.87              -0.00678              
 -91.9               -0.00662              
 -91.93              -0.00664              
 -91.96              -0.00691              
 -91.99              -0.00814              
 -92.02              -0.00933              
 -92.05              -0.00938              
 -92.08              -0.00993              
 -92.11              -0.01092              
 -92.14              -0.01082              
 -92.17              -0.01093              
 -92.2               -0.01012              
 -92.23              -0.00927              
 -92.26              -0.00948              
 -92.29              -0.00954              
 -92.32              -0.00852              
 -92.35              -0.00791              
 -92.38              -0.00813              
 -92.41              -0.00807              
 -92.44              -0.00717              
 -92.47              -0.00514              
 -92.5               -0.00326              
 -92.53              -0.00251              
 -92.56              -0.00254              
 -92.59              -0.00265              
 -92.62              -0.00231              
 -92.65              -0.00313              
 -92.68              -0.00539              
 -92.71              -0.00638              
 -92.74              -0.00835              
 -92.77              -0.01005              
 -92.8               -0.01114              
 -92.83              -0.01339              
 -92.86              -0.01581              
 -92.89              -0.01652              
 -92.92              -0.01626              
 -92.95              -0.01633              
 -92.98              -0.01632              
 -93.01              -0.01632              
 -93.04              -0.01632              
 -93.07              -0.01632              
 -93.1               -0.01632              
 -93.13              -0.01632              
 -93.16              -0.01632              
 -93.19              -0.01632              
 -93.22              -0.01632              
 -93.25              -0.01632              
 -93.28              -0.01632              
 -93.31              -0.01632              
 -93.34              -0.01632              
 -93.37              -0.01632              
 -93.4               -0.01632              
 -93.43              -0.01632              
 -93.46              -0.01632              
 -93.49              -0.01632              
 -93.52              -0.01632              
 -93.55              -0.01632              
 -93.58              -0.01631              
 -93.61              -0.01634              
 -93.64              -0.01630              
 -93.67              -0.01622              
 -93.7               -0.01722              
 -93.73              -0.01783              
 -93.76              -0.01768              
 -93.79              -0.01770              
 -93.82              -0.01758              
 -93.85              -0.01841              
 -93.88              -0.01932              
 -93.91              -0.01893              
 -93.94              -0.01778              
 -93.97              -0.01775              
 -94.                -0.01712              
 -94.03              -0.01618              
 -94.06              -0.01632              
 -94.09              -0.01634              
 -94.12              -0.01631              
 -94.15              -0.01632              
 -94.18              -0.01632              
 -94.21              -0.01632              
 -94.24              -0.01628              
 -94.27              -0.01645              
 -94.3               -0.01600              
 -94.33              -0.01489              
 -94.36              -0.01400              
 -94.39              -0.01084              
 -94.42              -0.00897              
 -94.45              -0.00963              
 -94.48              -0.00949              
 -94.51              -0.00730              
 -94.54              -0.00629              
 -94.57              -0.00717              
 -94.6               -0.00813              
 -94.63              -0.00809              
 -94.66              -0.00805              
 -94.69              -0.00804              
 -94.72              -0.00813              
 -94.75              -0.00806              
 -94.78              -0.00694              
 -94.81              -0.00649              
 -94.84              -0.00694              
 -94.87              -0.00639              
 -94.9               -0.00409              
 -94.93              -0.00377              
 -94.96              -0.00401              
 -94.99              -0.00392              
 -95.02              -0.00394              
 -95.05              -0.00393              
 -95.08              -0.00402              
 -95.11              -0.00370              
 -95.14              -0.00436              
 -95.17              -0.00663              
 -95.2               -0.00668              
 -95.23              -0.00768              
 -95.26              -0.01086              
 -95.29              -0.01378              
 -95.32              -0.01475              
 -95.35              -0.01671              
 -95.38              -0.01857              
 -95.41              -0.01912              
 -95.44              -0.01907              
 -95.47              -0.01918              
 -95.5               -0.01830              
 -95.53              -0.01749              
 -95.56              -0.01779              
 -95.59              -0.01782              
 -95.62              -0.01575              
 -95.65              -0.01428              
 -95.68              -0.01288              
 -95.71              -0.01075              
 -95.74              -0.01073              
 -95.77              -0.01087              
 -95.8               -0.01081              
 -95.83              -0.01080              
 -95.86              -0.01080              
 -95.89              -0.01164              
 -95.92              -0.01363              
 -95.95              -0.01556              
 -95.98              -0.01636              
 -96.01              -0.01636              
 -96.04              -0.01616              
 -96.07              -0.01691              
 -96.1               -0.01781              
 -96.13              -0.01770              
 -96.16              -0.01775              
 -96.19              -0.01714              
 -96.22              -0.01548              
 -96.25              -0.01318              
 -96.28              -0.01101              
 -96.31              -0.00983              
 -96.34              -0.00872              
 -96.37              -0.00795              
 -96.4               -0.00807              
 -96.43              -0.00809              
 -96.46              -0.00802              
 -96.49              -0.00819              
 -96.52              -0.00788              
 -96.55              -0.00673              
 -96.58              -0.00671              
 -96.61              -0.00616              
 -96.64              -0.00480              
 -96.67              -0.00390              
 -96.7               -0.00392              
 -96.73              -0.00392              
 -96.76              -0.00406              
 -96.79              -0.00370              
 -96.82              -0.00257              
 -96.85              -0.00259              
 -96.88              -0.00197              
 -96.91              -0.00061              
 -96.94               0.00024              
 -96.97               0.00021              
 -97.                 0.00002              
 -97.03               0.00078              
 -97.06               0.00175              
 -97.09               0.00152              
 -97.12               0.00037              
 -97.15               0.00007              
 -97.18               0.00020              
 -97.21               0.00019              
 -97.24               0.00020              
 -97.27              -0.00057              
 -97.3               -0.00274              
 -97.33              -0.00414              
 -97.36              -0.00395              
 -97.39              -0.00494              
 -97.42              -0.00724              
 -97.45              -0.00832              
 -97.48              -0.00801              
 -97.51              -0.00807              
 -97.54              -0.00806              
 -97.57              -0.00811              
 -97.6               -0.00791              
 -97.63              -0.00632              
 -97.66              -0.00299              
 -97.69              -0.00100              
 -97.72              -0.00254              
 -97.75              -0.00386              
 -97.78              -0.00109              
 -97.81               0.00243              
 -97.84               0.00310              
 -97.87               0.00320              
 -97.9                0.00458              
 -97.93               0.00563              
 -97.96               0.00574              
 -97.99               0.00579              
 -98.02               0.00855              
 -98.05               0.01274              
 -98.08               0.01276              
 -98.11               0.01219              
 -98.14               0.01353              
 -98.17               0.01578              
 -98.2                0.01668              
 -98.23               0.01639              
 -98.26               0.01861              
 -98.29               0.02208              
 -98.32               0.02362              
 -98.35               0.02351              
 -98.38               0.02449              
 -98.41               0.02507              
 -98.44               0.02494              
 -98.47               0.02493              
 -98.5                0.02393              
 -98.53               0.02256              
 -98.56               0.02223              
 -98.59               0.02198              
 -98.62               0.01970              
 -98.65               0.01719              
 -98.68               0.01658              
 -98.71               0.01649              
 -98.74               0.01521              
 -98.77               0.01406              
 -98.8                0.01385              
 -98.83               0.01395              
 -98.86               0.01393              
 -98.89               0.01394              
 -98.92               0.01383              
 -98.95               0.01452              
 -98.98               0.01584              
 -99.01               0.01673              
 -99.04               0.01671              
 -99.07               0.01662              
 -99.1                0.01682              
 -99.13               0.01642              
 -99.16               0.01530              
 -99.19               0.01528              
 -99.22               0.01518              
 -99.25               0.01577              
 -99.28               0.01674              
 -99.31               0.01664              
 -99.34               0.01766              
 -99.37               0.01821              
 -99.4                0.01802              
 -99.43               0.01806              
 -99.46               0.01806              
 -99.49               0.01805              
 -99.52               0.01807              
 -99.55               0.01804              
 -99.58               0.01805              
 -99.61               0.01820              
 -99.64               0.01731              
 -99.67               0.01660              
 -99.7                0.01664              
 -99.73               0.01555              
 -99.76               0.01422              
 -99.79               0.01396              
 -99.82               0.01370              
 -99.85               0.01256              
 -99.88               0.01254              
 -99.91               0.01235              
 -99.94               0.01329              
 -99.97               0.01565              
 -100.                0.01774              
 -100.03              0.02106              
 -100.06              0.02306              
 -100.09              0.02391              
 -100.12              0.02496              
 -100.15              0.02571              
 -100.18              0.02980              
 -100.21              0.03241              
 -100.24              0.03164              
 -100.27              0.03175              
 -100.3               0.03302              
 -100.33              0.03261              
 -100.36              0.03162              
 -100.39              0.03184              
 -100.42              0.03187              
 -100.45              0.03119              
 -100.48              0.02914              
 -100.51              0.02751              
 -100.54              0.02769              
 -100.57              0.02745              
 -100.6               0.02927              
 -100.63              0.03061              
 -100.66              0.03054              
 -100.69              0.03277              
 -100.72              0.03627              
 -100.75              0.03800              
 -100.78              0.0394               
 -100.81              0.04298              
 -100.84              0.04649              
 -100.87              0.04710              
 -100.9               0.04723              
 -100.93              0.04861              
 -100.96              0.04965              
 -100.99              0.04975              
 -101.02              0.04967              
 -101.05              0.04970              
 -101.08              0.04969              
 -101.11              0.04968              
 -101.14              0.04973              
 -101.17              0.04958              
 -101.2               0.04991              
 -101.23              0.05105              
 -101.26              0.05184              
 -101.29              0.05487              
 -101.32              0.05687              
 -101.35              0.05664              
 -101.38              0.05785              
 -101.41              0.05737              
 -101.44              0.05517              
 -101.47              0.05351              
 -101.5               0.05237              
 -101.53              0.04906              
 -101.56              0.04715              
 -101.59              0.04690              
 -101.62              0.04696              
 -101.65              0.04696              
 -101.68              0.04680              
 -101.71              0.04763              
 -101.74              0.04846              
 -101.77              0.04830              
 -101.8               0.04830              
 -101.83              0.04833              
 -101.86              0.04820              
 -101.89              0.04605              
 -101.92              0.04156              
 -101.95              0.03919              
 -101.98              0.03731              
 -102.01              0.03496              
 -102.04              0.03299              
 -102.07              0.03194              
 -102.1               0.03094              
 -102.13              0.02971              
 -102.16              0.02896              
 -102.19              0.02906              
 -102.22              0.02910              
 -102.25              0.02891              
 -102.28              0.02952              
 -102.31              0.03054              
 -102.34              0.03047              
 -102.37              0.03026              
 -102.4               0.03115              
 -102.43              0.03189              
 -102.46              0.03184              
 -102.49              0.03289              
 -102.52              0.03420              
 -102.55              0.03464              
 -102.58              0.03459              
 -102.61              0.03459              
 -102.64              0.03349              
 -102.67              0.03305              
 -102.7               0.03323              
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 -102.76              0.03318              
 -102.79              0.03319              
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 -102.91              0.03314              
 -102.94              0.03337              
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 -103.                0.03187              
 -103.03              0.03309              
 -103.06              0.03327              
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 -103.12              0.03569              
 -103.15              0.03878              
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 -103.21              0.03933              
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 -103.51              0.04162              
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 -103.75              0.04233              
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 -103.81              0.04460              
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 -104.11              0.04262              
 -104.14              0.04153              
 -104.17              0.04087              
 -104.2               0.03835              
 -104.23              0.03536              
 -104.26              0.03456              
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 -104.32              0.03454              
 -104.35              0.03464              
 -104.38              0.03446              
 -104.41              0.03435              
 -104.44              0.03754              
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 -104.5               0.03880              
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 -104.68              0.04686              
 -104.71              0.04706              
 -104.74              0.04689              
 -104.77              0.04694              
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 -104.83              0.04700              
 -104.86              0.04662              
 -104.89              0.04814              
 -104.92              0.04977              
 -104.95              0.04835              
 -104.98              0.04702              
 -105.01              0.04722              
 -105.04              0.04591              
 -105.07              0.04233              
 -105.1               0.04018              
 -105.13              0.04003              
 -105.16              0.03971              
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 -105.22              0.03588              
 -105.25              0.03465              
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 -105.31              0.03410              
 -105.34              0.03309              
 -105.37              0.03318              
 -105.4               0.03310              
 -105.43              0.03376              
 -105.46              0.03499              
 -105.49              0.03602              
 -105.52              0.03710              
 -105.55              0.03821              
 -105.58              0.03908              
 -105.61              0.03817              
 -105.64              0.03596              
 -105.67              0.03690              
 -105.7               0.03749              
 -105.73              0.03736              
 -105.76              0.03910              
 -105.79              0.04252              
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 -105.85              0.04332              
 -105.88              0.04435              
 -105.91              0.04419              
 -105.94              0.04417              
 -105.97              0.04420              
 -106.                0.04419              
 -106.03              0.04419              
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 -106.12              0.04422              
 -106.15              0.04413              
 -106.18              0.04423              
 -106.21              0.04531              
 -106.24              0.04644              
 -106.27              0.04750              
 -106.3               0.04856              
 -106.33              0.04964              
 -106.36              0.05083              
 -106.39              0.05117              
 -106.42              0.05104              
 -106.45              0.05107              
 -106.48              0.05106              
 -106.51              0.05111              
 -106.54              0.05094              
 -106.57              0.05133              
 -106.6               0.05245              
 -106.63              0.05250              
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 -106.84              0.05242              
 -106.87              0.05246              
 -106.9               0.05256              
 -106.93              0.05149              
 -106.96              0.05115              
 -106.99              0.05070              
 -107.02              0.04839              
 -107.05              0.04813              
 -107.08              0.04853              
 -107.11              0.04793              
 -107.14              0.04686              
 -107.17              0.04685              
 -107.2               0.04771              
 -107.23              0.04930              
 -107.26              0.05194              
 -107.29              0.05520              
 -107.32              0.05813              
 -107.35              0.06349              
 -107.38              0.06715              
 -107.41              0.06774              
 -107.44              0.06998              
 -107.47              0.07324              
 -107.5               0.07601              
 -107.53              0.07760              
 -107.56              0.07865              
 -107.59              0.08067              
 -107.62              0.08398              
 -107.65              0.08640              
 -107.68              0.08909              
 -107.71              0.09473              
 -107.74              0.09971              
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##END=
