##TITLE=	29Si MAS NMR spectrum of as-synthesized MCM-61
##JCAMP-DX=	5.01
##DATA TYPE=	NMR SPECTRUM
##DATA CLASS=	XYDATA
##ORIGIN=	"Shantz et al., Micropor. Mesopor. Mater., 31, 61-73 (1999) Figure 3"
##OWNER=	"processed by H. Koller, University of Münster"
##LONG DATE=	27.12.2019 11:00
##SOURCE REFERENCE=	MSO-29Si-Shantz-1999-MCM61
##DATA PROCESSING=	"Spectrum digitized with WebPlotDigitizer and deconvoluted with dmfit: D. Massiot et al., Magn. Reson. Chem., 40, 70-76 (2002)"
	
$$Sample information	
##NAMES=	MSO
##NAMES=	as-synthesized MCM-61
##NAMES=	as-synthesized MCM-61
##SAMPLE DESCRIPTION=	"synthetic MCM-61 with Si/Al=13.2 (chemical analysis)"
##TEMPERATURE=	N.A.
	
"
$$Bibliographic information"	
##$AUTHORS=	Shantz, D.F.; Burton, A.; Lobo, R.F.
##$TITLE=	Synthesis, structure solution, and characterization of the aluminosilicate MCM-61: the first aluminosilicate clathrate with 18-membered rings
##$JOURNAL=	Micropor. Mesopor. Mater.
##$VOLUME=	31
##$PAGES=	61-73
##$YEAR=	1999
##$DOI=	
##$FIGURE=	Figure 3
	
$$Peak information	(Positions in ppm, Relative peak areas, Peak widths in ppm, Lorentzian/Gaussian shape parameter)
##$NUM PEAKS=	3
##$PEAK TSITES=	0                    0                    0                                                                                                                                                                                                                                                                                                                                                                                                                                                                              
##$PEAK LABELS=	A                   B                    C                                                                                                                                                                                                                                                                                                                                                                                                                                                                              
##$Q TYPE=	Q4(0Al)      Q4(0Al)      Q4(1Al)                                                                                                                                                          
##$PEAK POSITIONS=	-115.29        -112.04        -106.6                                                                                                                                                                          
##$PEAK AREAS=	32.58             44.7             22.71                                                                                                                                                                                                                  
##$PEAK WIDTHS=	3.94               4.27               5.84                                                                                                                                                                                                                                  
##$PEAK SHAPES=	0.2               0.2               0.2                                                                                                                                                                                                                                  
##$PEAK_CQ=	
##$PEAK_etaQ=	
##$NUMBERING REF=	
##$ASSIGN REF=	
##$ASSIGN METHOD=	
	
$$Spectrum acquisition information	
##.OBSERVE NUCLEUS=	29Si
##.OBSERVE FREQUENCY=	59.63
##.PULSE SEQUENCE=	single pulse
##.MAS FREQUENCY=	3
	
$$Spectrum data information	
##XUNITS=	ppm
##YUNITS=	arbitrary units
##FIRSTX=	-70.40
##LASTX=	-139.00
##XFACTOR=	1
##YFACTOR=	1
##NPOINTS=	344
##FIRSTY=	-0.0317
	
$$Spectrum data	
##XYDATA=	(X++(Y..Y))
-70.4000	-0.0316
-70.6000	-0.0275
-70.8000	-0.0317
-71.0000	-0.0348
-71.2000	-0.0380
-71.4000	-0.0380
-71.6000	-0.0380
-71.8000	-0.0359
-72.0000	-0.0296
-72.2000	-0.0264
-72.4000	-0.0264
-72.6000	-0.0264
-72.8000	-0.0264
-73.0000	-0.0264
-73.2000	-0.0264
-73.4000	-0.0264
-73.6000	-0.0275
-73.8000	-0.0212
-74.0000	-0.0212
-74.2000	-0.0212
-74.4000	-0.0212
-74.6000	-0.0254
-74.8000	-0.0327
-75.0000	-0.0317
-75.2000	-0.0275
-75.4000	-0.0201
-75.6000	-0.0138
-75.8000	-0.0096
-76.0000	-0.0033
-76.2000	0.0009
-76.4000	0.0009
-76.6000	-0.0044
-76.8000	-0.0075
-77.0000	-0.0138
-77.2000	-0.0159
-77.4000	-0.0159
-77.6000	-0.0159
-77.8000	-0.0159
-78.0000	-0.0159
-78.2000	-0.0149
-78.4000	-0.0107
-78.6000	-0.0044
-78.8000	0.0009
-79.0000	-0.0002
-79.2000	-0.0044
-79.4000	-0.0044
-79.6000	-0.0075
-79.8000	-0.0044
-80.0000	-0.0075
-80.2000	-0.0107
-80.4000	-0.0107
-80.6000	-0.0044
-80.8000	-0.0012
-81.0000	0.0040
-81.2000	0.0072
-81.4000	0.0061
-81.6000	0.0061
-81.8000	0.0061
-82.0000	0.0061
-82.2000	0.0051
-82.4000	-0.0044
-82.6000	-0.0107
-82.8000	-0.0170
-83.0000	-0.0128
-83.2000	-0.0075
-83.4000	-0.0044
-83.6000	-0.0054
-83.8000	-0.0086
-84.0000	-0.0117
-84.2000	-0.0149
-84.4000	-0.0159
-84.6000	-0.0170
-84.8000	-0.0254
-85.0000	-0.0338
-85.2000	-0.0380
-85.4000	-0.0380
-85.6000	-0.0380
-85.8000	-0.0306
-86.0000	-0.0201
-86.2000	-0.0159
-86.4000	-0.0159
-86.6000	-0.0191
-86.8000	-0.0233
-87.0000	-0.0264
-87.2000	-0.0212
-87.4000	-0.0212
-87.6000	-0.0149
-87.8000	-0.0191
-88.0000	-0.0212
-88.2000	-0.0212
-88.4000	-0.0201
-88.6000	-0.0159
-88.8000	-0.0149
-89.0000	-0.0159
-89.2000	-0.0159
-89.4000	-0.0222
-89.6000	-0.0201
-89.8000	-0.0159
-90.0000	-0.0033
-90.2000	0.0040
-90.4000	0.0093
-90.6000	0.0114
-90.8000	0.0051
-91.0000	-0.0012
-91.2000	-0.0075
-91.4000	-0.0138
-91.6000	-0.0159
-91.8000	-0.0159
-92.0000	-0.0107
-92.2000	-0.0096
-92.4000	-0.0023
-92.6000	0.0040
-92.8000	0.0103
-93.0000	0.0177
-93.2000	0.0177
-93.4000	0.0156
-93.6000	0.0082
-93.8000	0.0019
-94.0000	-0.0044
-94.2000	-0.0138
-94.4000	-0.0159
-94.6000	-0.0138
-94.8000	-0.0086
-95.0000	-0.0012
-95.2000	0.0009
-95.4000	0.0009
-95.6000	0.0009
-95.8000	0.0009
-96.0000	0.0103
-96.2000	0.0198
-96.4000	0.0240
-96.6000	0.0187
-96.8000	0.0177
-97.0000	0.0177
-97.2000	0.0187
-97.4000	0.0240
-97.6000	0.0250
-97.8000	0.0271
-98.0000	0.0281
-98.2000	0.0302
-98.4000	0.0344
-98.6000	0.0439
-98.8000	0.0449
-99.0000	0.0512
-99.2000	0.0512
-99.4000	0.0491
-99.6000	0.0460
-99.8000	0.0449
-100.0000	0.0386
-100.2000	0.0407
-100.4000	0.0460
-100.6000	0.0512
-100.8000	0.0512
-101.0000	0.0512
-101.2000	0.0502
-101.4000	0.0502
-101.6000	0.0565
-101.8000	0.0638
-102.0000	0.0764
-102.2000	0.0859
-102.4000	0.0964
-102.6000	0.1037
-102.8000	0.1069
-103.0000	0.1142
-103.2000	0.1205
-103.4000	0.1300
-103.6000	0.1425
-103.8000	0.1530
-104.0000	0.1656
-104.2000	0.1877
-104.4000	0.2118
-104.6000	0.2381
-104.8000	0.2548
-105.0000	0.2758
-105.2000	0.2947
-105.4000	0.3052
-105.6000	0.3210
-105.8000	0.3283
-106.0000	0.3378
-106.2000	0.3388
-106.4000	0.3409
-106.6000	0.3441
-106.8000	0.3451
-107.0000	0.3483
-107.2000	0.3504
-107.4000	0.3504
-107.6000	0.3472
-107.8000	0.3462
-108.0000	0.3483
-108.2000	0.3556
-108.4000	0.3650
-108.6000	0.3850
-108.8000	0.4007
-109.0000	0.4228
-109.2000	0.4522
-109.4000	0.4857
-109.6000	0.5214
-109.8000	0.5424
-110.0000	0.5760
-110.2000	0.6169
-110.4000	0.6621
-110.6000	0.7019
-110.8000	0.7471
-111.0000	0.7922
-111.2000	0.8426
-111.4000	0.8877
-111.6000	0.9255
-111.8000	0.9633
-112.0000	0.9853
-112.2000	1.0000
-112.4000	1.0000
-112.6000	1.0000
-112.8000	0.9948
-113.0000	0.9885
-113.2000	0.9885
-113.4000	0.9853
-113.6000	0.9790
-113.8000	0.9654
-114.0000	0.9465
-114.2000	0.9328
-114.4000	0.9223
-114.6000	0.9108
-114.8000	0.8982
-115.0000	0.8814
-115.2000	0.8615
-115.4000	0.8363
-115.6000	0.8048
-115.8000	0.7670
-116.0000	0.7135
-116.2000	0.6694
-116.4000	0.6075
-116.6000	0.5277
-116.8000	0.4605
-117.0000	0.4091
-117.2000	0.3682
-117.4000	0.3220
-117.6000	0.2737
-117.8000	0.2276
-118.0000	0.2055
-118.2000	0.1845
-118.4000	0.1593
-118.6000	0.1404
-118.8000	0.1247
-119.0000	0.1142
-119.2000	0.1037
-119.4000	0.0922
-119.6000	0.0796
-119.8000	0.0649
-120.0000	0.0586
-120.2000	0.0523
-120.4000	0.0502
-120.6000	0.0460
-120.8000	0.0397
-121.0000	0.0397
-121.2000	0.0376
-121.4000	0.0365
-121.6000	0.0418
-121.8000	0.0449
-122.0000	0.0449
-122.2000	0.0439
-122.4000	0.0355
-122.6000	0.0344
-122.8000	0.0344
-123.0000	0.0344
-123.2000	0.0386
-123.4000	0.0397
-123.6000	0.0376
-123.8000	0.0302
-124.0000	0.0219
-124.2000	0.0177
-124.4000	0.0208
-124.6000	0.0261
-124.8000	0.0323
-125.0000	0.0355
-125.2000	0.0365
-125.4000	0.0292
-125.6000	0.0292
-125.8000	0.0229
-126.0000	0.0250
-126.2000	0.0323
-126.4000	0.0344
-126.6000	0.0344
-126.8000	0.0302
-127.0000	0.0208
-127.2000	0.0103
-127.4000	0.0051
-127.6000	-0.0023
-127.8000	-0.0086
-128.0000	-0.0159
-128.2000	-0.0201
-128.4000	-0.0243
-128.6000	-0.0243
-128.8000	-0.0191
-129.0000	-0.0075
-129.2000	0.0040
-129.4000	0.0114
-129.6000	0.0124
-129.8000	0.0103
-130.0000	0.0030
-130.2000	-0.0033
-130.4000	-0.0096
-130.6000	-0.0107
-130.8000	-0.0107
-131.0000	-0.0096
-131.2000	-0.0128
-131.4000	-0.0159
-131.6000	-0.0159
-131.8000	-0.0138
-132.0000	-0.0054
-132.2000	-0.0054
-132.4000	0.0009
-132.6000	0.0009
-132.8000	-0.0023
-133.0000	-0.0044
-133.2000	-0.0096
-133.4000	-0.0159
-133.6000	-0.0159
-133.8000	-0.0159
-134.0000	-0.0159
-134.2000	-0.0159
-134.4000	-0.0149
-134.6000	-0.0096
-134.8000	-0.0086
-135.0000	-0.0054
-135.2000	-0.0044
-135.4000	-0.0086
-135.6000	-0.0138
-135.8000	-0.0191
-136.0000	-0.0222
-136.2000	-0.0159
-136.4000	-0.0054
-136.6000	-0.0002
-136.8000	0.0009
-137.0000	0.0009
-137.2000	0.0009
-137.4000	0.0009
-137.6000	0.0009
-137.8000	0.0009
-138.0000	0.0009
-138.2000	-0.0044
-138.4000	-0.0054
-138.6000	-0.0117
-138.8000	-0.0159
-139.0000	-0.0159
##END=	
