##TITLE=              29Si CP MAS NMR spectrum of natural melanophlogite (cubic phase at 363 K)
##JCAMP-DX=           5.01
##DATA TYPE=          NMR SPECTRUM
##DATA CLASS=         XYDATA
##ORIGIN=             Fyfe and Gies. J. Inclusion Phenom. Mol. Recognit. Chem., 8, 235-239 (1990) Figure 1a
##OWNER=              Digitized and processed by Brouwer Lab, Redeemer University College
##LONG DATE=          2019/08/08 15:09:29
##SOURCE REFERENCE=   MEP-29Si-Fyfe-1990-363K
##DATA PROCESSING=    Spectrum digitized with WebPlotDigitizer and deconvoluted with Mathematica notebook

$$Sample information 
##NAMES=              MEP
##NAMES=              Melanophlogite
##SAMPLE DESCRIPTION= Melanophlogite, cubic phase
##TEMPERATURE=        363 K

$$Bibliographic information 
##$AUTHORS=           Fyfe, C.A., Gies, H.
##$TITLE=             A 29Si NMR study of natural and synthetic melanophlogites, the silica analogues of the clathrate hydrates of type I
##$JOURNAL=           Journal of Inclusion Phenomena and Molecular Recognition in Chemistry
##$VOLUME=            8
##$PAGES=             235-239
##$YEAR=              1990
##$DOI=               10.1007/BF01131300
##$FIGURE=            Figure 1a

$$Peak information    (Positions in ppm, Relative peak areas, Peak widths in ppm, Lorentzian/Gaussian shape parameter)
##$NUM PEAKS=         3
##$PEAK LABELS=        Si3        Si2        Si1       
##$PEAK TSITES=        T3         T2         T1        
##$PEAK POSITIONS=    -121.364   -119.956   -118.364   
##$PEAK AREAS=         3.         8.         12.       
##$PEAK WIDTHS=        0.81153    0.87386    0.80869   
##$PEAK SHAPES=        0.46668    0.46668    0.46668   
##$NUMBERING REF=     Gies, H. Z. Kristallogr. 164, 247-257 (1983)
##$ASSIGN REF=        Fyfe and Gies. J. Inclusion Phenom. Mol. Recognit. Chem., 8, 235-239 (1990) Figure 1a
##$ASSIGN METHOD=     relative intensities
##$COMMENT=           

$$Spectrum acquisition information 
##.OBSERVE NUCLEUS=   ^29Si
##.OBSERVE FREQUENCY= 79.6
##.PULSE SEQUENCE=    cross polarization
##.MAS FREQUENCY=     3500

$$Spectrum data information 
##XUNITS=             PPM
##YUNITS=             ARBITRARY UNITS
##FIRSTX=             -109.2                
##LASTX=              -129.24               
##XFACTOR=            1
##YFACTOR=            1
##NPOINTS=            1003
##FIRSTY=              0.28973              

$$Spectrum data
##XYDATA=             (X++(Y..Y))
 -109.2               0.28973              
 -109.22              0.30129              
 -109.24              0.30614              
 -109.26              0.30280              
 -109.28              0.30944              
 -109.3               0.34933              
 -109.32              0.42027              
 -109.34              0.48428              
 -109.36              0.50594              
 -109.38              0.49110              
 -109.4               0.46492              
 -109.42              0.44448              
 -109.44              0.42869              
 -109.46              0.41397              
 -109.48              0.39720              
 -109.5               0.37557              
 -109.52              0.34801              
 -109.54              0.31972              
 -109.56              0.29715              
 -109.58              0.28044              
 -109.6               0.26243              
 -109.62              0.23710              
 -109.64              0.20819              
 -109.66              0.18308              
 -109.68              0.16475              
 -109.7               0.14814              
 -109.72              0.12808              
 -109.74              0.10763              
 -109.76              0.09487              
 -109.78              0.09381              
 -109.8               0.09625              
 -109.82              0.09219              
 -109.84              0.08128              
 -109.86              0.07248              
 -109.88              0.07351              
 -109.9               0.08435              
 -109.92              0.10257              
 -109.94              0.12367              
 -109.96              0.14003              
 -109.98              0.14566              
 -110.                0.15029              
 -110.02              0.17143              
 -110.04              0.21608              
 -110.06              0.26592              
 -110.08              0.30017              
 -110.1               0.31701              
 -110.12              0.32958              
 -110.14              0.34782              
 -110.16              0.36740              
 -110.18              0.38061              
 -110.2               0.38374              
 -110.22              0.37798              
 -110.24              0.36485              
 -110.26              0.34612              
 -110.28              0.32362              
 -110.3               0.29837              
 -110.32              0.26979              
 -110.34              0.23720              
 -110.36              0.20108              
 -110.38              0.16265              
 -110.4               0.12371              
 -110.42              0.08787              
 -110.44              0.05884              
 -110.46              0.03417              
 -110.48              0.00518              
 -110.5              -0.03401              
 -110.52             -0.07309              
 -110.54             -0.09657              
 -110.56             -0.09940              
 -110.58             -0.09308              
 -110.6              -0.08947              
 -110.62             -0.09023              
 -110.64             -0.09165              
 -110.66             -0.09144              
 -110.68             -0.09115              
 -110.7              -0.09272              
 -110.72             -0.09446              
 -110.74             -0.09165              
 -110.76             -0.08167              
 -110.78             -0.07107              
 -110.8              -0.06867              
 -110.82             -0.07678              
 -110.84             -0.08926              
 -110.86             -0.10012              
 -110.88             -0.10873              
 -110.9              -0.11680              
 -110.92             -0.12548              
 -110.94             -0.13483              
 -110.96             -0.14471              
 -110.98             -0.15425              
 -111.               -0.16209              
 -111.02             -0.16661              
 -111.04             -0.16546              
 -111.06             -0.15624              
 -111.08             -0.13921              
 -111.1              -0.11754              
 -111.12             -0.09384              
 -111.14             -0.06689              
 -111.16             -0.03416              
 -111.18              0.00353              
 -111.2               0.03975              
 -111.22              0.06850              
 -111.24              0.09340              
 -111.26              0.12353              
 -111.28              0.16263              
 -111.3               0.19985              
 -111.32              0.22253              
 -111.34              0.23070              
 -111.36              0.23564              
 -111.38              0.24597              
 -111.4               0.25656              
 -111.42              0.25858              
 -111.44              0.24996              
 -111.46              0.23809              
 -111.48              0.22979              
 -111.5               0.22242              
 -111.52              0.20896              
 -111.54              0.18550              
 -111.56              0.15501              
 -111.58              0.12122              
 -111.6               0.08549              
 -111.62              0.04746              
 -111.64              0.00788              
 -111.66             -0.02834              
 -111.68             -0.05556              
 -111.7              -0.07374              
 -111.72             -0.08925              
 -111.74             -0.10760              
 -111.76             -0.12674              
 -111.78             -0.14184              
 -111.8              -0.14847              
 -111.82             -0.14298              
 -111.84             -0.12262              
 -111.86             -0.09317              
 -111.88             -0.06559              
 -111.9              -0.04659              
 -111.92             -0.03041              
 -111.94             -0.00937              
 -111.96              0.01795              
 -111.98              0.04703              
 -112.                0.07417              
 -112.02              0.10073              
 -112.04              0.12951              
 -112.06              0.15964              
 -112.08              0.18475              
 -112.1               0.19855              
 -112.12              0.19891              
 -112.14              0.18576              
 -112.16              0.16096              
 -112.18              0.13095              
 -112.2               0.10243              
 -112.22              0.07619              
 -112.24              0.04846              
 -112.26              0.01751              
 -112.28             -0.01020              
 -112.3              -0.02649              
 -112.32             -0.03277              
 -112.34             -0.04208              
 -112.36             -0.06462              
 -112.38             -0.08748              
 -112.4              -0.08860              
 -112.42             -0.05878              
 -112.44             -0.01331              
 -112.46              0.03070              
 -112.48              0.06738              
 -112.5               0.09799              
 -112.52              0.12457              
 -112.54              0.15113              
 -112.56              0.18188              
 -112.58              0.21769              
 -112.6               0.25603              
 -112.62              0.29329              
 -112.64              0.32109              
 -112.66              0.32965              
 -112.68              0.31642              
 -112.7               0.29028              
 -112.72              0.26006              
 -112.74              0.22544              
 -112.76              0.18129              
 -112.78              0.12656              
 -112.8               0.07047              
 -112.82              0.02328              
 -112.84             -0.01324              
 -112.86             -0.04441              
 -112.88             -0.07431              
 -112.9              -0.10138              
 -112.92             -0.12259              
 -112.94             -0.13558              
 -112.96             -0.13887              
 -112.98             -0.13124              
 -113.               -0.11273              
 -113.02             -0.08396              
 -113.04             -0.04752              
 -113.06             -0.01007              
 -113.08              0.02214              
 -113.1               0.05424              
 -113.12              0.09899              
 -113.14              0.16110              
 -113.16              0.21787              
 -113.18              0.24181              
 -113.2               0.22756              
 -113.22              0.19325              
 -113.24              0.15586              
 -113.26              0.11979              
 -113.28              0.08507              
 -113.3               0.05059              
 -113.32              0.01332              
 -113.34             -0.02943              
 -113.36             -0.07569              
 -113.38             -0.12085              
 -113.4              -0.16119              
 -113.42             -0.19538              
 -113.44             -0.22233              
 -113.46             -0.23732              
 -113.48             -0.23249              
 -113.5              -0.20234              
 -113.52             -0.15226              
 -113.54             -0.09064              
 -113.56             -0.02524              
 -113.58              0.03705              
 -113.6               0.09029              
 -113.62              0.13476              
 -113.64              0.17361              
 -113.66              0.20975              
 -113.68              0.24553              
 -113.7               0.28265              
 -113.72              0.31474              
 -113.74              0.32961              
 -113.76              0.31843              
 -113.78              0.28483              
 -113.8               0.23525              
 -113.82              0.17832              
 -113.84              0.12508              
 -113.86              0.08433              
 -113.88              0.05081              
 -113.9               0.01408              
 -113.92             -0.03055              
 -113.94             -0.07777              
 -113.96             -0.12147              
 -113.98             -0.15863              
 -114.               -0.18801              
 -114.02             -0.20752              
 -114.04             -0.21258              
 -114.06             -0.19836              
 -114.08             -0.16515              
 -114.1              -0.11793              
 -114.12             -0.06235              
 -114.14             -0.00650              
 -114.16              0.04094              
 -114.18              0.07776              
 -114.2               0.11108              
 -114.22              0.14765              
 -114.24              0.18540              
 -114.26              0.21795              
 -114.28              0.23885              
 -114.3               0.24146              
 -114.32              0.21997              
 -114.34              0.18124              
 -114.36              0.14178              
 -114.38              0.11340              
 -114.4               0.08887              
 -114.42              0.05685              
 -114.44              0.01706              
 -114.46             -0.01742              
 -114.48             -0.03531              
 -114.5              -0.04138              
 -114.52             -0.04661              
 -114.54             -0.05384              
 -114.56             -0.05049              
 -114.58             -0.02368              
 -114.6               0.02328              
 -114.62              0.07700              
 -114.64              0.12669              
 -114.66              0.17015              
 -114.68              0.20697              
 -114.7               0.24080              
 -114.72              0.27923              
 -114.74              0.32716              
 -114.76              0.37496              
 -114.78              0.40854              
 -114.8               0.42227              
 -114.82              0.42365              
 -114.84              0.42037              
 -114.86              0.41252              
 -114.88              0.39625              
 -114.9               0.36837              
 -114.92              0.32747              
 -114.94              0.27298              
 -114.96              0.21369              
 -114.98              0.16597              
 -115.                0.14100              
 -115.02              0.12787              
 -115.04              0.11036              
 -115.06              0.08291              
 -115.08              0.05352              
 -115.1               0.02996              
 -115.12              0.01266              
 -115.14             -0.00106              
 -115.16             -0.01249              
 -115.18             -0.02002              
 -115.2              -0.02203              
 -115.22             -0.02089              
 -115.24             -0.02157              
 -115.26             -0.02769              
 -115.28             -0.03823              
 -115.3              -0.05129              
 -115.32             -0.06726              
 -115.34             -0.08889              
 -115.36             -0.11756              
 -115.38             -0.14654              
 -115.4              -0.16644              
 -115.42             -0.17509              
 -115.44             -0.18208              
 -115.46             -0.19684              
 -115.48             -0.21700              
 -115.5              -0.23372              
 -115.52             -0.24041              
 -115.54             -0.23670              
 -115.56             -0.22335              
 -115.58             -0.20417              
 -115.6              -0.18556              
 -115.62             -0.17145              
 -115.64             -0.15455              
 -115.66             -0.12469              
 -115.68             -0.08021              
 -115.7              -0.03084              
 -115.72              0.01370              
 -115.74              0.04998              
 -115.76              0.07731              
 -115.78              0.09672              
 -115.8               0.11284              
 -115.82              0.13039              
 -115.84              0.14938              
 -115.86              0.16644              
 -115.88              0.17891              
 -115.9               0.18670              
 -115.92              0.19035              
 -115.94              0.19079              
 -115.96              0.18939              
 -115.98              0.18761              
 -116.                0.18734              
 -116.02              0.19055              
 -116.04              0.19811              
 -116.06              0.20892              
 -116.08              0.22145              
 -116.1               0.23206              
 -116.12              0.23587              
 -116.14              0.23210              
 -116.16              0.23152              
 -116.18              0.24625              
 -116.2               0.27512              
 -116.22              0.30482              
 -116.24              0.32377              
 -116.26              0.33064              
 -116.28              0.32716              
 -116.3               0.31715              
 -116.32              0.30749              
 -116.34              0.30428              
 -116.36              0.30562              
 -116.38              0.30578              
 -116.4               0.30052              
 -116.42              0.28901              
 -116.44              0.27119              
 -116.46              0.25106              
 -116.48              0.23569              
 -116.5               0.23026              
 -116.52              0.23263              
 -116.54              0.23898              
 -116.56              0.24729              
 -116.58              0.25762              
 -116.6               0.27044              
 -116.62              0.28817              
 -116.64              0.31394              
 -116.66              0.34832              
 -116.68              0.38714              
 -116.7               0.42595              
 -116.72              0.46258              
 -116.74              0.49635              
 -116.76              0.52657              
 -116.78              0.55251              
 -116.8               0.57355              
 -116.82              0.59115              
 -116.84              0.60879              
 -116.86              0.62884              
 -116.88              0.64775              
 -116.9               0.66018              
 -116.92              0.66347              
 -116.94              0.65904              
 -116.96              0.64896              
 -116.98              0.63827              
 -117.                0.63345              
 -117.02              0.63623              
 -117.04              0.63676              
 -117.06              0.62436              
 -117.08              0.60268              
 -117.1               0.58680              
 -117.12              0.58800              
 -117.14              0.60095              
 -117.16              0.61636              
 -117.18              0.63161              
 -117.2               0.65242              
 -117.22              0.68374              
 -117.24              0.72179              
 -117.26              0.75927              
 -117.28              0.79329              
 -117.3               0.82983              
 -117.32              0.87533              
 -117.34              0.92977              
 -117.36              0.98888              
 -117.38              1.04967              
 -117.4               1.11357              
 -117.42              1.18291              
 -117.44              1.26045              
 -117.46              1.3494               
 -117.48              1.45173              
 -117.5               1.56259              
 -117.52              1.67489              
 -117.54              1.78446              
 -117.56              1.89173              
 -117.58              1.99938              
 -117.6               2.12644              
 -117.62              2.30075              
 -117.64              2.52928              
 -117.66              2.7648               
 -117.68              2.95429              
 -117.7               3.09499              
 -117.72              3.2268               
 -117.74              3.38655              
 -117.76              3.59199              
 -117.78              3.8551               
 -117.8               4.15827              
 -117.82              4.44474              
 -117.84              4.66787              
 -117.86              4.8738               
 -117.88              5.14917              
 -117.9               5.52948              
 -117.92              5.94234              
 -117.94              6.30675              
 -117.96              6.60632              
 -117.98              6.86985              
 -118.                7.12573              
 -118.02              7.39769              
 -118.04              7.70746              
 -118.06              8.0488               
 -118.08              8.38493              
 -118.1               8.68653              
 -118.12              8.97601              
 -118.14              9.29389              
 -118.16              9.65396              
 -118.18              10.0241              
 -118.2               10.3704              
 -118.22              10.6875              
 -118.24              10.9858              
 -118.26              11.2693              
 -118.28              11.523               
 -118.3               11.7294              
 -118.32              11.8939              
 -118.34              12.0418              
 -118.36              12.1896              
 -118.38              12.3096              
 -118.4               12.3618              
 -118.42              12.338               
 -118.44              12.2743              
 -118.46              12.2021              
 -118.48              12.0903              
 -118.5               11.8788              
 -118.52              11.5469              
 -118.54              11.1627              
 -118.56              10.8012              
 -118.58              10.463               
 -118.6               10.0933              
 -118.62              9.65045              
 -118.64              9.14727              
 -118.66              8.60898              
 -118.68              8.06456              
 -118.7               7.54737              
 -118.72              7.08436              
 -118.74              6.66156              
 -118.76              6.24976              
 -118.78              5.84609              
 -118.8               5.49591              
 -118.82              5.24299              
 -118.84              5.05845              
 -118.86              4.86912              
 -118.88              4.63067              
 -118.9               4.38581              
 -118.92              4.19115              
 -118.94              4.05942              
 -118.96              3.9614               
 -118.98              3.86922              
 -119.                3.77017              
 -119.02              3.65635              
 -119.04              3.53157              
 -119.06              3.41707              
 -119.08              3.33199              
 -119.1               3.26555              
 -119.12              3.19208              
 -119.14              3.09687              
 -119.16              2.99165              
 -119.18              2.89163              
 -119.2               2.80584              
 -119.22              2.73849              
 -119.24              2.6903               
 -119.26              2.6489               
 -119.28              2.59896              
 -119.3               2.53602              
 -119.32              2.46891              
 -119.34              2.40884              
 -119.36              2.37734              
 -119.38              2.4                  
 -119.4               2.48701              
 -119.42              2.61859              
 -119.44              2.77159              
 -119.46              2.92384              
 -119.48              3.05378              
 -119.5               3.15853              
 -119.52              3.2941               
 -119.54              3.52498              
 -119.56              3.84232              
 -119.58              4.16276              
 -119.6               4.41961              
 -119.62              4.65119              
 -119.64              4.9293               
 -119.66              5.26532              
 -119.68              5.57452              
 -119.7               5.77708              
 -119.72              5.915                
 -119.74              6.09488              
 -119.76              6.37251              
 -119.78              6.67279              
 -119.8               6.90459              
 -119.82              7.05353              
 -119.84              7.16947              
 -119.86              7.29442              
 -119.88              7.4291               
 -119.9               7.56316              
 -119.92              7.68088              
 -119.94              7.75946              
 -119.96              7.7793               
 -119.98              7.74703              
 -120.                7.68057              
 -120.02              7.59002              
 -120.04              7.46923              
 -120.06              7.31139              
 -120.08              7.12707              
 -120.1               6.93885              
 -120.12              6.75672              
 -120.14              6.54734              
 -120.16              6.27032              
 -120.18              5.93888              
 -120.2               5.62401              
 -120.22              5.38426              
 -120.24              5.19187              
 -120.26              4.98926              
 -120.28              4.75025              
 -120.3               4.50184              
 -120.32              4.27263              
 -120.34              4.05711              
 -120.36              3.8305               
 -120.38              3.58504              
 -120.4               3.3598               
 -120.42              3.19908              
 -120.44              3.09646              
 -120.46              3.00054              
 -120.48              2.87132              
 -120.5               2.72727              
 -120.52              2.60287              
 -120.54              2.50995              
 -120.56              2.42891              
 -120.58              2.34065              
 -120.6               2.24732              
 -120.62              2.16086              
 -120.64              2.087                
 -120.66              2.01761              
 -120.68              1.94358              
 -120.7               1.86764              
 -120.72              1.80118              
 -120.74              1.75143              
 -120.76              1.70993              
 -120.78              1.665                
 -120.8               1.61578              
 -120.82              1.57375              
 -120.84              1.54931              
 -120.86              1.54233              
 -120.88              1.5488               
 -120.9               1.57017              
 -120.92              1.61769              
 -120.94              1.70139              
 -120.96              1.80711              
 -120.98              1.90623              
 -121.                1.98319              
 -121.02              2.06103              
 -121.04              2.16844              
 -121.06              2.30636              
 -121.08              2.44958              
 -121.1               2.57682              
 -121.12              2.69079              
 -121.14              2.80122              
 -121.16              2.90892              
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##END=
