##TITLE=              29Si MAS NMR spectrum of as-synthesized pure silica ITQ-12 with 1,3,4-trimethylimazolium
##JCAMP-DX=           5.01
##DATA TYPE=          NMR SPECTRUM
##DATA CLASS=         XYDATA
##ORIGIN=             Rojas et al. J. Am. Chem. Soc., 134, 2255-2263 (2012) Figure 3
##OWNER=              Digitized and processed by Brouwer Lab, Redeemer University College
##LONG DATE=          2019/08/08 14:42:16
##SOURCE REFERENCE=   ITW-29Si-Rojas-2012-asmade-134TMI
##DATA PROCESSING=    Spectrum digitized with WebPlotDigitizer and deconvoluted with Mathematica notebook

$$Sample information 
##NAMES=              ITW
##NAMES=              ITQ-12
##SAMPLE DESCRIPTION= ITQ-12, as-made, 134-TMI

$$Bibliographic information 
##$AUTHORS=           Rojas, A., Martinez-Morales, E., Zicovich-Wilson, C.M., Camblor, M.A.
##$TITLE=             Zeolite synthesis in fluoride media: Structure direction toward ITW by small methylimidazolium cations
##$JOURNAL=           Journal of the American Chemical Society
##$VOLUME=            134
##$PAGES=             2255-2263
##$YEAR=              2012
##$DOI=               10.1021/ja209832y
##$FIGURE=            Figure 3

$$Peak information    (Positions in ppm, Relative peak areas, Peak widths in ppm, Lorentzian/Gaussian shape parameter)
##$NUM PEAKS=         3
##$PEAK LABELS=        A          B          C         
##$PEAK TSITES=       
##$PEAK POSITIONS=    -115.891   -108.038   -107.828   
##$PEAK AREAS=         1.         1.         1.        
##$PEAK WIDTHS=        0.53829    0.57727    0.57727   
##$PEAK SHAPES=        0.40722    0.40722    0.40722   
##$NUMBERING REF=     
##$ASSIGN REF=        
##$ASSIGN METHOD=     
##$COMMENT=           

$$Spectrum acquisition information 
##.OBSERVE NUCLEUS=   ^29Si
##.OBSERVE FREQUENCY= 79.5
##.PULSE SEQUENCE=    single pulse
##.MAS FREQUENCY=     

$$Spectrum data information 
##XUNITS=             PPM
##YUNITS=             ARBITRARY UNITS
##FIRSTX=             -80.05                
##LASTX=              -149.8                
##XFACTOR=            1
##YFACTOR=            1
##NPOINTS=            1396
##FIRSTY=              0.00063              

$$Spectrum data
##XYDATA=             (X++(Y..Y))
 -80.05               0.00063              
 -80.1               -0.00141              
 -80.15              -0.00159              
 -80.2               -0.00153              
 -80.25              -0.00157              
 -80.3                0.00070              
 -80.35               0.00527              
 -80.4                0.00738              
 -80.45               0.00731              
 -80.5                0.00734              
 -80.55               0.00733              
 -80.6                0.00733              
 -80.65               0.00734              
 -80.7                0.00728              
 -80.75               0.00755              
 -80.8                0.00626              
 -80.85               0.00084              
 -80.9               -0.00190              
 -80.95              -0.00146              
 -81.                -0.00154              
 -81.05              -0.00167              
 -81.1               -0.00071              
 -81.15               0.00313              
 -81.2                0.00770              
 -81.25               0.01286              
 -81.3                0.01319              
 -81.35               0.00823              
 -81.4                0.00739              
 -81.45               0.00599              
 -81.5                0.00375              
 -81.55               0.00247              
 -81.6                0.00085              
 -81.65               0.00038              
 -81.7                0.00495              
 -81.75               0.00304              
 -81.8               -0.00155              
 -81.85              -0.00153              
 -81.9               -0.00151              
 -81.95               0.00114              
 -82.                 0.00525              
 -82.05               0.00203              
 -82.1               -0.00185              
 -82.15              -0.00152              
 -82.2               -0.00127              
 -82.25               0.00195              
 -82.3                0.00621              
 -82.35               0.00739              
 -82.4                0.00757              
 -82.45               0.00587              
 -82.5                0.00038              
 -82.55              -0.00187              
 -82.6               -0.00146              
 -82.65              -0.00157              
 -82.7               -0.00154              
 -82.75              -0.00154              
 -82.8               -0.00158              
 -82.85              -0.00144              
 -82.9               -0.00192              
 -82.95               0.00045              
 -83.                 0.00404              
 -83.05               0.00628              
 -83.1                0.00726              
 -83.15               0.00735              
 -83.2                0.00733              
 -83.25               0.00732              
 -83.3                0.00733              
 -83.35               0.00499              
 -83.4                0.00044              
 -83.45              -0.00165              
 -83.5               -0.00132              
 -83.55               0.00090              
 -83.6                0.00027              
 -83.65              -0.00178              
 -83.7               -0.00131              
 -83.75              -0.00245              
 -83.8               -0.00779              
 -83.85              -0.01076              
 -83.9               -0.01044              
 -83.95              -0.00989              
 -84.                -0.00619              
 -84.05              -0.00226              
 -84.1               -0.00156              
 -84.15              -0.00072              
 -84.2                0.00332              
 -84.25               0.00689              
 -84.3                0.00727              
 -84.35               0.00860              
 -84.4                0.01165              
 -84.45               0.01050              
 -84.5                0.00828              
 -84.55               0.00668              
 -84.6                0.00341              
 -84.65              -0.00128              
 -84.7               -0.00160              
 -84.75              -0.00154              
 -84.8               -0.00155              
 -84.85              -0.00153              
 -84.9                0.00088              
 -84.95               0.00543              
 -85.                 0.00740              
 -85.05               0.00731              
 -85.1                0.00734              
 -85.15               0.00733              
 -85.2                0.00733              
 -85.25               0.00735              
 -85.3                0.00725              
 -85.35               0.00777              
 -85.4                0.01123              
 -85.45               0.01533              
 -85.5                0.01626              
 -85.55               0.01651              
 -85.6                0.01436              
 -85.65               0.00886              
 -85.7                0.00704              
 -85.75               0.00740              
 -85.8                0.00731              
 -85.85               0.00734              
 -85.9                0.00732              
 -85.95               0.00736              
 -86.                 0.00726              
 -86.05               0.00755              
 -86.1                0.00919              
 -86.15               0.01350              
 -86.2                0.01620              
 -86.25               0.01419              
 -86.3                0.00963              
 -86.35               0.00504              
 -86.4                0.00049              
 -86.45              -0.00162              
 -86.5               -0.00142              
 -86.55               0.00126              
 -86.6                0.00575              
 -86.65               0.00744              
 -86.7                0.00727              
 -86.75               0.00744              
 -86.8                0.00682              
 -86.85               0.00428              
 -86.9                0.00209              
 -86.95              -0.00039              
 -87.                -0.00178              
 -87.05              -0.00133              
 -87.1               -0.00252              
 -87.15              -0.00503              
 -87.2               -0.00723              
 -87.25              -0.00971              
 -87.3               -0.01077              
 -87.35              -0.00898              
 -87.4               -0.00676              
 -87.45              -0.00290              
 -87.5                0.00122              
 -87.55               0.00302              
 -87.6                0.00061              
 -87.65              -0.00141              
 -87.7               -0.00159              
 -87.75              -0.00153              
 -87.8               -0.00158              
 -87.85               0.00068              
 -87.9                0.00300              
 -87.95               0.00787              
 -88.                 0.01422              
 -88.05               0.01104              
 -88.1                0.00702              
 -88.15               0.00755              
 -88.2                0.00663              
 -88.25               0.00132              
 -88.3               -0.00167              
 -88.35              -0.00252              
 -88.4               -0.00806              
 -88.45              -0.01075              
 -88.5               -0.01046              
 -88.55              -0.00979              
 -88.6               -0.00597              
 -88.65              -0.00217              
 -88.7               -0.00154              
 -88.75              -0.00070              
 -88.8                0.00389              
 -88.85               0.00430              
 -88.9               -0.00058              
 -88.95              -0.00175              
 -89.                -0.00145              
 -89.05              -0.00157              
 -89.1               -0.00154              
 -89.15              -0.00155              
 -89.2               -0.00155              
 -89.25              -0.00154              
 -89.3               -0.00156              
 -89.35              -0.00155              
 -89.4               -0.00387              
 -89.45              -0.00603              
 -89.5               -0.00612              
 -89.55              -0.00847              
 -89.6               -0.00768              
 -89.65              -0.00286              
 -89.7                0.00191              
 -89.75               0.00520              
 -89.8                0.00136              
 -89.85              -0.00193              
 -89.9               -0.00144              
 -89.95              -0.00158              
 -90.                -0.00154              
 -90.05              -0.00155              
 -90.1               -0.00155              
 -90.15              -0.00155              
 -90.2               -0.00155              
 -90.25              -0.00156              
 -90.3               -0.00151              
 -90.35              -0.00167              
 -90.4               -0.00033              
 -90.45               0.00397              
 -90.5                0.00661              
 -90.55               0.00750              
 -90.6                0.00715              
 -90.65               0.00552              
 -90.7               -0.00086              
 -90.75              -0.00579              
 -90.8               -0.00812              
 -90.85              -0.01043              
 -90.9               -0.00810              
 -90.95              -0.00354              
 -91.                -0.00149              
 -91.05              -0.00153              
 -91.1               -0.00175              
 -91.15              -0.00434              
 -91.2               -0.00605              
 -91.25              -0.00639              
 -91.3               -0.00870              
 -91.35              -0.00698              
 -91.4               -0.00256              
 -91.45              -0.00143              
 -91.5               -0.00158              
 -91.55              -0.00154              
 -91.6               -0.00155              
 -91.65              -0.00155              
 -91.7               -0.00155              
 -91.75              -0.00156              
 -91.8               -0.00152              
 -91.85              -0.00167              
 -91.9               -0.00039              
 -91.95               0.00407              
 -92.                 0.00593              
 -92.05               0.00563              
 -92.1                0.00367              
 -92.15               0.00101              
 -92.2               -0.00144              
 -92.25              -0.00157              
 -92.3               -0.00155              
 -92.35              -0.00155              
 -92.4               -0.00155              
 -92.45              -0.00154              
 -92.5               -0.00162              
 -92.55              -0.00426              
 -92.6               -0.00876              
 -92.65              -0.01057              
 -92.7               -0.01022              
 -92.75              -0.00697              
 -92.8               -0.00367              
 -92.85              -0.00761              
 -92.9               -0.01092              
 -92.95              -0.00981              
 -93.                -0.00650              
 -93.05              -0.00179              
 -93.1                0.00311              
 -93.15               0.00564              
 -93.2                0.00394              
 -93.25               0.00162              
 -93.3               -0.00088              
 -93.35              -0.00168              
 -93.4               -0.00151              
 -93.45              -0.00157              
 -93.5               -0.00150              
 -93.55              -0.00166              
 -93.6               -0.00122              
 -93.65               0.00042              
 -93.7                0.00256              
 -93.75               0.00684              
 -93.8                0.01175              
 -93.85               0.00744              
 -93.9                0.00284              
 -93.95               0.00055              
 -94.                -0.00162              
 -94.05              -0.00157              
 -94.1               -0.00132              
 -94.15               0.00093              
 -94.2                0.00021              
 -94.25              -0.00172              
 -94.3               -0.00160              
 -94.35              -0.00106              
 -94.4                0.00150              
 -94.45               0.00365              
 -94.5                0.00629              
 -94.55               0.00690              
 -94.6                0.00294              
 -94.65              -0.00084              
 -94.7               -0.00167              
 -94.75              -0.00151              
 -94.8               -0.00159              
 -94.85              -0.00142              
 -94.9               -0.00272              
 -94.95              -0.00694              
 -95.                -0.01029              
 -95.05              -0.00982              
 -95.1               -0.00867              
 -95.15              -0.00929              
 -95.2               -0.01036              
 -95.25              -0.01046              
 -95.3               -0.01044              
 -95.35              -0.01043              
 -95.4               -0.01043              
 -95.45              -0.00805              
 -95.5               -0.00349              
 -95.55              -0.00151              
 -95.6               -0.00144              
 -95.65               0.00140              
 -95.7                0.00579              
 -95.75               0.00761              
 -95.8                0.00649              
 -95.85               0.00120              
 -95.9               -0.00190              
 -95.95              -0.00145              
 -96.                -0.00157              
 -96.05              -0.00154              
 -96.1               -0.00156              
 -96.15              -0.00152              
 -96.2               -0.00165              
 -96.25              -0.00075              
 -96.3                0.00373              
 -96.35               0.00442              
 -96.4               -0.00044              
 -96.45              -0.00178              
 -96.5               -0.00149              
 -96.55              -0.00160              
 -96.6               -0.00144              
 -96.65               0.00094              
 -96.7                0.00471              
 -96.75               0.00722              
 -96.8                0.00746              
 -96.85               0.00306              
 -96.9               -0.00155              
 -96.95              -0.00153              
 -97.                -0.00156              
 -97.05              -0.00154              
 -97.1               -0.00155              
 -97.15              -0.00155              
 -97.2               -0.00155              
 -97.25              -0.00155              
 -97.3               -0.00155              
 -97.35              -0.00155              
 -97.4               -0.00155              
 -97.45              -0.00155              
 -97.5               -0.00155              
 -97.55              -0.00155              
 -97.6               -0.00155              
 -97.65              -0.00155              
 -97.7               -0.00155              
 -97.75              -0.00155              
 -97.8               -0.00155              
 -97.85              -0.00155              
 -97.9               -0.00156              
 -97.95              -0.00152              
 -98.                -0.00164              
 -98.05              -0.00100              
 -98.1                0.00065              
 -98.15               0.00371              
 -98.2                0.00520              
 -98.25               0.00116              
 -98.3               -0.00149              
 -98.35              -0.00158              
 -98.4                0.00064              
 -98.45               0.00521              
 -98.5                0.00737              
 -98.55               0.00731              
 -98.6                0.00734              
 -98.65               0.00733              
 -98.7                0.00733              
 -98.75               0.00733              
 -98.8                0.00733              
 -98.85               0.00733              
 -98.9                0.00733              
 -98.95               0.00733              
 -99.                 0.00732              
 -99.05               0.00735              
 -99.1                0.00725              
 -99.15               0.00765              
 -99.2                0.00544              
 -99.25              -0.00005              
 -99.3               -0.00180              
 -99.35              -0.00161              
 -99.4               -0.00046              
 -99.45               0.00378              
 -99.5                0.00702              
 -99.55               0.00745              
 -99.6                0.00729              
 -99.65               0.00735              
 -99.7                0.00734              
 -99.75               0.00727              
 -99.8                0.00922              
 -99.85               0.01390              
 -99.9                0.01183              
 -99.95               0.00729              
 -100.                0.00735              
 -100.05              0.00739              
 -100.1               0.01004              
 -100.15              0.01455              
 -100.2               0.01628              
 -100.25              0.01634              
 -100.3               0.01550              
 -100.35              0.01019              
 -100.4               0.00699              
 -100.45              0.00742              
 -100.5               0.00730              
 -100.55              0.00734              
 -100.6               0.00733              
 -100.65              0.00733              
 -100.7               0.00732              
 -100.75              0.00735              
 -100.8               0.00724              
 -100.85              0.00768              
 -100.9               0.00481              
 -100.95             -0.00057              
 -101.               -0.00175              
 -101.05             -0.00147              
 -101.1              -0.00155              
 -101.15             -0.00160              
 -101.2              -0.00161              
 -101.25              0.00023              
 -101.3               0.00477              
 -101.35              0.00729              
 -101.4               0.00733              
 -101.45              0.00733              
 -101.5               0.00733              
 -101.55              0.00735              
 -101.6               0.00723              
 -101.65              0.00451              
 -101.7               0.00003              
 -101.75             -0.00166              
 -101.8              -0.00152              
 -101.85             -0.00156              
 -101.9              -0.00152              
 -101.95             -0.00167              
 -102.               -0.00094              
 -102.05              0.00179              
 -102.1               0.00302              
 -102.15              0.00300              
 -102.2               0.00197              
 -102.25             -0.00071              
 -102.3              -0.00189              
 -102.35             -0.00027              
 -102.4               0.00200              
 -102.45              0.00551              
 -102.5               0.01223              
 -102.55              0.01627              
 -102.6               0.01497              
 -102.65              0.01230              
 -102.7               0.00952              
 -102.75              0.00747              
 -102.8               0.00729              
 -102.85              0.00734              
 -102.9               0.00733              
 -102.95              0.00733              
 -103.                0.00734              
 -103.05              0.00727              
 -103.1               0.00468              
 -103.15              0.00017              
 -103.2              -0.00168              
 -103.25             -0.00131              
 -103.3               0.00167              
 -103.35              0.00598              
 -103.4               0.00767              
 -103.45              0.00623              
 -103.5               0.00086              
 -103.55             -0.00190              
 -103.6              -0.00146              
 -103.65             -0.00157              
 -103.7              -0.00155              
 -103.75             -0.00154              
 -103.8              -0.00160              
 -103.85             -0.00136              
 -103.9              -0.00281              
 -103.95             -0.00533              
 -104.               -0.00739              
 -104.05             -0.01039              
 -104.1              -0.00861              
 -104.15             -0.00467              
 -104.2              -0.00011              
 -104.25              0.00463              
 -104.3               0.00726              
 -104.35              0.00738              
 -104.4               0.00523              
 -104.45              0.00066              
 -104.5              -0.00158              
 -104.55             -0.00148              
 -104.6               0.00106              
 -104.65              0.00559              
 -104.7               0.00743              
 -104.75              0.00727              
 -104.8               0.00750              
 -104.85              0.00655              
 -104.9               0.00124              
 -104.95             -0.00190              
 -105.               -0.00143              
 -105.05             -0.00166              
 -105.1              -0.00104              
 -105.15              0.00301              
 -105.2               0.00488              
 -105.25              0.00001              
 -105.3              -0.00079              
 -105.35              0.00213              
 -105.4               0.00420              
 -105.45              0.00678              
 -105.5               0.00744              
 -105.55              0.00731              
 -105.6               0.00732              
 -105.65              0.00742              
 -105.7               0.00980              
 -105.75              0.01356              
 -105.8               0.01614              
 -105.85              0.01623              
 -105.9               0.01622              
 -105.95              0.01622              
 -106.                0.01622              
 -106.05              0.01622              
 -106.1               0.01622              
 -106.15              0.01622              
 -106.2               0.01622              
 -106.25              0.01621              
 -106.3               0.01623              
 -106.35              0.01615              
 -106.4               0.01655              
 -106.45              0.01984              
 -106.5               0.02403              
 -106.55              0.02526              
 -106.6               0.02496              
 -106.65              0.02578              
 -106.7               0.02938              
 -106.75              0.03410              
 -106.8               0.03918              
 -106.85              0.05040              
 -106.9               0.06383              
 -106.95              0.07164              
 -107.                0.08093              
 -107.05              0.09895              
 -107.1               0.12737              
 -107.15              0.15473              
 -107.2               0.18934              
 -107.25              0.23799              
 -107.3               0.30609              
 -107.35              0.38866              
 -107.4               0.50357              
 -107.45              0.65191              
 -107.5               0.82879              
 -107.55              1.03389              
 -107.6               1.26062              
 -107.65              1.50631              
 -107.7               1.74524              
 -107.75              1.98724              
 -107.8               2.20712              
 -107.85              2.39183              
 -107.9               2.53123              
 -107.95              2.60656              
 -108.                2.53363              
 -108.05              2.34417              
 -108.1               2.1622               
 -108.15              1.94297              
 -108.2               1.61668              
 -108.25              1.29761              
 -108.3               1.03555              
 -108.35              0.80112              
 -108.4               0.61295              
 -108.45              0.47149              
 -108.5               0.35409              
 -108.55              0.27552              
 -108.6               0.21745              
 -108.65              0.17166              
 -108.7               0.14299              
 -108.75              0.11314              
 -108.8               0.09300              
 -108.85              0.08167              
 -108.9               0.07002              
 -108.95              0.06300              
 -109.                0.05612              
 -109.05              0.04929              
 -109.1               0.04477              
 -109.15              0.04014              
 -109.2               0.03563              
 -109.25              0.03067              
 -109.3               0.02388              
 -109.35              0.02003              
 -109.4               0.01775              
 -109.45              0.01602              
 -109.5               0.01627              
 -109.55              0.01620              
 -109.6               0.01624              
 -109.65              0.01613              
 -109.7               0.01654              
 -109.75              0.01436              
 -109.8               0.00903              
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##END=
