##TITLE=              29Si MAS NMR spectrum of as-synthesized pure silica ITQ-12 with 1,2,3-trimethylimazolium
##JCAMP-DX=           5.01
##DATA TYPE=          NMR SPECTRUM
##DATA CLASS=         XYDATA
##ORIGIN=             Rojas et al. J. Am. Chem. Soc., 134, 2255-2263 (2012) Figure 3
##OWNER=              Digitized and processed by Brouwer Lab, Redeemer University College
##LONG DATE=          2019/08/08 14:40:49
##SOURCE REFERENCE=   ITW-29Si-Rojas-2012-asmade-123TMI
##DATA PROCESSING=    Spectrum digitized with WebPlotDigitizer and deconvoluted with Mathematica notebook

$$Sample information 
##NAMES=              ITW
##NAMES=              ITQ-12
##SAMPLE DESCRIPTION= ITQ-12, as-made, 123-TMI

$$Bibliographic information 
##$AUTHORS=           Rojas, A., Martinez-Morales, E., Zicovich-Wilson, C.M., Camblor, M.A.
##$TITLE=             Zeolite synthesis in fluoride media: Structure direction toward ITW by small methylimidazolium cations
##$JOURNAL=           Journal of the American Chemical Society
##$VOLUME=            134
##$PAGES=             2255-2263
##$YEAR=              2012
##$DOI=               10.1021/ja209832y
##$FIGURE=            Figure 3

$$Peak information    (Positions in ppm, Relative peak areas, Peak widths in ppm, Lorentzian/Gaussian shape parameter)
##$NUM PEAKS=         6
##$PEAK LABELS=        A          B          C          D          E          F         
##$PEAK TSITES=       
##$PEAK POSITIONS=    -115.477   -110.217   -108.3     -107.603   -107.438   -106.485   
##$PEAK AREAS=         1.         1.         1.         1.         1.         1.        
##$PEAK WIDTHS=        0.55216    0.62309    0.40364    0.43177    0.43177    0.52951   
##$PEAK SHAPES=        1          1          1          1          1          1         
##$NUMBERING REF=     
##$ASSIGN REF=        
##$ASSIGN METHOD=     
##$COMMENT=           

$$Spectrum acquisition information 
##.OBSERVE NUCLEUS=   ^29Si
##.OBSERVE FREQUENCY= 79.5
##.PULSE SEQUENCE=    single pulse
##.MAS FREQUENCY=     

$$Spectrum data information 
##XUNITS=             PPM
##YUNITS=             ARBITRARY UNITS
##FIRSTX=             -80.05                
##LASTX=              -149.8                
##XFACTOR=            1
##YFACTOR=            1
##NPOINTS=            1396
##FIRSTY=              0.04089              

$$Spectrum data
##XYDATA=             (X++(Y..Y))
 -80.05               0.04089              
 -80.1                0.01803              
 -80.15              -0.01437              
 -80.2               -0.01572              
 -80.25              -0.01564              
 -80.3                0.00042              
 -80.35               0.03239              
 -80.4                0.06478              
 -80.45               0.09325              
 -80.5                0.07136              
 -80.55               0.04490              
 -80.6                0.04241              
 -80.65               0.00524              
 -80.7               -0.01785              
 -80.75              -0.01501              
 -80.8               -0.01560              
 -80.85              -0.01623              
 -80.9               -0.01172              
 -80.95               0.01372              
 -81.                 0.04086              
 -81.05               0.04691              
 -81.1                0.04589              
 -81.15               0.04615              
 -81.2                0.04608              
 -81.25               0.04610              
 -81.3                0.04608              
 -81.35               0.04617              
 -81.4                0.04585              
 -81.45               0.04708              
 -81.5                0.04299              
 -81.55               0.01541              
 -81.6               -0.01362              
 -81.65              -0.01615              
 -81.7               -0.01552              
 -81.75              -0.01558              
 -81.8               -0.01551              
 -81.85               0.00117              
 -81.9                0.03279              
 -81.95               0.04659              
 -82.                 0.04592              
 -82.05               0.04621              
 -82.1                0.04581              
 -82.15               0.04730              
 -82.2                0.04029              
 -82.25               0.00322              
 -82.3               -0.01806              
 -82.35              -0.01476              
 -82.4               -0.01649              
 -82.45              -0.01130              
 -82.5                0.01457              
 -82.55               0.04126              
 -82.6                0.04687              
 -82.65               0.04590              
 -82.7                0.04614              
 -82.75               0.04608              
 -82.8                0.0461               
 -82.85               0.04611              
 -82.9                0.04605              
 -82.95               0.04627              
 -83.                 0.04536              
 -83.05               0.02858              
 -83.1                0.00245              
 -83.15              -0.01506              
 -83.2               -0.01593              
 -83.25              -0.00079              
 -83.3                0.03092              
 -83.35               0.04630              
 -83.4                0.04599              
 -83.45               0.04618              
 -83.5                0.04584              
 -83.55               0.04731              
 -83.6                0.06748              
 -83.65               0.09837              
 -83.7                0.10720              
 -83.75               0.07955              
 -83.8                0.03275              
 -83.85               0.00907              
 -83.9               -0.00786              
 -83.95              -0.01334              
 -84.                 0.01690              
 -84.05               0.02854              
 -84.1               -0.00373              
 -84.15              -0.01784              
 -84.2               -0.01501              
 -84.25              -0.01583              
 -84.3               -0.01523              
 -84.35              -0.01682              
 -84.4               -0.00503              
 -84.45               0.00860              
 -84.5                0.01843              
 -84.55               0.02846              
 -84.6                0.03173              
 -84.65               0.00283              
 -84.7               -0.01520              
 -84.75              -0.01578              
 -84.8               -0.00010              
 -84.85               0.03162              
 -84.9                0.04642              
 -84.95               0.04597              
 -85.                 0.04618              
 -85.05               0.04587              
 -85.1                0.04706              
 -85.15               0.04148              
 -85.2                0.00494              
 -85.25              -0.01798              
 -85.3               -0.01479              
 -85.35              -0.01642              
 -85.4               -0.01193              
 -85.45               0.01304              
 -85.5                0.04054              
 -85.55               0.04694              
 -85.6                0.04584              
 -85.65               0.04632              
 -85.7                0.04543              
 -85.75               0.04853              
 -85.8                0.02804              
 -85.85              -0.00924              
 -85.9               -0.01690              
 -85.95              -0.01499              
 -86.                -0.01577              
 -86.05              -0.01555              
 -86.1               -0.01558              
 -86.15              -0.01563              
 -86.2               -0.01550              
 -86.25              -0.01580              
 -86.3               -0.00027              
 -86.35               0.03170              
 -86.4                0.06268              
 -86.45               0.05927              
 -86.5                0.02757              
 -86.55               0.01321              
 -86.6               -0.00377              
 -86.65              -0.01670              
 -86.7               -0.01527              
 -86.75              -0.01572              
 -86.8               -0.01541              
 -86.85              -0.01624              
 -86.9               -0.01207              
 -86.95               0.01288              
 -87.                 0.04023              
 -87.05               0.04775              
 -87.1                0.04047              
 -87.15               0.01330              
 -87.2               -0.01165              
 -87.25              -0.01715              
 -87.3               -0.00773              
 -87.35               0.02144              
 -87.4                0.04395              
 -87.45               0.04652              
 -87.5                0.04588              
 -87.55               0.04616              
 -87.6                0.04608              
 -87.65               0.04609              
 -87.7                0.04610              
 -87.75               0.04609              
 -87.8                0.04610              
 -87.85               0.04610              
 -87.9                0.04603              
 -87.95               0.04649              
 -88.                 0.04395              
 -88.05               0.00946              
 -88.1               -0.01870              
 -88.15              -0.03730              
 -88.2               -0.06598              
 -88.25              -0.05468              
 -88.3               -0.02083              
 -88.35               0.01128              
 -88.4                0.03899              
 -88.45               0.04704              
 -88.5                0.04585              
 -88.55               0.04616              
 -88.6                0.04608              
 -88.65               0.04610              
 -88.7                0.04609              
 -88.75               0.04610              
 -88.8                0.04610              
 -88.85               0.04610              
 -88.9                0.04610              
 -88.95               0.04609              
 -89.                 0.04611              
 -89.05               0.04606              
 -89.1                0.04618              
 -89.15               0.04617              
 -89.2                0.04580              
 -89.25               0.06000              
 -89.3                0.09218              
 -89.35               0.07653              
 -89.4                0.06178              
 -89.45               0.07771              
 -89.5                0.07687              
 -89.55               0.07597              
 -89.6                0.05672              
 -89.65               0.02346              
 -89.7               -0.00579              
 -89.75              -0.01632              
 -89.8               -0.01616              
 -89.85              -0.01164              
 -89.9                0.00612              
 -89.95               0.02123              
 -90.                 0.03871              
 -90.05               0.04734              
 -90.1                0.04577              
 -90.15               0.04619              
 -90.2                0.04603              
 -90.25               0.04628              
 -90.3                0.04544              
 -90.35               0.04849              
 -90.4                0.02634              
 -90.45              -0.01040              
 -90.5               -0.01798              
 -90.55              -0.01424              
 -90.6                0.00179              
 -90.65               0.02805              
 -90.7                0.04537              
 -90.75               0.04690              
 -90.8                0.01619              
 -90.85              -0.01572              
 -90.9               -0.01551              
 -90.95              -0.01522              
 -91.                 0.00287              
 -91.05               0.03419              
 -91.1                0.04676              
 -91.15               0.04590              
 -91.2                0.04614              
 -91.25               0.04611              
 -91.3                0.04595              
 -91.35               0.04670              
 -91.4                0.04283              
 -91.45               0.01828              
 -91.5               -0.00940              
 -91.55              -0.01725              
 -91.6               -0.01028              
 -91.65               0.01652              
 -91.7                0.04188              
 -91.75               0.04768              
 -91.8                0.03860              
 -91.85               0.00970              
 -91.9               -0.01325              
 -91.95              -0.01601              
 -92.                -0.01558              
 -92.05              -0.01489              
 -92.1                0.00158              
 -92.15               0.02772              
 -92.2                0.04619              
 -92.25               0.03203              
 -92.3                0.01541              
 -92.35               0.01523              
 -92.4               -0.00087              
 -92.45              -0.01603              
 -92.5               -0.01540              
 -92.55              -0.01583              
 -92.6               -0.01465              
 -92.65               0.00657              
 -92.7                0.03166              
 -92.75               0.00578              
 -92.8               -0.01817              
 -92.85              -0.01489              
 -92.9               -0.01577              
 -92.95              -0.01559              
 -93.                -0.01541              
 -93.05              -0.01638              
 -93.1               -0.01059              
 -93.15               0.01631              
 -93.2                0.04193              
 -93.25               0.04709              
 -93.3                0.04486              
 -93.35               0.05457              
 -93.4                0.07589              
 -93.45               0.05790              
 -93.5                0.02271              
 -93.55              -0.00095              
 -93.6               -0.00576              
 -93.65              -0.00185              
 -93.7                0.02757              
 -93.75               0.04572              
 -93.8                0.04614              
 -93.85               0.04610              
 -93.9                0.04622              
 -93.95               0.06344              
 -94.                 0.09344              
 -94.05               0.07131              
 -94.1                0.02602              
 -94.15               0.01310              
 -94.2               -0.00477              
 -94.25              -0.01508              
 -94.3                0.01027              
 -94.35               0.03099              
 -94.4                0.00247              
 -94.45              -0.01826              
 -94.5               -0.01494              
 -94.55              -0.01557              
 -94.6               -0.01637              
 -94.65              -0.01019              
 -94.7                0.01716              
 -94.75               0.04236              
 -94.8                0.04676              
 -94.85               0.04593              
 -94.9                0.04613              
 -94.95               0.04609              
 -95.                 0.04608              
 -95.05               0.04615              
 -95.1                0.04595              
 -95.15               0.04649              
 -95.2                0.04641              
 -95.25               0.04486              
 -95.3                0.07581              
 -95.35               0.07721              
 -95.4                0.04560              
 -95.45               0.02941              
 -95.5               -0.00249              
 -95.55              -0.01623              
 -95.6               -0.01461              
 -95.65               0.00604              
 -95.7                0.03172              
 -95.75               0.00623              
 -95.8               -0.01799              
 -95.85              -0.01551              
 -95.9               -0.01259              
 -95.95               0.01087              
 -96.                 0.04364              
 -96.05               0.07620              
 -96.1                0.10248              
 -96.15               0.10805              
 -96.2                0.10995              
 -96.25               0.09266              
 -96.3                0.05472              
 -96.35               0.04440              
 -96.4                0.04651              
 -96.45               0.04600              
 -96.5                0.04612              
 -96.55               0.04610              
 -96.6                0.04607              
 -96.65               0.04618              
 -96.7                0.04617              
 -96.75               0.04582              
 -96.8                0.04677              
 -96.85               0.01595              
 -96.9               -0.01581              
 -96.95              -0.01540              
 -97.                -0.01586              
 -97.05              -0.01449              
 -97.1                0.00215              
 -97.15               0.01886              
 -97.2                0.05718              
 -97.25               0.09445              
 -97.3                0.06679              
 -97.35               0.04317              
 -97.4                0.04847              
 -97.45               0.03738              
 -97.5               -0.00029              
 -97.55              -0.01782              
 -97.6               -0.01563              
 -97.65              -0.01114              
 -97.7                0.01904              
 -97.75               0.02756              
 -97.8               -0.00737              
 -97.85              -0.00852              
 -97.9                0.01105              
 -97.95               0.02572              
 -98.                 0.04331              
 -98.05               0.04752              
 -98.1                0.04516              
 -98.15               0.04799              
 -98.2                0.05952              
 -98.25               0.08937              
 -98.3                0.12155              
 -98.35               0.13885              
 -98.4                0.10748              
 -98.45               0.07609              
 -98.5                0.06030              
 -98.55               0.04542              
 -98.6                0.04608              
 -98.65               0.04731              
 -98.7                0.06711              
 -98.75               0.10013              
 -98.8                0.13069              
 -98.85               0.13292              
 -98.9                0.09541              
 -98.95               0.07041              
 -99.                 0.05448              
 -99.05               0.04479              
 -99.1                0.04624              
 -99.15               0.04683              
 -99.2                0.04052              
 -99.25               0.01284              
 -99.3               -0.01179              
 -99.35              -0.01713              
 -99.4               -0.00751              
 -99.45               0.02185              
 -99.5                0.04402              
 -99.55               0.04713              
 -99.6                0.04532              
 -99.65               0.04779              
 -99.7                0.05929              
 -99.75               0.08964              
 -99.8                0.10742              
 -99.85               0.10784              
 -99.9                0.10780              
 -99.95               0.10779              
 -100.                0.10783              
 -100.05              0.10761              
 -100.1               0.10880              
 -100.15              0.12727              
 -100.2               0.13571              
 -100.25              0.09903              
 -100.3               0.07217              
 -100.35              0.05595              
 -100.4               0.04708              
 -100.45              0.07469              
 -100.5               0.09191              
 -100.55              0.06157              
 -100.6               0.04372              
 -100.65              0.04594              
 -100.7               0.05144              
 -100.75              0.07911              
 -100.8               0.10413              
 -100.85              0.10846              
 -100.9               0.10763              
 -100.95              0.10784              
 -101.                0.10779              
 -101.05              0.10780              
 -101.1               0.1078               
 -101.15              0.10780              
 -101.2               0.10780              
 -101.25              0.10780              
 -101.3               0.10779              
 -101.35              0.10780              
 -101.4               0.10779              
 -101.45              0.10776              
 -101.5               0.10808              
 -101.55              0.12626              
 -101.6               0.15501              
 -101.65              0.13330              
 -101.7               0.10433              
 -101.75              0.08639              
 -101.8               0.05523              
 -101.85              0.04525              
 -101.9               0.04647              
 -101.95              0.04539              
 -102.                0.04963              
 -102.05              0.07447              
 -102.1               0.10217              
 -102.15              0.10844              
 -102.2               0.10834              
 -102.25              0.10227              
 -102.3               0.07260              
 -102.35              0.05823              
 -102.4               0.07061              
 -102.45              0.09520              
 -102.5               0.14443              
 -102.55              0.14932              
 -102.6               0.10540              
 -102.65              0.06497              
 -102.7               0.03610              
 -102.75              0.00277              
 -102.8              -0.01574              
 -102.85             -0.00132              
 -102.9               0.03029              
 -102.95              0.06220              
 -103.                0.09371              
 -103.05              0.10822              
 -103.1               0.10765              
 -103.15              0.10783              
 -103.2               0.10785              
 -103.25              0.10752              
 -103.3               0.10902              
 -103.35              0.10187              
 -103.4               0.06473              
 -103.45              0.04367              
 -103.5               0.04675              
 -103.55              0.04592              
 -103.6               0.04614              
 -103.65              0.04609              
 -103.7               0.04608              
 -103.75              0.04616              
 -103.8               0.04586              
 -103.85              0.04697              
 -103.9               0.03860              
 -103.95              0.00906              
 -104.               -0.01264              
 -104.05             -0.01857              
 -104.1              -0.00099              
 -104.15              0.02363              
 -104.2               0.03899              
 -104.25              0.04568              
 -104.3               0.04629              
 -104.35              0.04588              
 -104.4               0.06096              
 -104.45              0.09254              
 -104.5               0.07531              
 -104.55              0.04503              
 -104.6               0.04630              
 -104.65              0.04694              
 -104.7               0.06672              
 -104.75              0.09750              
 -104.8               0.10860              
 -104.85              0.10757              
 -104.9               0.10786              
 -104.95              0.10778              
 -105.                0.10778              
 -105.05              0.10787              
 -105.1               0.10750              
 -105.15              0.10897              
 -105.2               0.10116              
 -105.25              0.08351              
 -105.3               0.06873              
 -105.35              0.04981              
 -105.4               0.05288              
 -105.45              0.08187              
 -105.5               0.11483              
 -105.55              0.14443              
 -105.6               0.17874              
 -105.65              0.20956              
 -105.7               0.22383              
 -105.75              0.23075              
 -105.8               0.23130              
 -105.85              0.23126              
 -105.9               0.23105              
 -105.95              0.24680              
 -106.                0.27909              
 -106.05              0.32749              
 -106.1               0.39462              
 -106.15              0.51169              
 -106.2               0.65726              
 -106.25              0.79655              
 -106.3               0.92836              
 -106.35              1.09344              
 -106.4               1.24047              
 -106.45              1.34112              
 -106.5               1.36257              
 -106.55              1.2676               
 -106.6               1.16045              
 -106.65              1.06861              
 -106.7               0.96383              
 -106.75              0.85667              
 -106.8               0.77843              
 -106.85              0.73276              
 -106.9               0.72348              
 -106.95              0.72447              
 -107.                0.73261              
 -107.05              0.78412              
 -107.1               0.91213              
 -107.15              1.04231              
 -107.2               1.20387              
 -107.25              1.43485              
 -107.3               1.75656              
 -107.35              2.10807              
 -107.4               2.36911              
 -107.45              2.5606               
 -107.5               2.79671              
 -107.55              2.782                
 -107.6               2.57142              
 -107.65              2.37742              
 -107.7               2.09125              
 -107.75              1.75963              
 -107.8               1.48428              
 -107.85              1.25947              
 -107.9               1.10264              
 -107.95              1.01167              
 -108.                1.02311              
 -108.05              1.15478              
 -108.1               1.31064              
 -108.15              1.45569              
 -108.2               1.63014              
 -108.25              1.77471              
 -108.3               1.80435              
 -108.35              1.69011              
 -108.4               1.50562              
 -108.45              1.29346              
 -108.5               1.06543              
 -108.55              0.85902              
 -108.6               0.68601              
 -108.65              0.55447              
 -108.7               0.45982              
 -108.75              0.36400              
 -108.8               0.32405              
 -108.85              0.31052              
 -108.9               0.26414              
 -108.95              0.21595              
 -109.                0.20004              
 -109.05              0.18382              
 -109.1               0.16879              
 -109.15              0.17035              
 -109.2               0.19015              
 -109.25              0.21687              
 -109.3               0.19233              
 -109.35              0.16720              
 -109.4               0.16956              
 -109.45              0.17241              
 -109.5               0.19414              
 -109.55              0.23280              
 -109.6               0.28207              
 -109.65              0.32905              
 -109.7               0.37879              
 -109.75              0.41723              
 -109.8               0.45507              
 -109.85              0.51264              
 -109.9               0.58605              
 -109.95              0.67535              
 -110.                0.78395              
 -110.05              0.88690              
 -110.1               0.96662              
 -110.15              1.03683              
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##END=
