##TITLE=              31P MAS NMR spectrum of as-made AlPO-16 (cubic phase with quinuclidine template)
##JCAMP-DX=           5.01
##DATA TYPE=          NMR SPECTRUM
##DATA CLASS=         XYDATA
##ORIGIN=             Schott-Darie et al. Microporous Mater., 6513, 123-132 (1994) Figure 7a
##OWNER=              Digitized and processed by Brouwer Lab, Redeemer University
##LONG DATE=          2020/07/17 11:35:45
##SOURCE REFERENCE=   AST-31P-Schott-Darie-1994-asmade
##DATA PROCESSING=    Spectrum digitized with WebPlotDigitizer and deconvoluted with Mathematica notebook

$$Sample information 
##NAMES=              AST
##NAMES=              AlPO-16
##SAMPLE DESCRIPTION= AlPO-16, as-made

$$Bibliographic information 
##$AUTHORS=           Schott-Darie, C., Patarin, J., Goff, P.L.
##$TITLE=             Synthesis, characterization and Rietveld refinement of the tetragonal variant of AlPO4-16 prepared in fluoride medium
##$JOURNAL=           Microporous Materials
##$VOLUME=            6513
##$PAGES=             123-132
##$YEAR=              1994
##$DOI=               10.1016/0927-6513(94)00014-X
##$FIGURE=            Figure 7a

$$Peak information    (Positions in ppm, Relative peak areas, Peak widths in ppm, Lorentzian/Gaussian shape parameter)
##$NUM PEAKS=         2
##$PEAK LABELS=        P1         P2        
##$PEAK TSITES=        T1         T2        
##$PEAK POSITIONS=    -29.0269   -18.3509   
##$PEAK AREAS=         3.99999    1.        
##$PEAK WIDTHS=        7.36787    5.19088   
##$PEAK SHAPES=        1          1         
##$NUMBERING REF=     Michael Bennett and Kirchner. Zeolites, 11, 502-506 (1991)
##$ASSIGN REF=        Schott-Darie et al. Microporous Mater., 6513, 123-132 (1994) Figure 7a
##$ASSIGN METHOD=     relative intensities
##$COMMENT=           Peak assignments based on relative peak areas

$$Spectrum acquisition information 
##.OBSERVE NUCLEUS=   ^31P
##.OBSERVE FREQUENCY= 121.51
##.PULSE SEQUENCE=    single pulse
##.MAS FREQUENCY=     8000

$$Spectrum data information 
##XUNITS=             PPM
##YUNITS=             ARBITRARY UNITS
##FIRSTX=              16.6                 
##LASTX=              -58.6                 
##XFACTOR=            1
##YFACTOR=            1
##NPOINTS=            377
##FIRSTY=              0.00689              

$$Spectrum data
##XYDATA=             (X++(Y..Y))
  16.6                0.00689              
  16.4                0.00662              
  16.2                0.00666              
  16.                 0.00682              
  15.8                0.00698              
  15.6                0.00651              
  15.4                0.00589              
  15.2                0.00583              
  15.                 0.00585              
  14.8                0.00612              
  14.6                0.00657              
  14.4                0.00675              
  14.2                0.00623              
  14.                 0.00506              
  13.8                0.00395              
  13.6                0.00351              
  13.4                0.00353              
  13.2                0.00422              
  13.                 0.00490              
  12.8                0.00536              
  12.6                0.00582              
  12.4                0.00584              
  12.2                0.00583              
  12.                 0.00583              
  11.8                0.00584              
  11.6                0.00573              
  11.4                0.00555              
  11.2                0.00483              
  11.                 0.00386              
  10.8                0.00346              
  10.6                0.00302              
  10.4                0.00289              
  10.2                0.00338              
  10.                 0.00352              
  9.8                 0.00336              
  9.6                 0.00309              
  9.4                 0.00279              
  9.2                 0.00288              
  9.                  0.00305              
  8.8                 0.00278              
  8.6                 0.00291              
  8.4                 0.00379              
  8.2                 0.00480              
  8.                  0.00558              
  7.8                 0.00623              
  7.6                 0.00628              
  7.4                 0.00593              
  7.2                 0.00583              
  7.                  0.00584              
  6.8                 0.00608              
  6.6                 0.00665              
  6.4                 0.00734              
  6.2                 0.00802              
  6.                  0.00871              
  5.8                 0.00897              
  5.6                 0.00853              
  5.4                 0.00816              
  5.2                 0.00816              
  5.                  0.00776              
  4.8                 0.00705              
  4.6                 0.00678              
  4.4                 0.00648              
  4.2                 0.00601              
  4.                  0.00584              
  3.8                 0.00583              
  3.6                 0.00591              
  3.4                 0.00631              
  3.2                 0.00692              
  3.                  0.00776              
  2.8                 0.00811              
  2.6                 0.00740              
  2.4                 0.00677              
  2.2                 0.00632              
  2.                  0.00590              
  1.8                 0.00585              
  1.6                 0.00614              
  1.4                 0.00686              
  1.2                 0.00751              
  1.                  0.00783              
  0.8                 0.00804              
  0.6                 0.00818              
  0.4                 0.00900              
  0.2                 0.00929              
  0.00000             0.00848              
 -0.2                 0.00815              
 -0.4                 0.00883              
 -0.6                 0.00976              
 -0.8                 0.00999              
 -1.                  0.01043              
 -1.2                 0.01101              
 -1.4                 0.01137              
 -1.6                 0.01141              
 -1.8                 0.01107              
 -2.                  0.01111              
 -2.2                 0.01156              
 -2.4                 0.01184              
 -2.6                 0.01183              
 -2.8                 0.01225              
 -3.                  0.01345              
 -3.2                 0.01465              
 -3.4                 0.01509              
 -3.6                 0.01486              
 -3.8                 0.01422              
 -4.                  0.01402              
 -4.2                 0.01495              
 -4.4                 0.01605              
 -4.6                 0.01773              
 -4.8                 0.01919              
 -5.                  0.01980              
 -5.2                 0.02053              
 -5.4                 0.02161              
 -5.6                 0.02313              
 -5.8                 0.02470              
 -6.                  0.02567              
 -6.2                 0.02625              
 -6.4                 0.02715              
 -6.6                 0.02698              
 -6.8                 0.02607              
 -7.                  0.02573              
 -7.2                 0.02573              
 -7.4                 0.02573              
 -7.6                 0.02628              
 -7.8                 0.02719              
 -8.                  0.02799              
 -8.2                 0.02888              
 -8.4                 0.03001              
 -8.6                 0.03097              
 -8.8                 0.03170              
 -9.                  0.03350              
 -9.2                 0.03564              
 -9.4                 0.03684              
 -9.6                 0.03727              
 -9.8                 0.03739              
 -10.                 0.03812              
 -10.2                0.04012              
 -10.4                0.04191              
 -10.6                0.04288              
 -10.8                0.04336              
 -11.                 0.04475              
 -11.2                0.04718              
 -11.4                0.04958              
 -11.6                0.05156              
 -11.8                0.05425              
 -12.                 0.05651              
 -12.2                0.05779              
 -12.4                0.05851              
 -12.6                0.05845              
 -12.8                0.05825              
 -13.                 0.05875              
 -13.2                0.05955              
 -13.4                0.06059              
 -13.6                0.06255              
 -13.8                0.06506              
 -14.                 0.06735              
 -14.2                0.06872              
 -14.4                0.07115              
 -14.6                0.07550              
 -14.8                0.08067              
 -15.                 0.08463              
 -15.2                0.08860              
 -15.4                0.09453              
 -15.6                0.10160              
 -15.8                0.10786              
 -16.                 0.11278              
 -16.2                0.11869              
 -16.4                0.12537              
 -16.6                0.13176              
 -16.8                0.13564              
 -17.                 0.1401               
 -17.2                0.14653              
 -17.4                0.15252              
 -17.6                0.15723              
 -17.8                0.15929              
 -18.                 0.16052              
 -18.2                0.16151              
 -18.4                0.16141              
 -18.6                0.16096              
 -18.8                0.15915              
 -19.                 0.15609              
 -19.2                0.15262              
 -19.4                0.14904              
 -19.6                0.14672              
 -19.8                0.14441              
 -20.                 0.14154              
 -20.2                0.13834              
 -20.4                0.13574              
 -20.6                0.13403              
 -20.8                0.13197              
 -21.                 0.13091              
 -21.2                0.13078              
 -21.4                0.13086              
 -21.6                0.13181              
 -21.8                0.13352              
 -22.                 0.13462              
 -22.2                0.13557              
 -22.4                0.13725              
 -22.6                0.13864              
 -22.8                0.14040              
 -23.                 0.14209              
 -23.2                0.14327              
 -23.4                0.14537              
 -23.6                0.14844              
 -23.8                0.15163              
 -24.                 0.15433              
 -24.2                0.15872              
 -24.4                0.16506              
 -24.6                0.17175              
 -24.8                0.17696              
 -25.                 0.18056              
 -25.2                0.18708              
 -25.4                0.19645              
 -25.6                0.20492              
 -25.8                0.21016              
 -26.                 0.21696              
 -26.2                0.22535              
 -26.4                0.23563              
 -26.6                0.24387              
 -26.8                0.25046              
 -27.                 0.26230              
 -27.2                0.27402              
 -27.4                0.28476              
 -27.6                0.29184              
 -27.8                0.30116              
 -28.                 0.31344              
 -28.2                0.32430              
 -28.4                0.33314              
 -28.6                0.34019              
 -28.8                0.34852              
 -29.                 0.35428              
 -29.2                0.35627              
 -29.4                0.35485              
 -29.6                0.35150              
 -29.8                0.34577              
 -30.                 0.33709              
 -30.2                0.33128              
 -30.4                0.32247              
 -30.6                0.30857              
 -30.8                0.29264              
 -31.                 0.27821              
 -31.2                0.26848              
 -31.4                0.25311              
 -31.6                0.23579              
 -31.8                0.22096              
 -32.                 0.20983              
 -32.2                0.20184              
 -32.4                0.18794              
 -32.6                0.17231              
 -32.8                0.15962              
 -33.                 0.15061              
 -33.2                0.14083              
 -33.4                0.12999              
 -33.6                0.11851              
 -33.8                0.11011              
 -34.                 0.10488              
 -34.2                0.09942              
 -34.4                0.09325              
 -34.6                0.08839              
 -34.8                0.08458              
 -35.                 0.07841              
 -35.2                0.07274              
 -35.4                0.06762              
 -35.6                0.06399              
 -35.8                0.06004              
 -36.                 0.05531              
 -36.2                0.05178              
 -36.4                0.04916              
 -36.6                0.04696              
 -36.8                0.04282              
 -37.                 0.03877              
 -37.2                0.03558              
 -37.4                0.03406              
 -37.6                0.03259              
 -37.8                0.03026              
 -38.                 0.02745              
 -38.2                0.02470              
 -38.4                0.02261              
 -38.6                0.02071              
 -38.8                0.01918              
 -39.                 0.01808              
 -39.2                0.01705              
 -39.4                0.01604              
 -39.6                0.01527              
 -39.8                0.01484              
 -40.                 0.01449              
 -40.2                0.01366              
 -40.4                0.01240              
 -40.6                0.01162              
 -40.8                0.01116              
 -41.                 0.01093              
 -41.2                0.01049              
 -41.4                0.00959              
 -41.6                0.00856              
 -41.8                0.00794              
 -42.                 0.00801              
 -42.2                0.00817              
 -42.4                0.00767              
 -42.6                0.00695              
 -42.8                0.00682              
 -43                  0.00744              
 -43.2                0.00808              
 -43.4                0.00819              
 -43.6                0.00817              
 -43.8                0.00941              
 -44.                 0.01000              
 -44.2                0.00966              
 -44.4                0.00921              
 -44.6                0.00912              
 -44.8                0.00966              
 -45.                 0.01021              
 -45.2                0.01064              
 -45.4                0.01081              
 -45.6                0.01032              
 -45.8                0.00873              
 -46.                 0.00708              
 -46.2                0.00625              
 -46.4                0.00565              
 -46.6                0.00450              
 -46.8                0.00437              
 -47.                 0.00564              
 -47.2                0.00619              
 -47.4                0.00630              
 -47.6                0.00630              
 -47.8                0.00630              
 -48.                 0.00630              
 -48.2                0.00630              
 -48.4                0.00628              
 -48.6                0.00680              
 -48.8                0.00772              
 -49.                 0.00817              
 -49.2                0.00748              
 -49.4                0.00650              
 -49.6                0.00628              
 -49.8                0.00639              
 -50.                 0.00656              
 -50.2                0.00726              
 -50.4                0.00816              
 -50.6                0.00815              
 -50.8                0.00807              
 -51.                 0.00737              
 -51.2                0.00664              
 -51.4                0.00638              
 -51.6                0.00629              
 -51.8                0.00630              
 -52.                 0.00630              
 -52.2                0.00630              
 -52.4                0.00630              
 -52.6                0.00630              
 -52.8                0.00630              
 -53.                 0.00643              
 -53.2                0.00666              
 -53.4                0.00676              
 -53.6                0.00664              
 -53.8                0.00640              
 -54.                 0.00582              
 -54.2                0.00491              
 -54.4                0.00456              
 -54.6                0.00523              
 -54.8                0.00593              
 -55.                 0.00618              
 -55.2                0.00629              
 -55.4                0.00650              
 -55.6                0.00675              
 -55.8                0.00684              
 -56.                 0.00746              
 -56.2                0.00818              
 -56.4                0.00862              
 -56.6                0.00943              
 -56.8                0.00944              
 -57.                 0.00856              
 -57.2                0.00766              
 -57.4                0.00660              
 -57.6                0.00640              
 -57.8                0.00627              
 -58.                 0.00657              
 -58.2                0.00790              
 -58.4                0.00943              
 -58.6                0.01019              
##END=
