##TITLE=              31P MAS NMR spectrum of AlPO-D (formed by calcination of AlPO-CJ3)
##JCAMP-DX=           5.01
##DATA TYPE=          NMR SPECTRUM
##DATA CLASS=         XYDATA
##ORIGIN=             Wang et al. Microporous Mesoporous Mater., 39, 281-289 (2000) Figure 7b
##OWNER=              Digitized and processed by Brouwer Lab, Redeemer University
##LONG DATE=          2020/07/17 06:46:10
##SOURCE REFERENCE=   APD-31P-Wang-2000-calcined
##DATA PROCESSING=    Spectrum digitized with WebPlotDigitizer and deconvoluted with Mathematica notebook

$$Sample information 
##NAMES=              APD
##NAMES=              AlPO-D
##NAMES=              AlPO-CJ3
##SAMPLE DESCRIPTION= AlPO-D, calcined

$$Bibliographic information 
##$AUTHORS=           Wang, K., Yu, J., Zhu, G., Zou, Y., Xu, R.
##$TITLE=             Synthesis and characterization of a new microporous aluminophosphate [Al2P2O8][OCH2CH2NH3] with an open-framework analogous to AlPO4-D
##$JOURNAL=           Microporous and Mesoporous Materials
##$VOLUME=            39
##$PAGES=             281-289
##$YEAR=              2000
##$DOI=               10.1016/S1387-1811(00)00207-9
##$FIGURE=            Figure 7b

$$Peak information    (Positions in ppm, Relative peak areas, Peak widths in ppm, Lorentzian/Gaussian shape parameter)
##$NUM PEAKS=         4
##$PEAK LABELS=        A          B          C          D         
##$PEAK TSITES=       
##$PEAK POSITIONS=    -32.6219   -32.4219   -32.2219   -30.7558   
##$PEAK AREAS=         1.         1.         1.         1.        
##$PEAK WIDTHS=        4.26041    4.26041    4.26041    4.26041   
##$PEAK SHAPES=        0.03967    0.03967    0.03967    0.03967   
##$NUMBERING REF=     Keller et al. Solid State Ionics, 43, 93-102 (1990)
##$ASSIGN REF=        
##$ASSIGN METHOD=     
##$COMMENT=           Peak assignments are not available

$$Spectrum acquisition information 
##.OBSERVE NUCLEUS=   ^31P
##.OBSERVE FREQUENCY= 161.9
##.PULSE SEQUENCE=    single pulse
##.MAS FREQUENCY=     3000

$$Spectrum data information 
##XUNITS=             PPM
##YUNITS=             ARBITRARY UNITS
##FIRSTX=              27.2                 
##LASTX=              -109.6                
##XFACTOR=            1
##YFACTOR=            1
##NPOINTS=            343
##FIRSTY=             -0.00103              

$$Spectrum data
##XYDATA=             (X++(Y..Y))
  27.2               -0.00103              
  26.8               -0.00103              
  26.4               -0.00103              
  26.                -0.00103              
  25.6               -0.00103              
  25.2               -0.00103              
  24.8               -0.00104              
  24.4               -0.00101              
  24.                -0.00112              
  23.6               -0.00026              
  23.2               -0.00004              
  22.8               -0.00115              
  22.4               -0.00190              
  22.                -0.00199              
  21.6               -0.00197              
  21.2               -0.00197              
  20.8               -0.00197              
  20.4               -0.00198              
  20.                -0.00196              
  19.6               -0.00202              
  19.2               -0.00153              
  18.8               -0.00091              
  18.4               -0.00098              
  18.                -0.00105              
  17.6               -0.00103              
  17.2               -0.00104              
  16.8               -0.00103              
  16.4               -0.00104              
  16.                -0.00102              
  15.6               -0.00108              
  15.2               -0.00055              
  14.8                0.00048              
  14.4                0.00081              
  14.                 0.00092              
  13.6                0.00000              
  13.2               -0.00032              
  12.8               -0.00002              
  12.4               -0.00078              
  12.                -0.00112              
  11.6               -0.00056              
  11.2                0.00035              
  10.8                0.00086              
  10.4                0.00050              
  10.                 0.00029              
  9.6                 0.00075              
  9.2                 0.00075              
  8.8                 0.00028              
  8.4                -0.00007              
  8.                 -0.00010              
  7.6                -0.00010              
  7.2                -0.00008              
  6.8                -0.00015              
  6.4                 0.00064              
  6.                  0.00224              
  5.6                 0.00457              
  5.2                 0.00622              
  4.8                 0.00718              
  4.4                 0.00806              
  4.                  0.00700              
  3.6                 0.00533              
  3.2                 0.00256              
  2.8                -0.00030              
  2.4                -0.00105              
  2.                 -0.00103              
  1.6                -0.00104              
  1.2                -0.00103              
  0.8                -0.00103              
  0.4                -0.00105              
  0.00000            -0.00092              
 -0.4                -0.00073              
 -0.8                -0.00069              
 -1.2                -0.00014              
 -1.6                 0.00068              
 -2.                  0.00087              
 -2.4                 0.00066              
 -2.8                -0.00044              
 -3.2                -0.00063              
 -3.6                 0.00025              
 -4.                  0.00079              
 -4.4                 0.00084              
 -4.8                 0.00083              
 -5.2                 0.00083              
 -5.6                 0.00084              
 -6.                  0.00076              
 -6.4                 0.00036              
 -6.8                -0.00019              
 -7.2                -0.00151              
 -7.6                -0.00289              
 -8.                 -0.00386              
 -8.4                -0.00605              
 -8.8                -0.00874              
 -9.2                -0.01030              
 -9.6                -0.01141              
 -10.                -0.01132              
 -10.4               -0.01008              
 -10.8               -0.00790              
 -11.2               -0.00438              
 -11.6                0.00196              
 -12.                 0.01039              
 -12.4                0.01769              
 -12.8                0.02308              
 -13.2                0.02728              
 -13.6                0.02860              
 -14.                 0.02641              
 -14.4                0.02237              
 -14.8                0.01449              
 -15.2                0.00698              
 -15.6                0.00210              
 -16.                -0.00155              
 -16.4               -0.00502              
 -16.8               -0.00900              
 -17.2               -0.01163              
 -17.6               -0.01108              
 -18.                -0.00789              
 -18.4               -0.00600              
 -18.8               -0.00692              
 -19.2               -0.00842              
 -19.6               -0.00843              
 -20.                -0.00768              
 -20.4               -0.00683              
 -20.8               -0.00664              
 -21.2               -0.00664              
 -21.6               -0.00694              
 -22.                -0.00683              
 -22.4               -0.00573              
 -22.8               -0.00372              
 -23.2               -0.00181              
 -23.6               -0.00109              
 -24.                -0.00041              
 -24.4                0.00229              
 -24.8                0.00537              
 -25.2                0.00785              
 -25.6                0.01213              
 -26.                 0.01858              
 -26.4                0.02698              
 -26.8                0.04011              
 -27.2                0.05752              
 -27.6                0.08380              
 -28.                 0.11254              
 -28.4                0.15333              
 -28.8                0.21325              
 -29.2                0.27527              
 -29.6                0.34922              
 -30.                 0.45910              
 -30.4                0.57634              
 -30.8                0.66349              
 -31.2                0.72793              
 -31.6                0.78386              
 -32.                 0.81122              
 -32.4                0.79210              
 -32.8                0.74325              
 -33.2                0.67972              
 -33.6                0.58826              
 -34.                 0.48388              
 -34.4                0.39408              
 -34.8                0.30506              
 -35.2                0.21693              
 -35.6                0.15026              
 -36.                 0.09741              
 -36.4                0.05666              
 -36.8                0.03328              
 -37.2                0.01939              
 -37.6                0.01087              
 -38.                 0.00562              
 -38.4                0.00254              
 -38.8                0.00095              
 -39.2                0.00078              
 -39.6                0.00093              
 -40.                 0.00013              
 -40.4               -0.00034              
 -40.8                0.00047              
 -41.2                0.00085              
 -41.6                0.00082              
 -42.                 0.00084              
 -42.4                0.00083              
 -42.8                0.00085              
 -43.2                0.00054              
 -43.6               -0.00103              
 -44.                -0.00404              
 -44.4               -0.00612              
 -44.8               -0.00663              
 -45.2               -0.00667              
 -45.6               -0.00660              
 -46.                -0.00603              
 -46.4               -0.00444              
 -46.8               -0.00275              
 -47.2               -0.00202              
 -47.6               -0.00171              
 -48.                 0.00021              
 -48.4                0.00352              
 -48.8                0.00761              
 -49.2                0.01078              
 -49.6                0.01249              
 -50.                 0.01445              
 -50.4                0.01567              
 -50.8                0.01629              
 -51.2                0.01745              
 -51.6                0.01630              
 -52.                 0.01122              
 -52.4                0.00526              
 -52.8                0.00007              
 -53.2               -0.00357              
 -53.6               -0.00674              
 -54.                -0.00998              
 -54.4               -0.01243              
 -54.8               -0.01306              
 -55.2               -0.01166              
 -55.6               -0.01014              
 -56.                -0.00898              
 -56.4               -0.00710              
 -56.8               -0.00386              
 -57.2               -0.00159              
 -57.6               -0.00026              
 -58.                 0.00074              
 -58.4                0.00086              
 -58.8                0.00083              
 -59.2                0.00083              
 -59.6                0.00084              
 -60.                 0.00075              
 -60.4                0.00040              
 -60.8               -0.00002              
 -61.2               -0.00010              
 -61.6               -0.00013              
 -62.                 0.00031              
 -62.4                0.00029              
 -62.8               -0.00047              
 -63.2               -0.00098              
 -63.6               -0.00105              
 -64.                -0.00103              
 -64.4               -0.00103              
 -64.8               -0.00106              
 -65.2               -0.00075              
 -65.6               -0.00017              
 -66.                -0.00037              
 -66.4               -0.00103              
 -66.8               -0.00041              
 -67.2                0.00039              
 -67.6                0.00002              
 -68.                -0.00016              
 -68.4                0.00137              
 -68.8                0.00350              
 -69.2                0.00449              
 -69.6                0.00448              
 -70.                 0.00353              
 -70.4                0.00179              
 -70.8                0.00160              
 -71.2                0.00201              
 -71.6                0.00118              
 -72.                 0.00093              
 -72.4                0.00084              
 -72.8                0.00021              
 -73.2               -0.00009              
 -73.6               -0.00010              
 -74.                -0.00003              
 -74.4                0.00035              
 -74.8                0.00046              
 -75.2               -0.00001              
 -75.6                0.00018              
 -76.                 0.00083              
 -76.4                0.00043              
 -76.8                0.00026              
 -77.2                0.00029              
 -77.6               -0.00008              
 -78.                 0.00035              
 -78.4                0.00081              
 -78.8                0.00084              
 -79.2                0.00083              
 -79.6                0.00083              
 -80.                 0.00083              
 -80.4                0.00083              
 -80.8                0.00083              
 -81.2                0.00083              
 -81.6                0.00083              
 -82.                 0.00083              
 -82.4                0.00083              
 -82.8                0.00083              
 -83.2                0.00083              
 -83.6                0.00083              
 -84.                 0.00083              
 -84.4                0.00083              
 -84.8                0.00085              
 -85.2                0.00064              
 -85.6                0.00006              
 -86.                 0.00060              
 -86.4                0.00127              
 -86.8                0.00065              
 -87.2               -0.00007              
 -87.6                0.00030              
 -88.                 0.00129              
 -88.4                0.00057              
 -88.8                0.00005              
 -89.2                0.00081              
 -89.6                0.00091              
 -90.                 0.00084              
 -90.4                0.00050              
 -90.8               -0.00043              
 -91.2               -0.00085              
 -91.6               -0.00024              
 -92.                -0.00022              
 -92.4               -0.00098              
 -92.8               -0.00057              
 -93.2                0.00039              
 -93.6                0.00082              
 -94.                 0.00084              
 -94.4                0.00083              
 -94.8                0.00083              
 -95.2                0.00083              
 -95.6                0.00083              
 -96.                 0.00083              
 -96.4                0.00083              
 -96.8                0.00084              
 -97.2                0.00074              
 -97.6                0.00028              
 -98.                -0.00006              
 -98.4               -0.00010              
 -98.8               -0.00009              
 -99.2               -0.00010              
 -99.6               -0.00010              
 -100.               -0.00009              
 -100.4              -0.00011              
 -100.8              -0.00006              
 -101.2              -0.00040              
 -101.6              -0.00078              
 -102.               -0.00000              
 -102.4               0.00078              
 -102.8               0.00043              
 -103.2              -0.00062              
 -103.6              -0.00105              
 -104.               -0.00103              
 -104.4              -0.00104              
 -104.8              -0.00103              
 -105.2              -0.00104              
 -105.6              -0.00101              
 -106.               -0.00111              
 -106.4              -0.00038              
 -106.8               0.00073              
 -107.2               0.00087              
 -107.6               0.00082              
 -108.                0.00084              
 -108.4               0.00083              
 -108.8               0.00083              
 -109.2               0.00083              
 -109.6               0.00083              
##END=
