##TITLE=              31P MAS NMR spectrum of calcined AlPO-40
##JCAMP-DX=           5.01
##DATA TYPE=          NMR SPECTRUM
##DATA CLASS=         XYDATA
##ORIGIN=             Lourenco et al. Zeolites, 18, 398-407 (1997) Figure 7a
##OWNER=              Digitized and processed by Brouwer Lab, Redeemer University
##LONG DATE=          2020/07/16 11:27:57
##SOURCE REFERENCE=   AFR-31P-Lourenco-1997-calcined
##DATA PROCESSING=    Spectrum digitized with WebPlotDigitizer and deconvoluted with Mathematica notebook

$$Sample information 
##NAMES=              AFR
##NAMES=              AlPO-40
##SAMPLE DESCRIPTION= AlPO-40, calcined

$$Bibliographic information 
##$AUTHORS=           Lourenco, J.P., Ribeiro, M.F., RamA~\264a Ribeiro, F., Rocha, J., Onida, B., Garrone, E., Gabelica, Z.
##$TITLE=             Synthesis, characterization, and catalytic properties of AlPO4-40, CoAPO-40, and ZnAPO-40
##$JOURNAL=           Zeolites
##$VOLUME=            18
##$PAGES=             398-407
##$YEAR=              1997
##$DOI=               http://dx.doi.org/10.1016/S0144-2449(97)00028-6
##$FIGURE=            Figure 7a

$$Peak information    (Positions in ppm, Relative peak areas, Peak widths in ppm, Lorentzian/Gaussian shape parameter)
##$NUM PEAKS=         4
##$PEAK LABELS=        A          B          C          D         
##$PEAK TSITES=       
##$PEAK POSITIONS=    -28.9481   -27.9218   -26.85     -26.3132   
##$PEAK AREAS=         1.         1.         1.         1.        
##$PEAK WIDTHS=        1.63705    1.63705    1.63705    1.63705   
##$PEAK SHAPES=        0.23388    0.23388    0.23388    0.23388   
##$NUMBERING REF=     Meden et al. Microporous Mater., 11, 247-251 (1997)
##$ASSIGN REF=        
##$ASSIGN METHOD=     
##$COMMENT=           Peak assignments are not available

$$Spectrum acquisition information 
##.OBSERVE NUCLEUS=   ^31P
##.OBSERVE FREQUENCY= 162.0
##.PULSE SEQUENCE=    single pulse
##.MAS FREQUENCY=     

$$Spectrum data information 
##XUNITS=             PPM
##YUNITS=             ARBITRARY UNITS
##FIRSTX=              0.46                 
##LASTX=              -40.49                
##XFACTOR=            1
##YFACTOR=            1
##NPOINTS=            456
##FIRSTY=              0.00270              

$$Spectrum data
##XYDATA=             (X++(Y..Y))
  0.46                0.00270              
  0.37                0.00299              
  0.28                0.00268              
  0.19                0.00235              
  0.1                 0.00206              
  0.01                0.00143              
 -0.08                0.00098              
 -0.17                0.00096              
 -0.26                0.00096              
 -0.35                0.00126              
 -0.44                0.00189              
 -0.53                0.00228              
 -0.62                0.00232              
 -0.71                0.00231              
 -0.8                 0.00231              
 -0.89                0.00231              
 -0.98                0.00231              
 -1.07                0.00231              
 -1.16                0.00231              
 -1.25                0.00231              
 -1.34                0.00231              
 -1.43                0.00230              
 -1.52                0.00198              
 -1.61                0.00196              
 -1.7                 0.00224              
 -1.79                0.00285              
 -1.88                0.00323              
 -1.97                0.00281              
 -2.06                0.00264              
 -2.15                0.00232              
 -2.24                0.00231              
 -2.33                0.00232              
 -2.42                0.00231              
 -2.51                0.00231              
 -2.6                 0.00231              
 -2.69                0.00231              
 -2.78                0.00231              
 -2.87                0.00231              
 -2.96                0.00231              
 -3.05                0.00232              
 -3.14                0.00231              
 -3.23                0.00233              
 -3.32                0.00194              
 -3.41                0.00131              
 -3.5                 0.00098              
 -3.59                0.00092              
 -3.68                0.00144              
 -3.77                0.00229              
 -3.86                0.00232              
 -3.95                0.00231              
 -4.04                0.00230              
 -4.13                0.00349              
 -4.22                0.00497              
 -4.31                0.00411              
 -4.4                 0.00240              
 -4.49                0.00152              
 -4.58                0.00059              
 -4.67                0.00027              
 -4.76                0.00117              
 -4.85                0.00221              
 -4.94                0.00235              
 -5.03                0.00197              
 -5.12                0.00027              
 -5.21               -0.00039              
 -5.3                -0.00039              
 -5.39                0.00016              
 -5.48                0.00141              
 -5.57                0.00223              
 -5.66                0.00232              
 -5.75                0.00234              
 -5.84                0.00160              
 -5.93                0.00033              
 -6.02               -0.00011              
 -6.11                0.00102              
 -6.2                 0.00213              
 -6.29                0.00239              
 -6.38                0.00118              
 -6.47               -0.00006              
 -6.56               -0.00037              
 -6.65               -0.00045              
 -6.74                0.00064              
 -6.83                0.00208              
 -6.92                0.00234              
 -7.01                0.00231              
 -7.1                 0.00231              
 -7.19                0.00231              
 -7.28                0.00231              
 -7.37                0.00231              
 -7.46                0.00231              
 -7.55                0.00231              
 -7.64                0.00231              
 -7.73                0.00231              
 -7.82                0.00231              
 -7.91                0.00232              
 -8.                  0.00230              
 -8.09                0.00274              
 -8.18                0.00361              
 -8.27                0.00363              
 -8.36                0.00298              
 -8.45                0.00234              
 -8.54                0.00204              
 -8.63                0.00142              
 -8.72                0.00138              
 -8.81                0.00225              
 -8.9                 0.00230              
 -8.99                0.00232              
 -9.08                0.00294              
 -9.17                0.00357              
 -9.26                0.00422              
 -9.35                0.00458              
 -9.44                0.00417              
 -9.53                0.00363              
 -9.62                0.00299              
 -9.71                0.00268              
 -9.8                 0.00232              
 -9.89                0.00277              
 -9.98                0.00368              
 -10.07               0.00288              
 -10.16               0.00231              
 -10.25               0.00231              
 -10.34               0.00231              
 -10.43               0.00231              
 -10.52               0.00231              
 -10.61               0.00231              
 -10.7                0.00231              
 -10.79               0.00231              
 -10.88               0.00231              
 -10.97               0.00321              
 -11.06               0.00453              
 -11.15               0.00497              
 -11.24               0.00509              
 -11.33               0.00344              
 -11.42               0.00230              
 -11.51               0.00231              
 -11.6                0.00289              
 -11.69               0.00414              
 -11.78               0.00495              
 -11.87               0.00503              
 -11.96               0.00502              
 -12.05               0.00502              
 -12.14               0.00502              
 -12.23               0.00502              
 -12.32               0.00502              
 -12.41               0.00502              
 -12.5                0.00502              
 -12.59               0.00502              
 -12.68               0.00502              
 -12.77               0.00502              
 -12.86               0.00502              
 -12.95               0.00502              
 -13.04               0.00502              
 -13.13               0.00502              
 -13.22               0.00502              
 -13.31               0.00502              
 -13.4                0.00502              
 -13.49               0.00502              
 -13.58               0.00502              
 -13.67               0.00502              
 -13.76               0.00502              
 -13.85               0.00502              
 -13.94               0.00502              
 -14.03               0.00502              
 -14.12               0.00502              
 -14.21               0.00502              
 -14.3                0.00502              
 -14.39               0.00502              
 -14.48               0.00503              
 -14.57               0.00503              
 -14.66               0.00533              
 -14.75               0.00623              
 -14.84               0.00727              
 -14.93               0.00746              
 -15.02               0.00726              
 -15.11               0.00767              
 -15.2                0.00773              
 -15.29               0.00743              
 -15.38               0.00678              
 -15.47               0.00665              
 -15.56               0.00727              
 -15.65               0.00771              
 -15.74               0.00729              
 -15.83               0.00603              
 -15.92               0.00600              
 -16.01               0.00667              
 -16.1                0.00670              
 -16.19               0.00726              
 -16.28               0.00769              
 -16.37               0.00849              
 -16.46               0.00943              
 -16.55               0.00975              
 -16.64               0.01004              
 -16.73               0.01062              
 -16.82               0.01174              
 -16.91               0.01343              
 -17.                 0.01493              
 -17.09               0.01586              
 -17.18               0.01646              
 -17.27               0.01821              
 -17.36               0.02051              
 -17.45               0.02253              
 -17.54               0.02509              
 -17.63               0.02678              
 -17.72               0.02805              
 -17.81               0.02902              
 -17.9                0.02940              
 -17.99               0.02939              
 -18.08               0.02983              
 -18.17               0.03030              
 -18.26               0.02966              
 -18.35               0.02807              
 -18.44               0.02706              
 -18.53               0.02734              
 -18.62               0.02716              
 -18.71               0.02671              
 -18.8                0.02669              
 -18.89               0.02669              
 -18.98               0.02669              
 -19.07               0.02791              
 -19.16               0.02928              
 -19.25               0.02947              
 -19.34               0.02938              
 -19.43               0.03015              
 -19.52               0.03225              
 -19.61               0.03510              
 -19.7                0.03767              
 -19.79               0.03933              
 -19.88               0.04063              
 -19.97               0.04231              
 -20.06               0.04525              
 -20.15               0.04813              
 -20.24               0.04971              
 -20.33               0.05027              
 -20.42               0.05278              
 -20.51               0.05645              
 -20.6                0.05864              
 -20.69               0.06034              
 -20.78               0.06161              
 -20.87               0.06224              
 -20.96               0.06312              
 -21.05               0.06493              
 -21.14               0.06668              
 -21.23               0.06805              
 -21.32               0.07065              
 -21.41               0.07178              
 -21.5                0.07368              
 -21.59               0.07595              
 -21.68               0.07724              
 -21.77               0.07900              
 -21.86               0.08116              
 -21.95               0.08291              
 -22.04               0.08431              
 -22.13               0.08525              
 -22.22               0.08619              
 -22.31               0.08717              
 -22.4                0.08763              
 -22.49               0.08767              
 -22.58               0.08765              
 -22.67               0.08802              
 -22.76               0.08864              
 -22.85               0.08958              
 -22.94               0.09030              
 -23.03               0.09038              
 -23.12               0.09037              
 -23.21               0.09034              
 -23.3                0.08969              
 -23.39               0.08905              
 -23.48               0.08874              
 -23.57               0.08815              
 -23.66               0.08766              
 -23.75               0.08806              
 -23.84               0.08875              
 -23.93               0.08971              
 -24.02               0.09096              
 -24.11               0.09251              
 -24.2                0.09410              
 -24.29               0.09616              
 -24.38               0.09864              
 -24.47               0.10333              
 -24.56               0.10972              
 -24.65               0.11835              
 -24.74               0.13249              
 -24.83               0.15007              
 -24.92               0.16941              
 -25.01               0.19993              
 -25.1                0.22948              
 -25.19               0.26205              
 -25.28               0.29919              
 -25.37               0.34497              
 -25.46               0.40266              
 -25.55               0.47010              
 -25.64               0.53512              
 -25.73               0.59424              
 -25.82               0.65943              
 -25.91               0.72047              
 -26.                 0.79183              
 -26.09               0.86139              
 -26.18               0.91653              
 -26.27               0.96875              
 -26.36               1.01474              
 -26.45               1.05879              
 -26.54               1.09736              
 -26.63               1.12474              
 -26.72               1.1361               
 -26.81               1.14099              
 -26.9                1.14355              
 -26.99               1.13664              
 -27.08               1.11979              
 -27.17               1.09395              
 -27.26               1.06651              
 -27.35               1.04049              
 -27.44               1.01471              
 -27.53               0.99261              
 -27.62               0.97249              
 -27.71               0.9532               
 -27.8                0.93686              
 -27.89               0.92511              
 -27.98               0.91891              
 -28.07               0.91324              
 -28.16               0.90715              
 -28.25               0.90241              
 -28.34               0.89768              
 -28.43               0.89095              
 -28.52               0.88056              
 -28.61               0.86391              
 -28.7                0.84373              
 -28.79               0.81279              
 -28.88               0.78412              
 -28.97               0.75327              
 -29.06               0.71439              
 -29.15               0.67500              
 -29.24               0.62459              
 -29.33               0.55924              
 -29.42               0.48982              
 -29.51               0.43855              
 -29.6                0.38769              
 -29.69               0.34249              
 -29.78               0.30305              
 -29.87               0.25639              
 -29.96               0.21681              
 -30.05               0.18619              
 -30.14               0.15759              
 -30.23               0.13720              
 -30.32               0.11519              
 -30.41               0.09479              
 -30.5                0.07888              
 -30.59               0.06700              
 -30.68               0.05856              
 -30.77               0.05199              
 -30.86               0.04569              
 -30.95               0.04041              
 -31.04               0.03786              
 -31.13               0.03622              
 -31.22               0.03495              
 -31.31               0.03333              
 -31.4                0.03176              
 -31.49               0.03053              
 -31.58               0.02836              
 -31.67               0.02684              
 -31.76               0.02670              
 -31.85               0.02670              
 -31.94               0.02670              
 -32.03               0.02636              
 -32.12               0.02512              
 -32.21               0.02351              
 -32.3                0.02267              
 -32.39               0.02266              
 -32.48               0.02144              
 -32.57               0.02022              
 -32.66               0.01993              
 -32.75               0.01996              
 -32.84               0.01882              
 -32.93               0.01738              
 -33.02               0.01684              
 -33.11               0.01432              
 -33.2                0.01315              
 -33.29               0.01315              
 -33.38               0.01315              
 -33.47               0.01320              
 -33.56               0.01243              
 -33.65               0.01095              
 -33.74               0.01046              
 -33.83               0.01045              
 -33.92               0.01044              
 -34.01               0.01043              
 -34.1                0.01050              
 -34.19               0.00973              
 -34.28               0.00825              
 -34.37               0.00775              
 -34.46               0.00774              
 -34.55               0.00773              
 -34.64               0.00773              
 -34.73               0.00774              
 -34.82               0.00773              
 -34.91               0.00775              
 -35.                 0.00735              
 -35.09               0.00669              
 -35.18               0.00638              
 -35.27               0.00666              
 -35.36               0.00731              
 -35.45               0.00745              
 -35.54               0.00691              
 -35.63               0.00563              
 -35.72               0.00502              
 -35.81               0.00502              
 -35.9                0.00502              
 -35.99               0.00502              
 -36.08               0.00502              
 -36.17               0.00503              
 -36.26               0.00501              
 -36.35               0.00501              
 -36.44               0.00406              
 -36.53               0.00275              
 -36.62               0.00233              
 -36.71               0.00227              
 -36.8                0.00306              
 -36.89               0.00485              
 -36.98               0.00502              
 -37.07               0.00502              
 -37.16               0.00503              
 -37.25               0.00482              
 -37.34               0.00371              
 -37.43               0.00237              
 -37.52               0.00228              
 -37.61               0.00267              
 -37.7                0.00362              
 -37.79               0.00459              
 -37.88               0.00504              
 -37.97               0.00460              
 -38.06               0.00334              
 -38.15               0.00272              
 -38.24               0.00404              
 -38.33               0.00500              
 -38.42               0.00480              
 -38.51               0.00361              
 -38.6                0.00232              
 -38.69               0.00230              
 -38.78               0.00231              
 -38.87               0.00231              
 -38.96               0.00231              
 -39.05               0.00231              
 -39.14               0.00231              
 -39.23               0.00231              
 -39.32               0.00231              
 -39.41               0.00231              
 -39.5                0.00231              
 -39.59               0.00231              
 -39.68               0.00231              
 -39.77               0.00231              
 -39.86               0.00231              
 -39.95               0.00231              
 -40.04               0.00231              
 -40.13               0.00231              
 -40.22               0.00231              
 -40.31               0.00232              
 -40.4                0.00230              
 -40.49               0.00233              
##END=
